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"https://www.academia.edu/login?post_login_redirect_url=https%3A%2F%2Fwww.academia.edu%2F4285085%2FCure_Kinetics_Study_of_Two_Epoxy_Systems_with_Fourier_Tranform_Infrared_Spectroscopy_FTIR_and_Differential_Scanning_Calorimetry_DSC_%3Fshow_translation%3Dtrue"; window.loswp.previewableAttachments = [{"id":31753253,"identifier":"Attachment_31753253","shouldShowBulkDownload":false}]; window.loswp.shouldDetectTimezone = true; window.loswp.shouldShowBulkDownload = true; window.loswp.showSignupCaptcha = false window.loswp.willEdgeCache = false; window.loswp.work = {"work":{"id":4285085,"created_at":"2013-08-20T18:41:57.896-07:00","from_world_paper_id":null,"updated_at":"2024-11-15T06:25:58.837-08:00","_data":{"grobid_abstract":"This work was aimed at the study of cure kinetics of two commercial thermosetting epoxy systems, Epikote resin 816 LV/Epikure F205 and Epikote resin 240/Epikure F205, by Fourier Tranform Infrared Spectroscopy (FTIR) and Differential Scanning Calorimetry (DSC). The studied systems consist of a resin (A), based on a diglycidyl ether of bisphenol A and a hardener (B) based on the Isophorodiamine (IPDA) a cycloaliphatic diamine. These systems are used for the building and civil engineering industries, e.g. flooring compounds, adhesives, mortars and grouts. FTIR spectroscopy was employed to investigate the isothermal curing kinetics at 30, 50 or 70 • C and DSC analysis to study the non-isothermal curing kinetics at different heating rates 2.5, 5, 10 and 20 • C/min, from 20 to 300 • C. A kinetic model was employed to simulate the FTIR isothermal experimental data using two kinetic rate constants and incorporating also diffusion control at high degrees of conversion. Finally, the variation of the effective activation energy with the extent of curing was estimated using isoconversional analysis of non-isothermal DSC data.","grobid_abstract_attachment_id":"31753253"},"document_type":"paper","pre_hit_view_count_baseline":0,"quality":"high","language":"en","title":"Cure Kinetics Study of Two Epoxy Systems with Fourier Tranform Infrared Spectroscopy (FTIR) and Differential Scanning Calorimetry (DSC)","broadcastable":true,"draft":null,"has_indexable_attachment":true,"indexable":true}}["work"]; window.loswp.workCoauthors = [5189413]; window.loswp.locale = "en"; window.loswp.countryCode = "SG"; window.loswp.cwvAbTestBucket = ""; window.loswp.designVariant = "ds_vanilla"; window.loswp.fullPageMobileSutdModalVariant = "full_page_mobile_sutd_modal"; window.loswp.useOptimizedScribd4genScript = false; window.loginModal = {}; window.loginModal.appleClientId = 'edu.academia.applesignon'; window.userInChina = "false";</script><script defer="" src="https://accounts.google.com/gsi/client"></script><div class="ds-loswp-container"><div class="ds-work-card--grid-container"><div class="ds-work-card--container js-loswp-work-card"><div class="ds-work-card--cover"><div class="ds-work-cover--wrapper"><div class="ds-work-cover--container"><button class="ds-work-cover--clickable js-swp-download-button" data-signup-modal="{"location":"swp-splash-paper-cover","attachmentId":31753253,"attachmentType":"pdf"}"><img alt="First page of “Cure Kinetics Study of Two Epoxy Systems with Fourier Tranform Infrared Spectroscopy (FTIR) and Differential Scanning Calorimetry (DSC)”" class="ds-work-cover--cover-thumbnail" src="https://0.academia-photos.com/attachment_thumbnails/31753253/mini_magick20220707-10966-1ccv7d4.png?1657223151" /><img alt="PDF Icon" class="ds-work-cover--file-icon" src="//a.academia-assets.com/images/single_work_splash/adobe_icon.svg" /><div class="ds-work-cover--hover-container"><span class="material-symbols-outlined" style="font-size: 20px" translate="no">download</span><p>Download Free PDF</p></div><div class="ds-work-cover--ribbon-container">Download Free PDF</div><div class="ds-work-cover--ribbon-triangle"></div></button></div></div></div><div class="ds-work-card--work-information"><h1 class="ds-work-card--work-title">Cure Kinetics Study of Two Epoxy Systems with Fourier Tranform Infrared Spectroscopy (FTIR) and Differential Scanning Calorimetry (DSC)</h1><div class="ds-work-card--work-authors ds-work-card--detail"><a class="ds-work-card--author js-wsj-grid-card-author