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epoxy prepreg Hexply 1 1454 system, based on diglycidyl ether of bisphenol A (DEGBA)/dicyandiamid (DICY) reinforced by glass fiber. Cure kinetics of an autocatalytic-type reaction were analyzed by general form of conversion-dependent function. The characteristic feature of conversion-dependent function was determined using a reduced-plot method where the temperature-dependent reaction rate constant was analytically separated from the isothermal data. An autocatalytic kinetic model was used; it can predict the overall kinetic behavior in the whole studied cure temperature range (115-130-C). The activation energy and pre-exponential factor were determined as: E ¼ 94.8 kJ/mol and A ¼ 1.75 T 10 10 sec S1 and reaction order as 2.11 (m R n ¼ 0.65 R 1.46 ¼ 2.11). A kinetic model based on these values was developed by which the prediction is in good agreement with experimental values.","publication_date":"2009,,","publication_name":"Polym Advan Technol","grobid_abstract_attachment_id":"72297111"},"document_type":"paper","pre_hit_view_count_baseline":null,"quality":"high","language":"en","title":"Isothermal differential scanning calorimetry study of a glass/epoxy prepreg","broadcastable":true,"draft":null,"has_indexable_attachment":true,"indexable":true}}["work"]; window.loswp.workCoauthors = [84323387]; window.loswp.locale = "en"; window.loswp.countryCode = "SG"; window.loswp.cwvAbTestBucket = ""; window.loswp.designVariant = "ds_vanilla"; window.loswp.fullPageMobileSutdModalVariant = "full_page_mobile_sutd_modal"; window.loswp.useOptimizedScribd4genScript = false; window.loswp.appleClientId = 'edu.academia.applesignon';</script><script defer="" src="https://accounts.google.com/gsi/client"></script><div class="ds-loswp-container"><div 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class="ds-work-cover--ribbon-container">Download Free PDF</div><div class="ds-work-cover--ribbon-triangle"></div></button></div></div></div><div class="ds-work-card--work-information"><h1 class="ds-work-card--work-title">Isothermal differential scanning calorimetry study of a glass/epoxy prepreg</h1><div class="ds-work-card--work-authors ds-work-card--detail"><a class="ds-work-card--author js-wsj-grid-card-author ds2-5-body-md ds2-5-body-link" data-author-id="84323387" href="https://independent.academia.edu/MohammadBeheshty"><img alt="Profile image of Mohammad Beheshty" class="ds-work-card--author-avatar" src="//a.academia-assets.com/images/s65_no_pic.png" />Mohammad Beheshty</a></div><p class="ds-work-card--detail ds2-5-body-sm">2009, Polym Advan Technol</p><div class="ds-work-card--button-container"><button class="ds2-5-button js-swp-download-button" 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data-login_uri="https://www.academia.edu/registrations/google_one_tap" data-moment_callback="onGoogleOneTapEvent" id="g_id_onload"></div><div class="ds-top-related-works--grid-container"><div class="ds-related-content--container ds-top-related-works--container"><h2 class="ds-related-content--heading">Related papers</h2><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="0" data-entity-id="5305306" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/5305306/Isothermal_cure_kinetics_of_a_diglycidyl_ether_of_bisphenol_A_1_3_bisaminomethylcyclohexane_DGEBA_1_3BAC_epoxy_resin_system">Isothermal cure kinetics of a diglycidyl ether of bisphenol A/1,3-bisaminomethylcyclohexane (DGEBA/1,3BAC) epoxy resin system</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="7312082" href="https://independent.academia.edu/lopezjoaquin">joaquin lopez</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Applied Polymer Science, 1995</p><p class="ds-related-work--abstract ds2-5-body-sm">By employing differential scaning calorimetry, DSC, we have studied, under isothermal conditions, the kinetics of the cure reaction for a system containing a diglycidyl ether of bisphenol A (DGEBA) and 1,3-bisaminomethylcyclohexane (1,3-BAC) as a curing agent, over the temperature range of 60–110°C. We have determined the conversions reached at several cure temperatures and the reaction rates. The experimental data, showing an autocatalytic behavior, were compared with the model proposed by Kamal, which includes two rate constants, k1 and k2, and two reaction orders, m and n. This model gives a good description of cure kinetics up to the onset of vitrification. The activation energies for these rate constants were 44–57 kJ/mol. The reaction orders present a moderate change but their sum is in the range 2.5–3. Diffusion control is incorporated to describe the cure in the latter stages (postivitrification region). By combining the autocatalytic model and a diffusion factor, it was possible to predict the cure kinetics over the whole range of conversion. © 1995 John Wiley & Sons, Inc.