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(PDF) Kinetic Analysis of the Curing of a Partially Biobased Epoxy Resin Using Dynamic Differential Scanning Calorimetry | Diego Lascano - Academia.edu
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The" /> <title>(PDF) Kinetic Analysis of the Curing of a Partially Biobased Epoxy Resin Using Dynamic Differential Scanning Calorimetry | Diego Lascano - Academia.edu</title> <link rel="canonical" href="https://www.academia.edu/78182261/Kinetic_Analysis_of_the_Curing_of_a_Partially_Biobased_Epoxy_Resin_Using_Dynamic_Differential_Scanning_Calorimetry" /> <script async src="https://www.googletagmanager.com/gtag/js?id=G-5VKX33P2DS"></script> <script> window.dataLayer = window.dataLayer || []; function gtag(){dataLayer.push(arguments);} gtag('js', new Date()); gtag('config', 'G-5VKX33P2DS', { cookie_domain: 'academia.edu', send_page_view: false, }); gtag('event', 'page_view', { 'controller': "single_work", 'action': "show", 'controller_action': 'single_work#show', 'logged_in': 'false', 'edge': 'unknown', // Send nil if there is no A/B test bucket, in case some records get logged // with missing data - that way we can distinguish between the two cases. // ab_test_bucket should be of the form <ab_test_name>:<bucket> 'ab_test_bucket': null, }) </script> <script> var $controller_name = 'single_work'; var $action_name = "show"; var $rails_env = 'production'; var $app_rev = '49879c2402910372f4abc62630a427bbe033d190'; var $domain = 'academia.edu'; var $app_host = "academia.edu"; var $asset_host = "academia-assets.com"; var $start_time = new Date().getTime(); var $recaptcha_key = "6LdxlRMTAAAAADnu_zyLhLg0YF9uACwz78shpjJB"; var $recaptcha_invisible_key = "6Lf3KHUUAAAAACggoMpmGJdQDtiyrjVlvGJ6BbAj"; var $disableClientRecordHit = false; </script> <script> window.require = { config: function() { return function() {} } } </script> <script> window.Aedu = window.Aedu || {}; window.Aedu.hit_data = null; window.Aedu.serverRenderTime = new Date(1732505170000); window.Aedu.timeDifference = new Date().getTime() - 1732505170000; </script> <script type="application/ld+json">{"@context":"https://schema.org","@type":"ScholarlyArticle","abstract":"This research presents a cure kinetics study of an epoxy system consisting of a partially bio-sourced resin based on diglycidyl ether of bisphenol A (DGEBA) with amine hardener and a biobased reactive diluent from plants representing 31 wt %. The kinetic study has been carried out using differential scanning calorimetry (DSC) under non-isothermal conditions at different heating rates. Integral and derivative isoconversional methods or model free kinetics (MFK) have been applied to the experimental data in order to evaluate the apparent activation energy, Ea, followed by the application of the appropriate reaction model. The bio-sourced system showed activation energy that is independent of the extent of conversion, with Ea values between 57 and 62 kJ·mol−1, corresponding to typical activation energies of conventional epoxy resins. The reaction model was studied by comparing the calculated y(α) and z(α) functions with standard master plot curves. A two-parameter autocatalytic kinetic...","author":[{"@context":"https://schema.org","@type":"Person","name":"Diego Lascano"}],"contributor":[],"dateCreated":"2022-05-01","dateModified":null,"datePublished":"2019-01-01","headline":"Kinetic Analysis of the Curing of a Partially Biobased Epoxy Resin Using Dynamic Differential Scanning Calorimetry","inLanguage":"en","keywords":["Materials Science","Polymers","Medicine"],"locationCreated":null,"publication":"Polymers","publisher":{"@context":"https://schema.org","@type":"Organization","name":"MDPI AG"},"image":null,"thumbnailUrl":null,"url":"https://www.academia.edu/78182261/Kinetic_Analysis_of_the_Curing_of_a_Partially_Biobased_Epoxy_Resin_Using_Dynamic_Differential_Scanning_Calorimetry","sourceOrganization":[{"@context":"https://schema.org","@type":"EducationalOrganization","name":null}]}</script><link rel="stylesheet" media="all" 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"https://www.academia.edu/login?post_login_redirect_url=https%3A%2F%2Fwww.academia.edu%2F78182261%2FKinetic_Analysis_of_the_Curing_of_a_Partially_Biobased_Epoxy_Resin_Using_Dynamic_Differential_Scanning_Calorimetry%3Fauto%3Ddownload"; window.loswp.translateUrl = "https://www.academia.edu/login?post_login_redirect_url=https%3A%2F%2Fwww.academia.edu%2F78182261%2FKinetic_Analysis_of_the_Curing_of_a_Partially_Biobased_Epoxy_Resin_Using_Dynamic_Differential_Scanning_Calorimetry%3Fshow_translation%3Dtrue"; window.loswp.previewableAttachments = [{"id":85319008,"identifier":"Attachment_85319008","shouldShowBulkDownload":false}]; window.loswp.shouldDetectTimezone = true; window.loswp.shouldShowBulkDownload = true; window.loswp.showSignupCaptcha = false window.loswp.willEdgeCache = false; window.loswp.work = {"work":{"id":78182261,"created_at":"2022-05-01T23:28:30.348-07:00","from_world_paper_id":203977182,"updated_at":"2024-03-19T09:32:01.713-07:00","_data":{"abstract":"This research presents a cure kinetics study of an epoxy system consisting of a partially bio-sourced resin based on diglycidyl ether of bisphenol A (DGEBA) with amine hardener and a biobased reactive diluent from plants representing 31 wt %. The kinetic study has been carried out using differential scanning calorimetry (DSC) under non-isothermal conditions at different heating rates. Integral and derivative isoconversional methods or model free kinetics (MFK) have been applied to the experimental data in order to evaluate the apparent activation energy, Ea, followed by the application of the appropriate reaction model. The bio-sourced system showed activation energy that is independent of the extent of conversion, with Ea values between 57 and 62 kJ·mol−1, corresponding to typical activation energies of conventional epoxy resins. The reaction model was studied by comparing the calculated y(α) and z(α) functions with standard master plot curves. A two-parameter autocatalytic kinetic...","publisher":"MDPI AG","publication_date":"2019,,","publication_name":"Polymers"},"document_type":"paper","pre_hit_view_count_baseline":null,"quality":"high","language":"en","title":"Kinetic Analysis of the Curing of a Partially Biobased Epoxy Resin Using Dynamic Differential Scanning Calorimetry","broadcastable":true,"draft":null,"has_indexable_attachment":true,"indexable":true}}["work"]; window.loswp.workCoauthors = [57189910]; window.loswp.locale = "en"; window.loswp.countryCode = "SG"; window.loswp.cwvAbTestBucket = ""; window.loswp.designVariant = "ds_vanilla"; window.loswp.fullPageMobileSutdModalVariant = "full_page_mobile_sutd_modal"; window.loswp.useOptimizedScribd4genScript = false; window.loswp.appleClientId = 'edu.academia.applesignon';</script><script defer="" src="https://accounts.google.com/gsi/client"></script><div class="ds-loswp-container"><div class="ds-work-card--grid-container"><div class="ds-work-card--container js-loswp-work-card"><div class="ds-work-card--cover"><div class="ds-work-cover--wrapper"><div class="ds-work-cover--container"><button class="ds-work-cover--clickable js-swp-download-button" data-signup-modal="{"location":"swp-splash-paper-cover","attachmentId":85319008,"attachmentType":"pdf"}"><img alt="First page of “Kinetic Analysis of the Curing of a Partially Biobased Epoxy Resin Using Dynamic Differential Scanning Calorimetry”" class="ds-work-cover--cover-thumbnail" src="https://0.academia-photos.com/attachment_thumbnails/85319008/mini_magick20220501-12123-i9h31j.png?1651473003" /><img alt="PDF Icon" class="ds-work-cover--file-icon" src="//a.academia-assets.com/assets/single_work_splash/adobe.icon-574afd46eb6b03a77a153a647fb47e30546f9215c0ee6a25df597a779717f9ef.svg" /><div class="ds-work-cover--hover-container"><span class="material-symbols-outlined" style="font-size: 20px" translate="no">download</span><p>Download Free PDF</p></div><div class="ds-work-cover--ribbon-container">Download Free PDF</div><div class="ds-work-cover--ribbon-triangle"></div></button></div></div></div><div class="ds-work-card--work-information"><h1 class="ds-work-card--work-title">Kinetic Analysis of the Curing of a Partially Biobased Epoxy Resin Using Dynamic Differential Scanning Calorimetry</h1><div class="ds-work-card--work-authors ds-work-card--detail"><a class="ds-work-card--author js-wsj-grid-card-author ds2-5-body-md ds2-5-body-link" data-author-id="57189910" href="https://independent.academia.edu/DiegoLascano1"><img alt="Profile image of Diego Lascano" class="ds-work-card--author-avatar" src="https://0.academia-photos.com/57189910/18843765/18802194/s65_diego.lascano.jpg" />Diego