ds2-5-body-md ds2-5-body-link" data-author-id="5189413" href="https://auth.academia.edu/%CE%95%CE%99%CE%A1%CE%97%CE%9D%CE%97%CE%A3%CE%B9%CE%B4%CE%B5%CF%81%CE%AF%CE%B4%CE%BF%CF%85"><img alt="Profile image of Ειρήνη Σιδερίδου-Καραγιαννίδου" class="ds-work-card--author-avatar" src="https://0.academia-photos.com/5189413/2286327/37608585/s65__._-_.png" />Ειρήνη Σιδερίδου-Καραγιαννίδου</a></div><div class="ds-work-card--detail"><div class="ds-work-card--work-metadata"><div class="ds-work-card--work-metadata__stat"><span class="material-symbols-outlined" style="font-size: 20px" translate="no">visibility</span><p class="ds2-5-body-sm" id="work-metadata-view-count">…</p></div><div class="ds-work-card--work-metadata__stat"><span class="material-symbols-outlined" style="font-size: 20px" translate="no">description</span><p class="ds2-5-body-sm">10 pages</p></div><div class="ds-work-card--work-metadata__stat"><span class="material-symbols-outlined" style="font-size: 20px" translate="no">link</span><p class="ds2-5-body-sm">1 file</p></div></div><script>(async () => { const workId = 4285085; 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if (!viewCountBody) { throw new Error('Failed to find work views element'); } viewCountBody.textContent = `${commaizedViewCount} views`; } catch (error) { // Remove the whole views element if there was some issue parsing. document.getElementById('work-metadata-view-count')?.parentNode?.remove(); throw new Error(`Failed to parse view count: ${viewCount}`, error); } }; // If the DOM is still loading, wait for it to be ready before updating the view count. if (document.readyState === "loading") { document.addEventListener('DOMContentLoaded', () => { updateViewCount(viewCount); }); // Otherwise, just update it immediately. } else { updateViewCount(viewCount); } })();</script></div><p class="ds-work-card--work-abstract ds-work-card--detail ds2-5-body-md">This work was aimed at the study of cure kinetics of two commercial thermosetting epoxy systems, Epikote resin 816 LV/Epikure F205 and Epikote resin 240/Epikure F205, by Fourier Tranform Infrared Spectroscopy (FTIR) and Differential Scanning Calorimetry (DSC). The studied systems consist of a resin (A), based on a diglycidyl ether of bisphenol A and a hardener (B) based on the Isophorodiamine (IPDA) a cycloaliphatic diamine. These systems are used for the building and civil engineering industries, e.g. flooring compounds, adhesives, mortars and grouts. FTIR spectroscopy was employed to investigate the isothermal curing kinetics at 30, 50 or 70 • C and DSC analysis to study the non-isothermal curing kinetics at different heating rates 2.5, 5, 10 and 20 • C/min, from 20 to 300 • C. A kinetic model was employed to simulate the FTIR isothermal experimental data using two kinetic rate constants and incorporating also diffusion control at high degrees of conversion. Finally, the variation of the effective activation energy with the extent of curing was estimated using isoconversional analysis of non-isothermal DSC data.</p><div class="ds-work-card--button-container"><button class="ds2-5-button js-swp-download-button" data-signup-modal="{"location":"continue-reading-button--work-card","attachmentId":31753253,"attachmentType":"pdf","workUrl":"https://www.academia.edu/4285085/Cure_Kinetics_Study_of_Two_Epoxy_Systems_with_Fourier_Tranform_Infrared_Spectroscopy_FTIR_and_Differential_Scanning_Calorimetry_DSC_"}">See full PDF</button><button class="ds2-5-button ds2-5-button--secondary js-swp-download-button" data-signup-modal="{"location":"download-pdf-button--work-card","attachmentId":31753253,"attachmentType":"pdf","workUrl":"https://www.academia.edu/4285085/Cure_Kinetics_Study_of_Two_Epoxy_Systems_with_Fourier_Tranform_Infrared_Spectroscopy_FTIR_and_Differential_Scanning_Calorimetry_DSC_"}"><span class="material-symbols-outlined" style="font-size: 20px" translate="no">download</span>Download PDF</button></div><div class="ds-signup-banner-trigger-container"><div class="ds-signup-banner-trigger ds-signup-banner-trigger-control"></div></div><div class="ds-signup-banner ds-signup-banner-control"><div id="ds-signup-banner-close-button"><button class="ds2-5-button ds2-5-button--secondary ds2-5-button--inverse"><span