</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Isothermal cure kinetics of a diglycidyl ether of bisphenol A/1,3-bisaminomethylcyclohexane (DGEBA/1,3BAC) epoxy resin system","attachmentId":49355821,"attachmentType":"pdf","work_url":"https://www.academia.edu/5305306/Isothermal_cure_kinetics_of_a_diglycidyl_ether_of_bisphenol_A_1_3_bisaminomethylcyclohexane_DGEBA_1_3BAC_epoxy_resin_system","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/5305306/Isothermal_cure_kinetics_of_a_diglycidyl_ether_of_bisphenol_A_1_3_bisaminomethylcyclohexane_DGEBA_1_3BAC_epoxy_resin_system"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="1" data-entity-id="78182261" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/78182261/Kinetic_Analysis_of_the_Curing_of_a_Partially_Biobased_Epoxy_Resin_Using_Dynamic_Differential_Scanning_Calorimetry">Kinetic Analysis of the Curing of a Partially Biobased Epoxy Resin Using Dynamic Differential Scanning Calorimetry</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="57189910" href="https://independent.academia.edu/DiegoLascano1">Diego Lascano</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Polymers, 2019</p><p class="ds-related-work--abstract ds2-5-body-sm">This research presents a cure kinetics study of an epoxy system consisting of a partially bio-sourced resin based on diglycidyl ether of bisphenol A (DGEBA) with amine hardener and a biobased reactive diluent from plants representing 31 wt %. The kinetic study has been carried out using differential scanning calorimetry (DSC) under non-isothermal conditions at different heating rates. Integral and derivative isoconversional methods or model free kinetics (MFK) have been applied to the experimental data in order to evaluate the apparent activation energy, Ea, followed by the application of the appropriate reaction model. The bio-sourced system showed activation energy that is independent of the extent of conversion, with Ea values between 57 and 62 kJ·mol−1, corresponding to typical activation energies of conventional epoxy resins. The reaction model was studied by comparing the calculated y(α) and z(α) functions with standard master plot curves. A two-parameter autocatalytic kinetic...</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Kinetic Analysis of the Curing of a Partially Biobased Epoxy Resin Using Dynamic Differential Scanning Calorimetry","attachmentId":85319008,"attachmentType":"pdf","work_url":"https://www.academia.edu/78182261/Kinetic_Analysis_of_the_Curing_of_a_Partially_Biobased_Epoxy_Resin_Using_Dynamic_Differential_Scanning_Calorimetry","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/78182261/Kinetic_Analysis_of_the_Curing_of_a_Partially_Biobased_Epoxy_Resin_Using_Dynamic_Differential_Scanning_Calorimetry"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="2" data-entity-id="23945433" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/23945433/Thermal_analysis_of_curing_process_of_epoxy_prepreg">Thermal analysis of curing process of epoxy prepreg</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="46560640" href="https://independent.academia.edu/SPang1">S. Pang</a><span>, </span><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="46248005" href="https://lsu.academia.edu/IoanNegulescu">Ioan I Negulescu</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Applied Polymer Science, 2002</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Thermal analysis of curing process of epoxy prepreg","attachmentId":44329983,"attachmentType":"pdf","work_url":"https://www.academia.edu/23945433/Thermal_analysis_of_curing_process_of_epoxy_prepreg","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/23945433/Thermal_analysis_of_curing_process_of_epoxy_prepreg"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="3" data-entity-id="27419200" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/27419200/Investigation_of_the_curing_reactions_of_some_multifunctional_epoxy_resins_using_differential_scanning_calorimetry">Investigation of the curing reactions of some multifunctional epoxy resins using differential scanning calorimetry</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="51458251" href="https://independent.academia.edu/DanRosu3">Dan Rosu</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Thermochimica Acta, 2001</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Investigation of the curing reactions of some multifunctional epoxy resins using differential scanning