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<!DOCTYPE html> <html > <head> <meta charset="utf-8"> <meta rel="search" type="application/opensearchdescription+xml" href="/open_search.xml" title="Academia.edu"> <meta content="width=device-width, initial-scale=1" name="viewport"> <meta name="google-site-verification" content="bKJMBZA7E43xhDOopFZkssMMkBRjvYERV-NaN4R6mrs"> <meta name="csrf-param" content="authenticity_token" /> <meta name="csrf-token" content="2B7EPsULKaXySLolSESdHFd4y/ox/4VYAQWD1WvW6487e7uX/foSUi4KvWXE+zcMuDi96wrc7iUaesU77bSV5w==" /> <meta name="citation_title" content="Isothermal cure kinetics of a diglycidyl ether of bisphenol A/1,3-bisaminomethylcyclohexane (DGEBA/1,3-BAC) epoxy resin system" /> <meta name="citation_publication_date" content="1995" /> <meta name="citation_journal_title" content="Journal of Applied Polymer Science" /> <meta name="citation_author" content="L. Barral" /> <meta name="citation_author" content="J. Cano" /> <meta name="citation_author" content="A. J. 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Ramírez" /> <meta name="citation_volume" content="56" /> <meta name="citation_issue" content="9" /> <meta name="citation_firstpage" content="1029-1037" /> <meta name="citation_issn" content="0021-8995" /> <meta name="twitter:card" content="summary" /> <meta name="twitter:url" content="https://www.academia.edu/5305306/Isothermal_cure_kinetics_of_a_diglycidyl_ether_of_bisphenol_A_1_3_bisaminomethylcyclohexane_DGEBA_1_3BAC_epoxy_resin_system" /> <meta name="twitter:title" content="Isothermal cure kinetics of a diglycidyl ether of bisphenol A/1,3-bisaminomethylcyclohexane (DGEBA/1,3BAC) epoxy resin system" /> <meta name="twitter:description" content="By employing differential scaning calorimetry, DSC, we have studied, under isothermal conditions, the kinetics of the cure reaction for a system containing a diglycidyl ether of bisphenol A (DGEBA) and 1,3-bisaminomethylcyclohexane (1,3-BAC) as a" /> <meta name="twitter:image" content="http://a.academia-assets.com/images/twitter-card.jpeg" /> <meta property="fb:app_id" content="2369844204" /> <meta property="og:type" content="article" /> <meta property="og:url" content="https://www.academia.edu/5305306/Isothermal_cure_kinetics_of_a_diglycidyl_ether_of_bisphenol_A_1_3_bisaminomethylcyclohexane_DGEBA_1_3BAC_epoxy_resin_system" /> <meta property="og:title" content="Isothermal cure kinetics of a diglycidyl ether of bisphenol A/1,3-bisaminomethylcyclohexane (DGEBA/1,3BAC) epoxy resin system" /> <meta property="og:image" content="http://a.academia-assets.com/images/open-graph-icons/fb-paper.gif" /> <meta property="og:description" content="By employing differential scaning calorimetry, DSC, we have studied, under isothermal conditions, the kinetics of the cure reaction for a system containing a diglycidyl ether of bisphenol A (DGEBA) and 1,3-bisaminomethylcyclohexane (1,3-BAC) as a" /> <meta property="article:author" content="https://independent.academia.edu/lopezjoaquin" /> <meta name="description" content="By employing differential scaning calorimetry, DSC, we have studied, under isothermal conditions, the kinetics of the cure reaction for a system containing a diglycidyl ether of bisphenol A (DGEBA) and 1,3-bisaminomethylcyclohexane (1,3-BAC) as a" /> <title>(PDF) Isothermal cure kinetics of a diglycidyl ether of bisphenol A/1,3-bisaminomethylcyclohexane (DGEBA/1,3BAC) epoxy resin system | joaquin lopez - Academia.edu</title> <link rel="canonical" href="https://www.academia.edu/5305306/Isothermal_cure_kinetics_of_a_diglycidyl_ether_of_bisphenol_A_1_3_bisaminomethylcyclohexane_DGEBA_1_3BAC_epoxy_resin_system" /> <script async src="https://www.googletagmanager.com/gtag/js?id=G-5VKX33P2DS"></script> <script> window.dataLayer = window.dataLayer || []; function gtag(){dataLayer.push(arguments);} gtag('js', new Date()); gtag('config', 'G-5VKX33P2DS', { cookie_domain: 'academia.edu', send_page_view: false, }); gtag('event', 'page_view', { 'controller': "single_work", 'action': "show", 'controller_action': 'single_work#show', 'logged_in': 'false', 'edge': 'unknown', // Send nil if there is no A/B test bucket, in case some records get logged // with missing data - that way we can distinguish between the two cases. // ab_test_bucket should be of the form <ab_test_name>:<bucket> 'ab_test_bucket': null, }) </script> <script> var $controller_name = 'single_work'; var $action_name = "show"; var $rails_env = 'production'; var $app_rev = '49879c2402910372f4abc62630a427bbe033d190'; var $domain = 'academia.edu'; var $app_host = "academia.edu"; var $asset_host = "academia-assets.com"; var $start_time = new Date().getTime(); var $recaptcha_key = "6LdxlRMTAAAAADnu_zyLhLg0YF9uACwz78shpjJB"; var $recaptcha_invisible_key = "6Lf3KHUUAAAAACggoMpmGJdQDtiyrjVlvGJ6BbAj"; var $disableClientRecordHit = false; </script> <script> window.require = { config: function() { return function() {} } } </script> <script> window.Aedu = window.Aedu || {}; window.Aedu.hit_data = null; window.Aedu.serverRenderTime = new Date(1732498967000); window.Aedu.timeDifference = new Date().getTime() - 1732498967000; </script> <script type="application/ld+json">{"@context":"https://schema.org","@type":"ScholarlyArticle","abstract":"By employing differential scaning calorimetry, DSC, we have studied, under isothermal conditions, the kinetics of the cure reaction for a system containing a diglycidyl ether of bisphenol A (DGEBA) and 1,3-bisaminomethylcyclohexane (1,3-BAC) as a curing agent, over the temperature range of 60–110°C. We have determined the conversions reached at several cure temperatures and the reaction rates. The experimental data, showing an autocatalytic behavior, were compared with the model proposed by Kamal, which includes two rate constants, k1 and k2, and two reaction orders, m and n. This model gives a good description of cure kinetics up to the onset of vitrification. The activation energies for these rate constants were 44–57 kJ/mol. The reaction orders present a moderate change but their sum is in the range 2.5–3. Diffusion control is incorporated to describe the cure in the latter stages (postivitrification region). By combining the autocatalytic model and a diffusion factor, it was possible to predict the cure kinetics over the whole range of conversion. © 1995 John Wiley \u0026amp; Sons, Inc.","author":[{"@context":"https://schema.org","@type":"Person","name":"joaquin lopez"}],"contributor":[],"dateCreated":"2013-12-03","dateModified":"2014-04-24","datePublished":"1995-01-01","headline":"Isothermal cure kinetics of a diglycidyl ether of bisphenol A/1,3-bisaminomethylcyclohexane (DGEBA/1,3BAC) epoxy resin system","inLanguage":"en","keywords":[],"locationCreated":null,"publication":"Journal of Applied Polymer Science","publisher":{"@context":"https://schema.org","@type":"Organization","name":null},"image":null,"thumbnailUrl":null,"url":"https://www.academia.edu/5305306/Isothermal_cure_kinetics_of_a_diglycidyl_ether_of_bisphenol_A_1_3_bisaminomethylcyclohexane_DGEBA_1_3BAC_epoxy_resin_system","sourceOrganization":[{"@context":"https://schema.org","@type":"EducationalOrganization","name":null}]}</script><link rel="stylesheet" media="all" href="//a.academia-assets.com/assets/single_work_page/loswp-352e32ba4e89304dc0b4fa5b3952eef2198174c54cdb79066bc62e91c68a1a91.css" /><link rel="stylesheet" media="all" href="//a.academia-assets.com/assets/design_system/body-8d679e925718b5e8e4b18e9a4fab37f7eaa99e43386459376559080ac8f2856a.css" /><link rel="stylesheet" media="all" href="//a.academia-assets.com/assets/design_system/button-3cea6e0ad4715ed965c49bfb15dedfc632787b32ff6d8c3a474182b231146ab7.css" /><link rel="stylesheet" media="all" 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[{"id":49355821,"identifier":"Attachment_49355821","shouldShowBulkDownload":false}]; window.loswp.shouldDetectTimezone = true; window.loswp.shouldShowBulkDownload = true; window.loswp.showSignupCaptcha = false window.loswp.willEdgeCache = false; window.loswp.work = {"work":{"id":5305306,"created_at":"2013-12-03T07:07:22.131-08:00","from_world_paper_id":121197959,"updated_at":"2021-01-17T13:15:29.929-08:00","_data":{"abstract":"By employing differential scaning calorimetry, DSC, we have studied, under isothermal conditions, the kinetics of the cure reaction for a system containing a diglycidyl ether of bisphenol A (DGEBA) and 1,3-bisaminomethylcyclohexane (1,3-BAC) as a curing agent, over the temperature range of 60–110°C. We have determined the conversions reached at several cure temperatures and the reaction rates. The experimental data, showing an autocatalytic behavior, were compared with the model proposed by Kamal, which includes two rate constants, k1 and k2, and two reaction orders, m and n. This model gives a good description of cure kinetics up to the onset of vitrification. The activation energies for these rate constants were 44–57 kJ/mol. The reaction orders present a moderate change but