class="material-symbols-outlined" style="font-size: 20px" translate="no">close</span></button></div><div class="ds-signup-banner-ctas"><img src="//a.academia-assets.com/images/academia-logo-capital-white.svg" /><h4 class="ds2-5-heading-serif-sm">Sign up for access to the world's latest research</h4><button class="ds2-5-button ds2-5-button--inverse ds2-5-button--full-width js-swp-download-button" data-signup-modal="{"location":"signup-banner"}">Sign up for free<span class="material-symbols-outlined" style="font-size: 20px" translate="no">arrow_forward</span></button></div><div class="ds-signup-banner-divider"></div><div class="ds-signup-banner-reasons"><div class="ds-signup-banner-reasons-item"><span class="material-symbols-outlined" style="font-size: 24px" translate="no">check</span><span>Get notified about relevant papers</span></div><div class="ds-signup-banner-reasons-item"><span class="material-symbols-outlined" style="font-size: 24px" translate="no">check</span><span>Save papers to use in your research</span></div><div class="ds-signup-banner-reasons-item"><span class="material-symbols-outlined" style="font-size: 24px" translate="no">check</span><span>Join the discussion with peers</span></div><div class="ds-signup-banner-reasons-item"><span class="material-symbols-outlined" style="font-size: 24px" translate="no">check</span><span>Track your impact</span></div></div></div><script>(() => { // Set up signup banner show/hide behavior: // 1. 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The kinetic parameters of the curing process were determined by isoconversional method given by Ma Âlek for the kinetic analysis of the data obtained by the thermal treatment. A two-parameter (m, n) autocatalytic model (S Ï esta Âk±Berggren equation) was found to be the most adequate selected to describe the cure kinetics of the studied epoxy resins. Reactive diluent decreases both the activation energy and the cure kinetic parameters. Non-isothermal DSC curves obtained using the experimental data show a good agreement with that theoretically calculated. #</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Cure kinetics of epoxy resins studied by non-isothermal DSC data","attachmentId":47675852,"attachmentType":"pdf","work_url":"https://www.academia.edu/27419199/Cure_kinetics_of_epoxy_resins_studied_by_non_isothermal_DSC_data","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/27419199/Cure_kinetics_of_epoxy_resins_studied_by_non_isothermal_DSC_data"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="1" data-entity-id="27419200" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/27419200/Investigation_of_the_curing_reactions_of_some_multifunctional_epoxy_resins_using_differential_scanning_calorimetry">Investigation of the curing reactions of some multifunctional epoxy resins using differential scanning calorimetry</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="51458251" href="https://independent.academia.edu/DanRosu3">Dan Rosu</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Thermochimica Acta, 2001</p><p class="ds-related-work--abstract ds2-5-body-sm">Curing reaction of three tetrafunctional epoxy resins in the presence of tetraethylene tetramine was examined by differential scanning calorimetry at different heating rates. The kinetic parameters of the curing reaction were determined using various computational methods (Barrett, Borchardt±Daniels and Kissinger). The heating rate shows a great in¯uence on the curing process. The activation energy varied in the range 43±80 kJ/mol, and the order of the curing reaction is observed to be %1.0 with slight variations. #</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Investigation of the curing reactions of some multifunctional epoxy resins using differential scanning calorimetry","attachmentId":47675853,"attachmentType":"pdf","work_url":"https://www.academia.edu/27419200/Investigation_of_the_curing_reactions_of_some_multifunctional_epoxy_resins_using_differential_scanning_calorimetry","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/27419200/Investigation_of_the_curing_reactions_of_some_multifunctional_epoxy_resins_using_differential_scanning_calorimetry"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="2" data-entity-id="73017526" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/73017526/Curing_Kinetic_of_an_Epoxy_amine_System_by_Calorimetric_Method_and_FT_IR_Spectroscopy">Curing