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}) } })();</script></ul></li></ul></div></div><div class="u-borderBottom1 u-borderColorGrayLighter"><div class="clearfix u-pv7x u-mb0x js-work-card work_17802921 coauthored" data-work_id="17802921" itemscope="itemscope" itemtype="https://schema.org/ScholarlyArticle"><div class="header"><div class="title u-fontSerif u-fs22 u-lineHeight1_3"><a class="u-tcGrayDarkest js-work-link" href="https://www.academia.edu/17802921/Structural_and_thermal_investigation_of_gadolinium_gallium_mixed_oxides_obtained_by_coprecipitation_Observation_of_a_new_metastable_phase">Structural and thermal investigation of gadolinium gallium mixed oxides obtained by coprecipitation: Observation of a new metastable phase</a></div></div><div class="u-pb4x u-mt3x"><div class="summary u-fs14 u-fw300 u-lineHeight1_5 u-tcGrayDarkest"><div class="summarized">Polycrystalline gadolinium gallium mixed oxides were prepared by coprecipitation and annealing at various temperatures below 1000° C. The oxide materials appear to be X-ray amorphous after a heat treatment at 500° C for 30h, but after 30h... <a class="more_link u-tcGrayDark u-linkUnstyled" data-container=".work_17802921" data-show=".complete" data-hide=".summarized" data-more-link-behavior="true" href="#">more</a></div><div class="complete hidden">Polycrystalline gadolinium gallium mixed oxides were prepared by coprecipitation and annealing at various temperatures below 1000° C. The oxide materials appear to be X-ray amorphous after a heat treatment at 500° C for 30h, but after 30h at 800 and 900° C a major, unreported, hexagonal phase, isostructural with TAlO3 compounds (where T= Y, Eu, Gd, Tb, Dy, Ho, Er) appears to crystallize. On the other hand, a highly energetic mechanical treatment of the amorphous powder previously annealed at 500° C changes considerably ...</div></div></div><ul class="InlineList u-ph0x u-fs13"><li class="InlineList-item logged_in_only"><div class="share_on_academia_work_button"><a class="academia_share Button Button--inverseBlue Button--sm js-bookmark-button" data-academia-share="Work/17802921" data-share-source="work_strip" data-spinner="small_white_hide_contents"><i class="fa fa-plus"></i><span class="work-strip-link-text u-ml1x" data-content="button_text">Bookmark</span></a></div></li><li class="InlineList-item"><div class="download"><a id="89f4a85a4c5611f341ac9eba4f3ffd05" rel="nofollow" data-download="{"attachment_id":42228264,"asset_id":17802921,"asset_type":"Work","always_allow_download":false,"track":null,"button_location":"work_strip","source":null,"hide_modal":null}" class="Button Button--sm Button--inverseGreen js-download-button prompt_button doc_download" href="https://www.academia.edu/attachments/42228264/download_file?st=MTczMjQ5ODc3MSw4LjIyMi4yMDguMTQ2&s=work_strip"><i class="fa fa-arrow-circle-o-down fa-lg"></i><span class="u-textUppercase u-ml1x" data-content="button_text">Download</span></a></div></li><li class="InlineList-item"><ul class="InlineList InlineList--bordered u-ph0x"><li class="InlineList-item InlineList-item--bordered"><span class="InlineList-item-text">by <span itemscope="itemscope" itemprop="author" itemtype="https://schema.org/Person"><a class="u-tcGrayDark u-fw700" data-has-card-for-user="37724607" href="https://uniss.academia.edu/StefanoEnzo">Stefano Enzo</a><script data-card-contents-for-user="37724607" type="text/json">{"id":37724607,"first_name":"Stefano","last_name":"Enzo","domain_name":"uniss","page_name":"StefanoEnzo","display_name":"Stefano Enzo","profile_url":"https://uniss.academia.edu/StefanoEnzo?f_ri=246949","photo":"/images/s65_no_pic.png"}</script></span></span><span class="u-displayInlineBlock InlineList-item-text"> and <span class="u-textDecorationUnderline u-clickable InlineList-item-text js-work-more-authors-17802921">+1</span><div class="hidden js-additional-users-17802921"><div><span itemscope="itemscope" itemprop="author" itemtype="https://schema.org/Person"><a