their sum is in the range 2.5–3. Diffusion control is incorporated to describe the cure in the latter stages (postivitrification region). By combining the autocatalytic model and a diffusion factor, it was possible to predict the cure kinetics over the whole range of conversion. © 1995 John Wiley \u0026 Sons, Inc.","publication_date":"1995,,","publication_name":"Journal of Applied Polymer Science"},"document_type":"paper","pre_hit_view_count_baseline":null,"quality":"high","language":"en","title":"Isothermal cure kinetics of a diglycidyl ether of bisphenol A/1,3-bisaminomethylcyclohexane (DGEBA/1,3BAC) epoxy resin system","broadcastable":true,"draft":null,"has_indexable_attachment":true,"indexable":true}}["work"]; window.loswp.workCoauthors = [7312082]; window.loswp.locale = "en"; window.loswp.countryCode = "SG"; window.loswp.cwvAbTestBucket = ""; window.loswp.designVariant = "ds_vanilla"; window.loswp.fullPageMobileSutdModalVariant = "full_page_mobile_sutd_modal"; window.loswp.useOptimizedScribd4genScript = false; window.loswp.appleClientId = 'edu.academia.applesignon';</script><script defer="" src="https://accounts.google.com/gsi/client"></script><div class="ds-loswp-container"><div class="ds-work-card--grid-container"><div class="ds-work-card--container js-loswp-work-card"><div class="ds-work-card--cover"><div class="ds-work-cover--wrapper"><div class="ds-work-cover--container"><button class="ds-work-cover--clickable js-swp-download-button" data-signup-modal="{"location":"swp-splash-paper-cover","attachmentId":49355821,"attachmentType":"pdf"}"><img alt="First page of “Isothermal cure kinetics of a diglycidyl ether of bisphenol A/1,3-bisaminomethylcyclohexane (DGEBA/1,3BAC) epoxy resin system”" class="ds-work-cover--cover-thumbnail" src="https://0.academia-photos.com/attachment_thumbnails/49355821/mini_magick20190131-14271-hjzny2.png?1548992097" /><img alt="PDF Icon" class="ds-work-cover--file-icon" src="//a.academia-assets.com/assets/single_work_splash/adobe.icon-574afd46eb6b03a77a153a647fb47e30546f9215c0ee6a25df597a779717f9ef.svg" /><div class="ds-work-cover--hover-container"><span class="material-symbols-outlined" style="font-size: 20px" translate="no">download</span><p>Download Free PDF</p></div><div class="ds-work-cover--ribbon-container">Download Free PDF</div><div class="ds-work-cover--ribbon-triangle"></div></button></div></div></div><div class="ds-work-card--work-information"><h1 class="ds-work-card--work-title">Isothermal cure kinetics of a diglycidyl ether of bisphenol A/1,3-bisaminomethylcyclohexane (DGEBA/1,3BAC) epoxy resin system</h1><div class="ds-work-card--work-authors ds-work-card--detail"><a class="ds-work-card--author js-wsj-grid-card-author ds2-5-body-md ds2-5-body-link" data-author-id="7312082" href="https://independent.academia.edu/lopezjoaquin"><img alt="Profile image of joaquin lopez" class="ds-work-card--author-avatar" src="//a.academia-assets.com/images/s65_no_pic.png" />joaquin lopez</a></div><p class="ds-work-card--detail ds2-5-body-sm">1995, Journal of Applied Polymer Science</p><p class="ds-work-card--work-abstract ds-work-card--detail ds2-5-body-md">By employing differential scaning calorimetry, DSC, we have studied, under isothermal conditions, the kinetics of the cure reaction for a system containing a diglycidyl ether of bisphenol A (DGEBA) and 1,3-bisaminomethylcyclohexane (1,3-BAC) as a curing agent, over the temperature range of 60–110°C. We have determined the conversions reached at several cure temperatures and the reaction rates. The experimental data, showing an autocatalytic behavior, were compared with the model proposed by Kamal, which includes two rate constants, k1 and k2, and two reaction orders, m and n. This model gives a good description of cure kinetics up to the onset of vitrification. The activation energies for these rate constants were 44–57 kJ/mol. The reaction orders present a moderate change but their sum is in the range 2.5–3. Diffusion control is incorporated to describe the cure in the latter stages (postivitrification region). By combining the autocatalytic model and a diffusion factor, it was possible to predict the cure kinetics over the whole range of conversion. © 1995 John Wiley & Sons, Inc.