Kinetic of an Epoxy-amine System by Calorimetric Method and FT-IR Spectroscopy</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="36908407" href="https://independent.academia.edu/LuminitaWagner">Luminita Wagner</a></div><p class="ds-related-work--metadata ds2-5-body-xs">2009</p><p class="ds-related-work--abstract ds2-5-body-sm">The study presents experimental data regarding the curing reactions of some epoxy systems consisting of diglycidyl ethers of bisphenol A and different amine hardeners at room temperature and at microwaves. The curing reaction of the system composed of an epoxy resin (ROPOXID P 401) and 4,4’-diaminodiphenylmethane (HT 972) was studied by differential scanning calorimetry (DSC) and FT-IR spectroscopy. The degree of conversion obtained using FT-IR method is very close to that obtained using calorimetric method.</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Curing Kinetic of an Epoxy-amine System by Calorimetric Method and FT-IR Spectroscopy","attachmentId":81706880,"attachmentType":"pdf","work_url":"https://www.academia.edu/73017526/Curing_Kinetic_of_an_Epoxy_amine_System_by_Calorimetric_Method_and_FT_IR_Spectroscopy","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/73017526/Curing_Kinetic_of_an_Epoxy_amine_System_by_Calorimetric_Method_and_FT_IR_Spectroscopy"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="3" data-entity-id="103512507" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/103512507/Analyzing_the_network_formation_and_curing_kinetics_of_epoxy_resins_by_in_situ_near_infrared_measurements_with_variable_heating_rates">Analyzing the network formation and curing kinetics of epoxy resins by in situ near-infrared measurements with variable heating rates</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="51009502" href="https://independent.academia.edu/SturmHeinz">Heinz Sturm</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Thermochimica Acta, 2015</p><p class="ds-related-work--abstract ds2-5-body-sm">Near-infrared spectroscopy (NIR) turned out to be well suited for analyzing the degree of cure for epoxy systems. In contrast to Dynamic Scanning Calorimetry (DSC), where the degree of epoxy conversion is determined indirectly by the released heat of reaction, NIR spectroscopy is able to determine the conversion directly by analyzing structural changes. Therefore a new heatable NIR cell was equipped with an integrated thermocouple, which enables the real sample temperature to be controlled and monitored in situ during epoxy curing. Dynamic scans at different heating rates were used for kinetic modelling, to define kinetic parameters and to predict real curing processes. The kinetic models and their parameters were validated with an isothermal and a more complex multi-step curing scenario. Two available commercial epoxy systems based on DGEBA were used with an anhydride and with an amine hardener. NIR results were compared with DSC data. The simulated conversion predicted with a model *Manuscript A c c e p t e d M a n u s c r i p t 2 fitted on the basis of NIR and DSC dynamic scans showed good agreement with the conversion measured in the isothermal curing validation test.. Due to the proven reliability of NIR in measuring the reaction progress of curing, it can be considered a versatile measurement system for in situ monitoring of component production in the automotive, aerospace and wind energy sectors.</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Analyzing the network formation and curing kinetics of epoxy resins by in situ near-infrared measurements with variable heating rates","attachmentId":103500125,"attachmentType":"pdf","work_url":"https://www.academia.edu/103512507/Analyzing_the_network_formation_and_curing_kinetics_of_epoxy_resins_by_in_situ_near_infrared_measurements_with_variable_heating_rates","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/103512507/Analyzing_the_network_formation_and_curing_kinetics_of_epoxy_resins_by_in_situ_near_infrared_measurements_with_variable_heating_rates"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="4" data-entity-id="78182261" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/78182261/Kinetic_Analysis_of_the_Curing_of_a_Partially_Biobased_Epoxy_Resin_Using_Dynamic_Differential_Scanning_Calorimetry">Kinetic