href="https://uniss.academia.edu/MarcoBazzoni">Marco Bazzoni</a></span></div></div></span><script>(function(){ var popoverSettings = { el: $('.js-work-more-authors-17802921'), placement: 'bottom', hide_delay: 200, html: true, content: function(){ return $('.js-additional-users-17802921').html(); 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The oxide materials appear to be X-ray amorphous after a heat treatment at 500° C for 30h, but after 30h at 800 and 900° C a major, unreported, hexagonal phase, isostructural with TAlO3 compounds (where T= Y, Eu, Gd, Tb, Dy, Ho, Er) appears to crystallize. 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href="https://www.academia.edu/1070915/The_effect_of_particle_size_on_the_thermal_decomposition_kinetics_of_potassium_bromate">The effect of particle size on the thermal decomposition kinetics of potassium bromate</a></div></div><div class="u-pb4x u-mt3x"></div><ul class="InlineList u-ph0x u-fs13"><li class="InlineList-item logged_in_only"><div class="share_on_academia_work_button"><a class="academia_share Button Button--inverseBlue Button--sm js-bookmark-button" data-academia-share="Work/1070915" data-share-source="work_strip" data-spinner="small_white_hide_contents"><i class="fa fa-plus"></i><span class="work-strip-link-text u-ml1x" data-content="button_text">Bookmark</span></a></div></li><li class="InlineList-item"><div class="download"><a id="7c635355f96ae935354422493084a511" rel="nofollow" data-download="{"attachment_id":51115055,"asset_id":1070915,"asset_type":"Work","always_allow_download":false,"track":null,"button_location":"work_strip","source":null,"hide_modal":null}" 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})();</script></ul></li></ul></div></div><div class="u-borderBottom1 u-borderColorGrayLighter"><div class="clearfix u-pv7x u-mb0x js-work-card work_2476574" data-work_id="2476574" itemscope="itemscope" itemtype="https://schema.org/ScholarlyArticle"><div class="header"><div class="title u-fontSerif u-fs22 u-lineHeight1_3"><a class="u-tcGrayDarkest js-work-link" href="https://www.academia.edu/2476574/Influence_of_platinum_and_barium_precursors_on_the_NSR_behavior_of_Pt_Ba_Al_2O_3_monoliths_for_lean_burn_engines">Influence of platinum and barium precursors on the NSR behavior of Pt–Ba/Al 2O 3 monoliths for lean-burn engines</a></div></div><div class="u-pb4x u-mt3x"><div class="summary u-fs14 u-fw300 u-lineHeight1_5 u-tcGrayDarkest"><div class="summarized">The influence of platinum and barium precursors on the catalytic performance of monolithic Pt–Ba/Al2O3 NOx storage catalysts was studied. The precursors used in the preparation were: tetraammineplatinum nitrate [Pt(NH3)4(NO3)2] and... <a class="more_link u-tcGrayDark u-linkUnstyled" data-container=".work_2476574" data-show=".complete" data-hide=".summarized" data-more-link-behavior="true" href="#">more</a></div><div class="complete hidden">The influence of platinum and barium precursors on the catalytic performance of monolithic Pt–Ba/Al2O3 NOx storage catalysts was studied. The precursors used in the preparation were: tetraammineplatinum nitrate [Pt(NH3)4(NO3)2] and hexachloroplatinic acid [H2Pt(Cl)6] for incorporation of platinum by adsorption from solution (ion exchange); and barium acetate [Ba(CH3–COO)2] and barium nitrate [Ba(NO3)2] for incorporation of barium by dry impregnation. The prepared samples were characterized by XRD, H2 chemisorption and thermogravimetry, to determine the distribution and dispersion of the metallic phases. The catalytic activity of the prepared monolithic catalysts was tested for lean/rich NOx storage and reduction in a flow reactor using hydrogen as reducing agent. The catalyst prepared from tetraammineplatinum nitrate and barium acetate was the most active in the NOx storage during the lean period. NOx storage capacity (NSC) and selectivity were dependent with temperature. The higher NSC was obtained at temperature 330–350 °C. About 80% selectivity to nitrogen was achieved with catalysts prepared from tetraammineplatinum nitrate, versus 70% when the platinum was incorporated from hexachloroplatinic acid.