</p><div class="ds-work-card--button-container"><button class="ds2-5-button js-swp-download-button" data-signup-modal="{"location":"continue-reading-button--work-card","attachmentId":49355821,"attachmentType":"pdf","workUrl":"https://www.academia.edu/5305306/Isothermal_cure_kinetics_of_a_diglycidyl_ether_of_bisphenol_A_1_3_bisaminomethylcyclohexane_DGEBA_1_3BAC_epoxy_resin_system"}">See full PDF</button><button class="ds2-5-button ds2-5-button--secondary js-swp-download-button" data-signup-modal="{"location":"download-pdf-button--work-card","attachmentId":49355821,"attachmentType":"pdf","workUrl":"https://www.academia.edu/5305306/Isothermal_cure_kinetics_of_a_diglycidyl_ether_of_bisphenol_A_1_3_bisaminomethylcyclohexane_DGEBA_1_3BAC_epoxy_resin_system"}"><span class="material-symbols-outlined" style="font-size: 20px" 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href="https://www.academia.edu/33928531/Kinetics_of_curing_reaction_of_a_diglycidyl_ether_of_bisphenol_A_1_3_bisaminomethyl_cyclohexane_DGEBA_1_3_BAC_epoxy_resin_system">Kinetics of curing reaction of a diglycidyl ether of bisphenol A/1,3-bisaminomethyl-cyclohexane (DGEBA/1,3-BAC) epoxy resin system</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="39990380" href="https://independent.academia.edu/CamiloRamirez41">Camilo Ramirez</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Thermal Analysis, 1996</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Kinetics of curing reaction of a diglycidyl ether of bisphenol A/1,3-bisaminomethyl-cyclohexane (DGEBA/1,3-BAC) epoxy resin 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data-author-id="33291173" href="https://utfsm.academia.edu/CarlosCastro">Carlos Castro</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Applied Polymer Science, 2001</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Cure kinetics of diglycidylether of bisphenol A- ethylenediamine revisited using a mechanistic model","attachmentId":49217141,"attachmentType":"pdf","work_url":"https://www.academia.edu/28800060/Cure_kinetics_of_diglycidylether_of_bisphenol_A_ethylenediamine_revisited_using_a_mechanistic_model","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/28800060/Cure_kinetics_of_diglycidylether_of_bisphenol_A_ethylenediamine_revisited_using_a_mechanistic_model"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="4" data-entity-id="78182261" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/78182261/Kinetic_Analysis_of_the_Curing_of_a_Partially_Biobased_Epoxy_Resin_Using_Dynamic_Differential_Scanning_Calorimetry">Kinetic Analysis of the Curing of a Partially Biobased Epoxy Resin Using Dynamic Differential Scanning Calorimetry</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="57189910" href="https://independent.academia.edu/DiegoLascano1">Diego Lascano</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Polymers, 2019</p><p class="ds-related-work--abstract ds2-5-body-sm">This research presents a cure kinetics study of an epoxy system consisting of a partially bio-sourced resin based on diglycidyl ether of bisphenol A (DGEBA) with amine hardener and a biobased reactive diluent from plants representing 31 wt %. The kinetic study has been carried out using differential scanning calorimetry (DSC) under non-isothermal conditions at different heating rates. Integral and derivative isoconversional methods or model free kinetics (MFK) have been applied to the experimental data in order to evaluate the apparent activation energy, Ea, followed by the application of the appropriate reaction model. The bio-sourced system showed activation energy that is independent of the extent of conversion, with Ea values between 57 and 62 kJ·mol−1, corresponding to typical activation energies of conventional epoxy resins. The reaction model was studied by comparing the calculated y(α) and z(α) functions with standard master plot curves. A two-parameter autocatalytic kinetic...</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Kinetic Analysis of the Curing of a Partially Biobased Epoxy Resin Using Dynamic Differential Scanning Calorimetry","attachmentId":85319008,"attachmentType":"pdf","work_url":"https://www.academia.edu/78182261/Kinetic_Analysis_of_the_Curing_of_a_Partially_Biobased_Epoxy_Resin_Using_Dynamic_Differential_Scanning_Calorimetry","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/78182261/Kinetic_Analysis_of_the_Curing_of_a_Partially_Biobased_Epoxy_Resin_Using_Dynamic_Differential_Scanning_Calorimetry"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="5" data-entity-id="47305022" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/47305022/Cure_kinetics_of_amine_cured_diglycidyl_ether_of_bisphenol">Cure kinetics of amine-cured diglycidyl