Analysis of the Curing of a Partially Biobased Epoxy Resin Using Dynamic Differential Scanning Calorimetry</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="57189910" href="https://independent.academia.edu/DiegoLascano1">Diego Lascano</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Polymers, 2019</p><p class="ds-related-work--abstract ds2-5-body-sm">This research presents a cure kinetics study of an epoxy system consisting of a partially bio-sourced resin based on diglycidyl ether of bisphenol A (DGEBA) with amine hardener and a biobased reactive diluent from plants representing 31 wt %. The kinetic study has been carried out using differential scanning calorimetry (DSC) under non-isothermal conditions at different heating rates. Integral and derivative isoconversional methods or model free kinetics (MFK) have been applied to the experimental data in order to evaluate the apparent activation energy, Ea, followed by the application of the appropriate reaction model. The bio-sourced system showed activation energy that is independent of the extent of conversion, with Ea values between 57 and 62 kJ·mol−1, corresponding to typical activation energies of conventional epoxy resins. The reaction model was studied by comparing the calculated y(α) and z(α) functions with standard master plot curves. A two-parameter autocatalytic kinetic...</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Kinetic Analysis of the Curing of a Partially Biobased Epoxy Resin Using Dynamic Differential Scanning Calorimetry","attachmentId":85319008,"attachmentType":"pdf","work_url":"https://www.academia.edu/78182261/Kinetic_Analysis_of_the_Curing_of_a_Partially_Biobased_Epoxy_Resin_Using_Dynamic_Differential_Scanning_Calorimetry","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/78182261/Kinetic_Analysis_of_the_Curing_of_a_Partially_Biobased_Epoxy_Resin_Using_Dynamic_Differential_Scanning_Calorimetry"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="5" data-entity-id="88555489" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/88555489/Alternating_differential_scanning_calorimetry_Isothermal_curing_of_the_epoxy_resin">Alternating differential scanning calorimetry: Isothermal curing of the epoxy resin</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="16092051" href="https://independent.academia.edu/IdaPoljansek">Ida Poljansek</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Acta Chimica Slovenica, 2003</p><p class="ds-related-work--abstract ds2-5-body-sm">In this study the quasi-isothermal curing of diepoxide resin with triamine was investigated by alternating differential scanning calorimetry (ADSC), which is a temperature modulated DSC technique. The complex heat capacity measurements were carried out to analyze the vitrification process at curing temperatures (T c) below the maximum glass transition of the fully cured epoxy. The modulus of the complex heat capacity /c p * / increases until a maximum and then an abrupt decay of /c p * /, due to the vitrification of the system was observed. The phase angle and out-of phase heat capacity show an asymmetric wide peak during the vitrification process. The abrupt decay of /c p * / at vitrification decreases with the increase of T c and disappears at temperature T g∝. The decay of /c p * / during vitrification may be normalized between unity and zero by defining a mobility factor. This mobility factor was used to simulate the reaction rate during the stage where the reaction is controlled by diffusion. The observed reaction rate was simulated by the product of the kinetic reaction rate, determined by the auto-catalytic model, and the mobility factor.