</div></div></div><ul class="InlineList u-ph0x u-fs13"><li class="InlineList-item logged_in_only"><div class="share_on_academia_work_button"><a class="academia_share Button Button--inverseBlue Button--sm js-bookmark-button" data-academia-share="Work/2476574" data-share-source="work_strip" data-spinner="small_white_hide_contents"><i class="fa fa-plus"></i><span class="work-strip-link-text u-ml1x" data-content="button_text">Bookmark</span></a></div></li><li class="InlineList-item"><div class="download"><a id="74fe5f7ea4821367dca8ffb58d929835" rel="nofollow" data-download="{"attachment_id":50605928,"asset_id":2476574,"asset_type":"Work","always_allow_download":false,"track":null,"button_location":"work_strip","source":null,"hide_modal":null}" class="Button Button--sm Button--inverseGreen js-download-button prompt_button doc_download" href="https://www.academia.edu/attachments/50605928/download_file?st=MTczMjQ5ODc3MSw4LjIyMi4yMDguMTQ2&s=work_strip"><i class="fa fa-arrow-circle-o-down fa-lg"></i><span class="u-textUppercase u-ml1x" data-content="button_text">Download</span></a></div></li><li class="InlineList-item"><ul class="InlineList InlineList--bordered u-ph0x"><li class="InlineList-item InlineList-item--bordered"><span class="InlineList-item-text">by <span itemscope="itemscope" itemprop="author" itemtype="https://schema.org/Person"><a class="u-tcGrayDark u-fw700" data-has-card-for-user="2033184" href="https://ehu.academia.edu/JuanRam%C3%B3nGonz%C3%A1lezVelasco">Juan Ramón González Velasco</a><script data-card-contents-for-user="2033184" type="text/json">{"id":2033184,"first_name":"Juan Ramón","last_name":"González Velasco","domain_name":"ehu","page_name":"JuanRamónGonzálezVelasco","display_name":"Juan Ramón González Velasco","profile_url":"https://ehu.academia.edu/JuanRam%C3%B3nGonz%C3%A1lezVelasco?f_ri=246949","photo":"https://0.academia-photos.com/2033184/669616/831115/s65_juan_ram_n.gonz_lez_velasco.jpg"}</script></span></span></li><li class="js-paper-rank-work_2476574 InlineList-item InlineList-item--bordered hidden"><span class="js-paper-rank-view hidden u-tcGrayDark" data-paper-rank-work-id="2476574"><i class="u-m1x fa fa-bar-chart"></i><strong class="js-paper-rank"></strong></span><script>$(function() { new Works.PaperRankView({ workId: 2476574, container: ".js-paper-rank-work_2476574", }); 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The precursors used in the preparation were: tetraammineplatinum nitrate [Pt(NH3)4(NO3)2] and hexachloroplatinic acid [H2Pt(Cl)6] for incorporation of platinum by adsorption from solution (ion exchange); and barium acetate [Ba(CH3–COO)2] and barium nitrate [Ba(NO3)2] for incorporation of barium by dry impregnation. The prepared samples were characterized by XRD, H2 chemisorption and thermogravimetry, to determine the distribution and dispersion of the metallic phases. The catalytic activity of the prepared monolithic catalysts was tested for lean/rich NOx storage and reduction in a flow reactor using hydrogen as reducing agent. The catalyst prepared from tetraammineplatinum nitrate and barium acetate was the most active in the NOx storage during the lean period. NOx storage capacity (NSC) and selectivity were dependent with temperature. The higher NSC was obtained at temperature 330–350 °C. About 80% selectivity to nitrogen was achieved with catalysts prepared from tetraammineplatinum nitrate, versus 70% when the platinum was incorporated from hexachloroplatinic acid.","downloadable_attachments":[{"id":50605928,"asset_id":2476574,"asset_type":"Work","always_allow_download":false}],"ordered_authors":[{"id":2033184,"first_name":"Juan Ramón","last_name":"González Velasco","domain_name":"ehu","page_name":"JuanRamónGonzálezVelasco","display_name":"Juan Ramón González 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