ether of bisphenol</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="138024496" href="https://independent.academia.edu/JoaquinLopez124">Joaquin Lopez</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Thermochimica Acta, 2000</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Cure kinetics of amine-cured diglycidyl ether of bisphenol","attachmentId":66467780,"attachmentType":"pdf","work_url":"https://www.academia.edu/47305022/Cure_kinetics_of_amine_cured_diglycidyl_ether_of_bisphenol","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/47305022/Cure_kinetics_of_amine_cured_diglycidyl_ether_of_bisphenol"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="6" data-entity-id="7095341" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/7095341/Curing_kinetics_and_thermal_stability_of_diglycidyl_ether_of_bisphenol">Curing kinetics and thermal stability of diglycidyl ether of bisphenol</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="12189830" href="https://independent.academia.edu/PoojaSharma71">Pooja Sharma</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Thermal Analysis and Calorimetry, 2008</p><p class="ds-related-work--abstract ds2-5-body-sm">Curing kinetics of diglycidyl ether of bisphenol-A (DGEBA) in the presence of varying molar ratios of aromatic imide-amines and 4,4′-diaminodiphenylsulfone (DDS) were investigated by the dynamic differential scanning calorimetry. The imide-amines were prepared by reacting 1 mole of benzophenone 3,3′,4,4′-tetracarboxylic acid dianhydride (B) with 2.5 moles of 4,4′-diaminodiphenyl ether (E)/ or 4,4′-diaminodiphenyl methane (M)/ or 4,4′-diaminodiphenylsulfone (S) and designated as BE/ or BM/ or BS. The mixture of imide-amines and DDS at ratio of 0:1, 0.25:0.75, 0.5:0.5, 0.75:0.25 and 1:0 were used to investigate the curing behaviour of DGEBA. The multiple heating rate method (5, 10, 15 and 20°C min−1) was used to study the curing kinetics of epoxy resins. The peak exotherm temperature was found to be dependent on the heating rate, structure of imide-amines as well as on the ratio of imide-amine: DDS used. A broad exotherm was observed in the temperature range of 180–230°C on curing with mixture of imide-amines and DDS. Curing of DGEBA with mixture of imide-amines and/or DDS resulted in a decrease in characteristic curing temperatures. Activation energy of curing reaction as determined in accordance to the Ozawa’s method was found to be dependent on the structure of amine. The thermal stability of the isothermally cured resins was also evaluated using dynamic thermogravimetry in a nitrogen atmosphere. The char yield was highest in case of resins cured using mixture of DDS: BS (0.25:0.75; EBS-3), DDS: BM (0.5: 0.5; EBM-2) and DDS: BE (0.5: 0.5; EBE-2).</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Curing kinetics and thermal stability of diglycidyl ether of bisphenol","attachmentId":48601912,"attachmentType":"pdf","work_url":"https://www.academia.edu/7095341/Curing_kinetics_and_thermal_stability_of_diglycidyl_ether_of_bisphenol","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/7095341/Curing_kinetics_and_thermal_stability_of_diglycidyl_ether_of_bisphenol"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="7" data-entity-id="4084167" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/4084167/Cure_kinetics_of_ternary_blends_of_epoxy_resins_studied_by_nonisothermal_DSC_data">Cure kinetics of ternary blends of epoxy resins studied by nonisothermal DSC data</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="4924324" href="https://independent.academia.edu/GarimaTripathi">Garima Tripathi</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Applied Polymer Science, 2009</p><p class="ds-related-work--abstract ds2-5-body-sm">The curing kinetics of blends of diglycidyl ether of bisphenol A (DGEBA), cycloaliphatic epoxy resins, and carboxyl-terminated butadiene-acrylonitrile random copolymer (CTBN) in presence of 4,4′-diamino diphenyl sulfone (DDS) as the curing agent was studied by nonisothermal differential scanning calorimetry (DSC) technique at different heating rates. The kinetic parameters of the curing process were determined by isoconversional method given by Malek for the kinetic analysis of the data obtained by the thermal treatment. A two-parameter (m, n) autocatalytic model (Sestak-Berggren equation) was found to be the most adequate selected to describe the cure kinetics of the studied epoxy resins. The values of Ea were