</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Alternating differential scanning calorimetry: Isothermal curing of the epoxy resin","attachmentId":92507903,"attachmentType":"pdf","work_url":"https://www.academia.edu/88555489/Alternating_differential_scanning_calorimetry_Isothermal_curing_of_the_epoxy_resin","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/88555489/Alternating_differential_scanning_calorimetry_Isothermal_curing_of_the_epoxy_resin"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="6" data-entity-id="4084167" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/4084167/Cure_kinetics_of_ternary_blends_of_epoxy_resins_studied_by_nonisothermal_DSC_data">Cure kinetics of ternary blends of epoxy resins studied by nonisothermal DSC data</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="4924324" href="https://independent.academia.edu/GarimaTripathi">Garima Tripathi</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Applied Polymer Science, 2009</p><p class="ds-related-work--abstract ds2-5-body-sm">The curing kinetics of blends of diglycidyl ether of bisphenol A (DGEBA), cycloaliphatic epoxy resins, and carboxyl-terminated butadiene-acrylonitrile random copolymer (CTBN) in presence of 4,4′-diamino diphenyl sulfone (DDS) as the curing agent was studied by nonisothermal differential scanning calorimetry (DSC) technique at different heating rates. The kinetic parameters of the curing process were determined by isoconversional method given by Malek for the kinetic analysis of the data obtained by the thermal treatment. A two-parameter (m, n) autocatalytic model (Sestak-Berggren equation) was found to be the most adequate selected to describe the cure kinetics of the studied epoxy resins. The values of Ea were found to be 88.6 kJ mol−1 and 61.6 kJ mol−1, respectively, for the studied two sample series. Nonisothermal DSC curves obtained using the experimental data show a good agreement with that theoretically calculated. © 2009 Wiley Periodicals, Inc. J Appl Polym Sci, 2009</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Cure kinetics of ternary blends of epoxy resins studied by nonisothermal DSC data","attachmentId":50042789,"attachmentType":"pdf","work_url":"https://www.academia.edu/4084167/Cure_kinetics_of_ternary_blends_of_epoxy_resins_studied_by_nonisothermal_DSC_data","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/4084167/Cure_kinetics_of_ternary_blends_of_epoxy_resins_studied_by_nonisothermal_DSC_data"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="7" data-entity-id="14955533" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/14955533/Mechanism_and_Kinetics_of_Epoxy_Amine_Cure_Studied_by_Differential_Scanning_Calorimetry">Mechanism and Kinetics of Epoxy−Amine Cure Studied by Differential Scanning Calorimetry</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="33950313" href="https://landaverde.academia.edu/NicolasSbirrazzuoli">Nicolas Sbirrazzuoli</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Macromolecules, 1996</p><p class="ds-related-work--abstract ds2-5-body-sm">The isoconversional kinetic analysis has been applied to nonisothermal DSC data on the cure of an epoxynovolac resin. The process reveals a dependence of the activation energy (ER) on conversion (R). The shape of the dependence has been interpreted in the terms of the reaction mechanisms. It has been found that the model dR/dt ) (k1 + R m k2)(1 -R) n used for the kinetically controlled cure gives rise to the dependence of ER on R similar to the experimentally found one. To completely describe the diffusioncontrolled cure, the effect of both T and R on the change in diffusivity has been taken into account. The equation for the specific rate constant of diffusion, kD(T,R) ) Do exp(-ED/RT + KR), has been induced. Its use allows us to obtain a model dependence of ER on R closely matching the experimental one. A technique of predicting isothermal cure from the sole dependence of ER on R has been considered.</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Mechanism and Kinetics of Epoxy−Amine Cure Studied by Differential Scanning Calorimetry","attachmentId":43703683,"attachmentType":"pdf","work_url":"https://www.academia.edu/14955533/Mechanism_and_Kinetics_of_Epoxy_Amine_Cure_Studied_by_Differential_Scanning_Calorimetry","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/14955533/Mechanism_and_Kinetics_of_Epoxy_Amine_Cure_Studied_by_Differential_Scanning_Calorimetry"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="8" data-entity-id="5305306" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/5305306/Isothermal_cure_kinetics_of_a_diglycidyl_ether_of_bisphenol_A_1_3_bisaminomethylcyclohexane_DGEBA_1_3BAC_epoxy_resin_system">Isothermal