calorimetry","attachmentId":47675853,"attachmentType":"pdf","work_url":"https://www.academia.edu/27419200/Investigation_of_the_curing_reactions_of_some_multifunctional_epoxy_resins_using_differential_scanning_calorimetry","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/27419200/Investigation_of_the_curing_reactions_of_some_multifunctional_epoxy_resins_using_differential_scanning_calorimetry"><span 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data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Cure kinetics of epoxy resins studied by non-isothermal DSC data","attachmentId":47675852,"attachmentType":"pdf","work_url":"https://www.academia.edu/27419199/Cure_kinetics_of_epoxy_resins_studied_by_non_isothermal_DSC_data","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/27419199/Cure_kinetics_of_epoxy_resins_studied_by_non_isothermal_DSC_data"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="5" data-entity-id="33928531" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/33928531/Kinetics_of_curing_reaction_of_a_diglycidyl_ether_of_bisphenol_A_1_3_bisaminomethyl_cyclohexane_DGEBA_1_3_BAC_epoxy_resin_system">Kinetics of curing reaction of a diglycidyl ether of bisphenol A/1,3-bisaminomethyl-cyclohexane (DGEBA/1,3-BAC) epoxy resin system</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="39990380" href="https://independent.academia.edu/CamiloRamirez41">Camilo Ramirez</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Thermal Analysis, 1996</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Kinetics of curing reaction of a diglycidyl ether of bisphenol A/1,3-bisaminomethyl-cyclohexane (DGEBA/1,3-BAC) epoxy resin system","attachmentId":53896773,"attachmentType":"pdf","work_url":"https://www.academia.edu/33928531/Kinetics_of_curing_reaction_of_a_diglycidyl_ether_of_bisphenol_A_1_3_bisaminomethyl_cyclohexane_DGEBA_1_3_BAC_epoxy_resin_system","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/33928531/Kinetics_of_curing_reaction_of_a_diglycidyl_ether_of_bisphenol_A_1_3_bisaminomethyl_cyclohexane_DGEBA_1_3_BAC_epoxy_resin_system"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="6" data-entity-id="14955533" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/14955533/Mechanism_and_Kinetics_of_Epoxy_Amine_Cure_Studied_by_Differential_Scanning_Calorimetry">Mechanism and Kinetics of Epoxy−Amine Cure Studied by Differential Scanning Calorimetry</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="33950313" href="https://landaverde.academia.edu/NicolasSbirrazzuoli">Nicolas Sbirrazzuoli</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Macromolecules, 1996</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Mechanism and Kinetics of Epoxy−Amine Cure Studied by Differential Scanning 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href="https://independent.academia.edu/IvanaPartridge">Ivana Partridge</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Applied Polymer Science, 2012</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Cure kinetics, glass transition temperature development, and dielectric spectroscopy of a low temperature cure epoxy/amine system","attachmentId":39520716,"attachmentType":"pdf","work_url":"https://www.academia.edu/17460090/Cure_kinetics_glass_transition_temperature_development_and_dielectric_spectroscopy_of_a_low_temperature_cure_epoxy_amine_system","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline 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class="ds-related-work--metadata ds2-5-body-xs">1984</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Curing reaction of epoxy resins with diamines","attachmentId":78561091,"attachmentType":"pdf","work_url":"https://www.academia.edu/67879082/Curing_reaction_of_epoxy_resins_with_diamines","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-related-work-grid-card-view-pdf" href="https://www.academia.edu/67879082/Curing_reaction_of_epoxy_resins_with_diamines"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div 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data-author-id="200819124" href="https://independent.academia.edu/CyrilSladic">Cyril Sladic</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Macromolecular Chemistry and Physics, 2003</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"A Study of Epoxy-Amine Cure Kinetics by Combining Isoconversional Analysis with Temperature Modulated DSC and Dynamic Rheometry","attachmentId":70955762,"attachmentType":"pdf","work_url":"https://www.academia.edu/54730958/A_Study_of_Epoxy_Amine_Cure_Kinetics_by_Combining_Isoconversional_Analysis_with_Temperature_Modulated_DSC_and_Dynamic_Rheometry","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline 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