found to be 88.6 kJ mol−1 and 61.6 kJ mol−1, respectively, for the studied two sample series. Nonisothermal DSC curves obtained using the experimental data show a good agreement with that theoretically calculated. © 2009 Wiley Periodicals, Inc. J Appl Polym Sci, 2009</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Cure kinetics of ternary blends of epoxy resins studied by nonisothermal DSC data","attachmentId":50042789,"attachmentType":"pdf","work_url":"https://www.academia.edu/4084167/Cure_kinetics_of_ternary_blends_of_epoxy_resins_studied_by_nonisothermal_DSC_data","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/4084167/Cure_kinetics_of_ternary_blends_of_epoxy_resins_studied_by_nonisothermal_DSC_data"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="8" data-entity-id="27419197" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/27419197/Cure_kinetics_of_a_liquid_crystalline_epoxy_resin_studied_by_non_isothermal_data">Cure kinetics of a liquid-crystalline epoxy resin studied by non-isothermal data</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="51458251" href="https://independent.academia.edu/DanRosu3">Dan Rosu</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Polymer Testing, 2004</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Cure kinetics of a liquid-crystalline epoxy resin studied by non-isothermal data","attachmentId":47675861,"attachmentType":"pdf","work_url":"https://www.academia.edu/27419197/Cure_kinetics_of_a_liquid_crystalline_epoxy_resin_studied_by_non_isothermal_data","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/27419197/Cure_kinetics_of_a_liquid_crystalline_epoxy_resin_studied_by_non_isothermal_data"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="9" data-entity-id="27419200" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/27419200/Investigation_of_the_curing_reactions_of_some_multifunctional_epoxy_resins_using_differential_scanning_calorimetry">Investigation of the curing reactions of some multifunctional epoxy resins using differential scanning calorimetry</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="51458251" href="https://independent.academia.edu/DanRosu3">Dan Rosu</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Thermochimica Acta, 2001</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Investigation of the curing reactions of some multifunctional epoxy resins using differential scanning 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You can download the paper by clicking the button above.</p></div></div></div></div><div class="ds-sidebar--container js-work-sidebar"><div class="ds-related-content--container"><h2 class="ds-related-content--heading">Related papers</h2><div class="ds-related-work--container js-related-work-sidebar-card" data-collection-position="0" data-entity-id="117179527" data-sort-order="default"><a class="ds-related-work--title js-related-work-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/117179527/Effects_of_diffusion_on_the_kinetic_study_and_TTT_cure_diagram_for_an_epoxy_diamine_system">Effects of diffusion on the kinetic study and TTT cure diagram for an epoxy/diamine system</a><div class="ds-related-work--metadata"><a class="js-related-work-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="45089310" href="https://independent.academia.edu/FragaFrancisco">Francisco Fraga López</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Applied Polymer Science, 1998</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Effects of diffusion on the kinetic study and TTT cure diagram for an epoxy/diamine system","attachmentId":113104819,"attachmentType":"pdf","work_url":"https://www.academia.edu/117179527/Effects_of_diffusion_on_the_kinetic_study_and_TTT_cure_diagram_for_an_epoxy_diamine_system","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-related-work-grid-card-view-pdf" href="https://www.academia.edu/117179527/Effects_of_diffusion_on_the_kinetic_study_and_TTT_cure_diagram_for_an_epoxy_diamine_system"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-related-work-sidebar-card" data-collection-position="1" data-entity-id="67879082" data-sort-order="default"><a class="ds-related-work--title js-related-work-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/67879082/Curing_reaction_of_epoxy_resins_with_diamines">Curing reaction of epoxy resins with diamines</a><div class="ds-related-work--metadata"><a