cure kinetics of a diglycidyl ether of bisphenol A/1,3-bisaminomethylcyclohexane (DGEBA/1,3BAC) epoxy resin system</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="7312082" href="https://independent.academia.edu/lopezjoaquin">joaquin lopez</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Applied Polymer Science, 1995</p><p class="ds-related-work--abstract ds2-5-body-sm">By employing differential scaning calorimetry, DSC, we have studied, under isothermal conditions, the kinetics of the cure reaction for a system containing a diglycidyl ether of bisphenol A (DGEBA) and 1,3-bisaminomethylcyclohexane (1,3-BAC) as a curing agent, over the temperature range of 60–110°C. We have determined the conversions reached at several cure temperatures and the reaction rates. The experimental data, showing an autocatalytic behavior, were compared with the model proposed by Kamal, which includes two rate constants, k1 and k2, and two reaction orders, m and n. This model gives a good description of cure kinetics up to the onset of vitrification. The activation energies for these rate constants were 44–57 kJ/mol. The reaction orders present a moderate change but their sum is in the range 2.5–3. Diffusion control is incorporated to describe the cure in the latter stages (postivitrification region). By combining the autocatalytic model and a diffusion factor, it was possible to predict the cure kinetics over the whole range of conversion. © 1995 John Wiley & Sons, Inc.</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Isothermal cure kinetics of a diglycidyl ether of bisphenol A/1,3-bisaminomethylcyclohexane (DGEBA/1,3BAC) epoxy resin system","attachmentId":49355821,"attachmentType":"pdf","work_url":"https://www.academia.edu/5305306/Isothermal_cure_kinetics_of_a_diglycidyl_ether_of_bisphenol_A_1_3_bisaminomethylcyclohexane_DGEBA_1_3BAC_epoxy_resin_system","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/5305306/Isothermal_cure_kinetics_of_a_diglycidyl_ether_of_bisphenol_A_1_3_bisaminomethylcyclohexane_DGEBA_1_3BAC_epoxy_resin_system"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="9" data-entity-id="27419197" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/27419197/Cure_kinetics_of_a_liquid_crystalline_epoxy_resin_studied_by_non_isothermal_data">Cure kinetics of a liquid-crystalline epoxy resin studied by non-isothermal data</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="51458251" href="https://independent.academia.edu/DanRosu3">Dan Rosu</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Polymer Testing, 2004</p><p class="ds-related-work--abstract ds2-5-body-sm">The curing kinetics of diglycidyl ether of 4,4Ј-bisphenol (DGEBP) epoxy mesogenic resin in the presence of sulphanilamide (SAA) was studied by non-isothermal differential scanning calorimetry (DSC) at different heating rates. At low heating rates (2-5°C min Ϫ1 ), the curing reaction takes place by two processes evidenced by the presence of a double peak on the DSC thermograms. The first process is due to the reaction of primary amine with epoxy, while the second one corresponds to the formation of the crosslinked network with liquid crystalline (LC) properties by the attack of the secondary amine previously formed onto the epoxide groups unreacted in the first stage of the reaction. An activation energy (E a = 59 kJ mol Ϫ1 ) was evaluated for the second process and an autocatalytic kinetic model (Š esták-Berggren equation) was proposed to better describe the cure kinetics of the studied system. The theoretical DSC curves calculated using the kinetic parameters determined in non-isothermal conditions show good agreement with those experimentally determined. </p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Cure kinetics of a liquid-crystalline epoxy resin studied by non-isothermal data","attachmentId":47675861,"attachmentType":"pdf","work_url":"https://www.academia.edu/27419197/Cure_kinetics_of_a_liquid_crystalline_epoxy_resin_studied_by_non_isothermal_data","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/27419197/Cure_kinetics_of_a_liquid_crystalline_epoxy_resin_studied_by_non_isothermal_data"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div></div></div><div class="ds-sticky-ctas--wrapper js-loswp-sticky-ctas hidden"><div class="ds-sticky-ctas--grid-container"><div class="ds-sticky-ctas--container"><button class="ds2-5-button js-swp-download-button" data-signup-modal="{"location":"continue-reading-button--sticky-ctas","attachmentId":31753253,"attachmentType":"pdf","workUrl":null}">See full PDF</button><button class="ds2-5-button ds2-5-button--secondary js-swp-download-button" data-signup-modal="{"location":"download-pdf-button--sticky-ctas","attachmentId":31753253,"attachmentType":"pdf","workUrl":null}"><span class="material-symbols-outlined" style="font-size: 20px" translate="no">download</span>Download PDF</button></div></div></div><div class="ds-below-fold--grid-container"><div class="ds-work--container js-loswp-embedded-document"><div class="attachment_preview" data-attachment="Attachment_31753253" style="display: none"><div class="js-scribd-document-container"><div class="scribd--document-loading js-scribd-document-loader" style="display: block;"><img alt="Loading..." src="//a.academia-assets.com/images/loaders/paper-load.gif" /><p>Loading Preview</p></div></div><div style="text-align: center;"><div class="scribd--no-preview-alert js-preview-unavailable"><p>Sorry, preview is currently unavailable. You can download the paper by clicking the button above.</p></div></div></div></div><div class="ds-sidebar--container js-work-sidebar"><div class="ds-related-content--container"><h2 class="ds-related-content--heading">Related papers</h2><div class="ds-related-work--container js-related-work-sidebar-card" data-collection-position="0" data-entity-id="4945928" data-sort-order="default"><a class="ds-related-work--title js-related-work-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/4945928/Kinetics_Study_of_Curing_by_FT_IR_and_Dynamic_Thermomechanical_Analysis_of_the_Glass_Conservation_Epoxy_Resin_HXTAL_NYL_1">Kinetics Study of Curing by FT-IR and Dynamic Thermomechanical Analysis of the Glass-Conservation Epoxy Resin HXTAL-NYL-1</a><div class="ds-related-work--metadata"><a class="js-related-work-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="5189413" href="https://auth.academia.edu/%CE%95%CE%99%CE%A1%CE%97%CE%9D%CE%97%CE%A3%CE%B9%CE%B4%CE%B5%CF%81%CE%AF%CE%B4%CE%BF%CF%85">Ειρήνη Σιδερίδου-Καραγιαννίδου</a></div><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Kinetics Study of Curing by FT-IR and Dynamic Thermomechanical Analysis of the Glass-Conservation Epoxy Resin HXTAL-NYL-1","attachmentId":32201975,"attachmentType":"pdf","work_url":"https://www.academia.edu/4945928/Kinetics_Study_of_Curing_by_FT_IR_and_Dynamic_Thermomechanical_Analysis_of_the_Glass_Conservation_Epoxy_Resin_HXTAL_NYL_1","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-related-work-grid-card-view-pdf" href="https://www.academia.edu/4945928/Kinetics_Study_of_Curing_by_FT_IR_and_Dynamic_Thermomechanical_Analysis_of_the_Glass_Conservation_Epoxy_Resin_HXTAL_NYL_1"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-related-work-sidebar-card" data-collection-position="1" data-entity-id="78182275" data-sort-order="default"><a class="ds-related-work--title js-related-work-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/78182275/Kinetic_Analysis_of_the_Curing_Process_of_Biobased_Epoxy_Resin_from_Epoxidized_Linseed_Oil_by_Dynamic_Differential_Scanning_Calorimetry">Kinetic Analysis of the Curing Process of Biobased Epoxy Resin from Epoxidized Linseed Oil by Dynamic Differential Scanning Calorimetry</a><div class="ds-related-work--metadata"><a class="js-related-work-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="57189910" href="https://independent.academia.edu/DiegoLascano1">Diego Lascano</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Polymers, 2021</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Kinetic Analysis of the Curing Process of Biobased Epoxy Resin from Epoxidized Linseed Oil by Dynamic Differential Scanning Calorimetry","attachmentId":85319022,"attachmentType":"pdf","work_url":"https://www.academia.edu/78182275/Kinetic_Analysis_of_the_Curing_Process_of_Biobased_Epoxy_Resin_from_Epoxidized_Linseed_Oil_by_Dynamic_Differential_Scanning_Calorimetry","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline 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