class="js-related-work-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="19689022" href="https://independent.academia.edu/CarmenRiccardi">Carmen Riccardi</a></div><p class="ds-related-work--metadata ds2-5-body-xs">1984</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Curing reaction of epoxy resins with diamines","attachmentId":78561091,"attachmentType":"pdf","work_url":"https://www.academia.edu/67879082/Curing_reaction_of_epoxy_resins_with_diamines","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-related-work-grid-card-view-pdf" href="https://www.academia.edu/67879082/Curing_reaction_of_epoxy_resins_with_diamines"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-related-work-sidebar-card" data-collection-position="2" data-entity-id="11383116" data-sort-order="default"><a class="ds-related-work--title js-related-work-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/11383116/Influence_of_the_filler_CaCO_3_on_the_cure_kinetic_of_the_epoxy_network_diglycidyl_ether_of_bisphenol_a_BADGE_n_0_with_isophorone_diamine">Influence of the filler CaCO 3 on the cure kinetic of the epoxy network diglycidyl ether of bisphenol a (BADGE n = 0) with isophorone diamine</a><div class="ds-related-work--metadata"><a class="js-related-work-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="27676762" href="https://itgustavoamadero.academia.edu/IvanVazquez">Ivan Vazquez</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Applied Polymer Science, 2009</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Influence of the filler CaCO 3 on the cure kinetic of the epoxy network diglycidyl ether of bisphenol a (BADGE n = 0) with isophorone diamine","attachmentId":46740090,"attachmentType":"pdf","work_url":"https://www.academia.edu/11383116/Influence_of_the_filler_CaCO_3_on_the_cure_kinetic_of_the_epoxy_network_diglycidyl_ether_of_bisphenol_a_BADGE_n_0_with_isophorone_diamine","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-related-work-grid-card-view-pdf" href="https://www.academia.edu/11383116/Influence_of_the_filler_CaCO_3_on_the_cure_kinetic_of_the_epoxy_network_diglycidyl_ether_of_bisphenol_a_BADGE_n_0_with_isophorone_diamine"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-related-work-sidebar-card" data-collection-position="3" data-entity-id="14955533" data-sort-order="default"><a class="ds-related-work--title js-related-work-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/14955533/Mechanism_and_Kinetics_of_Epoxy_Amine_Cure_Studied_by_Differential_Scanning_Calorimetry">Mechanism and Kinetics of Epoxy−Amine Cure Studied by Differential Scanning Calorimetry</a><div class="ds-related-work--metadata"><a class="js-related-work-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="33950313" href="https://landaverde.academia.edu/NicolasSbirrazzuoli">Nicolas Sbirrazzuoli</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Macromolecules, 1996</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Mechanism and Kinetics of Epoxy−Amine Cure Studied by Differential Scanning 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data-entity-id="51181076" data-sort-order="default"><a class="ds-related-work--title js-related-work-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/51181076/Cure_mechanisms_of_diglycidyl_ether_of_bisphenol_A_DGEBA_epoxy_with_diethanolamine">Cure mechanisms of diglycidyl ether of bisphenol A (DGEBA) epoxy with diethanolamine</a><div class="ds-related-work--metadata"><a class="js-related-work-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="14858979" href="https://independent.academia.edu/NFredj">Narjes Fredj</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Polymer, 2016</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Cure mechanisms of diglycidyl ether of bisphenol A (DGEBA) epoxy with 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href="https://www.academia.edu/54982701/Epoxy_resins_based_on_trimethylolpropane_II_Kinetic_and_thermodynamic_parameters_of_cure_withm_XDA">Epoxy resins based on trimethylolpropane. II. Kinetic and thermodynamic parameters of cure withm-XDA</a><div class="ds-related-work--metadata"><a class="js-related-work-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="32953802" href="https://independent.academia.edu/MArturoL%C3%B3pezQuintela">M. Arturo López Quintela</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Applied Polymer Science, 1995</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Epoxy resins based on trimethylolpropane. II. 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