Lascano</a></div><p class="ds-work-card--detail ds2-5-body-sm">2019, Polymers</p><p class="ds-work-card--work-abstract ds-work-card--detail ds2-5-body-md">This research presents a cure kinetics study of an epoxy system consisting of a partially bio-sourced resin based on diglycidyl ether of bisphenol A (DGEBA) with amine hardener and a biobased reactive diluent from plants representing 31 wt %. The kinetic study has been carried out using differential scanning calorimetry (DSC) under non-isothermal conditions at different heating rates. Integral and derivative isoconversional methods or model free kinetics (MFK) have been applied to the experimental data in order to evaluate the apparent activation energy, Ea, followed by the application of the appropriate reaction model. The bio-sourced system showed activation energy that is independent of the extent of conversion, with Ea values between 57 and 62 kJ·mol−1, corresponding to typical activation energies of conventional epoxy resins. The reaction model was studied by comparing the calculated y(α) and z(α) functions with standard master plot curves. A two-parameter autocatalytic kinetic...</p><div class="ds-work-card--button-container"><button class="ds2-5-button js-swp-download-button" data-signup-modal="{"location":"continue-reading-button--work-card","attachmentId":85319008,"attachmentType":"pdf","workUrl":"https://www.academia.edu/78182261/Kinetic_Analysis_of_the_Curing_of_a_Partially_Biobased_Epoxy_Resin_Using_Dynamic_Differential_Scanning_Calorimetry"}">See full PDF</button><button class="ds2-5-button ds2-5-button--secondary js-swp-download-button" data-signup-modal="{"location":"download-pdf-button--work-card","attachmentId":85319008,"attachmentType":"pdf","workUrl":"https://www.academia.edu/78182261/Kinetic_Analysis_of_the_Curing_of_a_Partially_Biobased_Epoxy_Resin_Using_Dynamic_Differential_Scanning_Calorimetry"}"><span class="material-symbols-outlined" style="font-size: 20px" translate="no">download</span>Download PDF</button></div></div></div></div><div data-auto_select="false" data-client_id="331998490334-rsn3chp12mbkiqhl6e7lu2q0mlbu0f1b" data-doc_id="85319008" data-landing_url="https://www.academia.edu/78182261/Kinetic_Analysis_of_the_Curing_of_a_Partially_Biobased_Epoxy_Resin_Using_Dynamic_Differential_Scanning_Calorimetry" data-login_uri="https://www.academia.edu/registrations/google_one_tap" data-moment_callback="onGoogleOneTapEvent" id="g_id_onload"></div><div class="ds-top-related-works--grid-container"><div class="ds-related-content--container ds-top-related-works--container"><h2 class="ds-related-content--heading">Related papers</h2><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="0" data-entity-id="78182275" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/78182275/Kinetic_Analysis_of_the_Curing_Process_of_Biobased_Epoxy_Resin_from_Epoxidized_Linseed_Oil_by_Dynamic_Differential_Scanning_Calorimetry">Kinetic Analysis of the Curing Process of Biobased Epoxy Resin from Epoxidized Linseed Oil by Dynamic Differential Scanning Calorimetry</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="57189910" href="https://independent.academia.edu/DiegoLascano1">Diego Lascano</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Polymers, 2021</p><p class="ds-related-work--abstract ds2-5-body-sm">The curing process of epoxy resin based on epoxidized linseed oil (ELO) is studied using dynamic differential scanning calorimetry (DSC) in order to determine the kinetic triplet (Ea, f(α) and A) at different heating rates. The apparent activation energy, Ea, has been calculated by several differential and integral isoconversional methods, namely Kissinger, Friedman, Flynn–Wall–Ozawa (FWO), Kissinger–Akahira–Sunose (KAS) and Starink. All methods provide similar values of Ea (between 66 and 69 kJ/mol), and this shows independence versus the heating rate used. The epoxy resins crosslinking is characterized by a multi-step process. However, for the sake of the simplicity and to facilitate the understanding of the influence of the oxirane location on the curing kinetic, this can be assimilated to a single-step process. The reaction model has a high proportion of autocatalytic process, fulfilling that αM is between 0 and αp and αM &lt; αp∞. Using as reference the model proposed by Šesták...</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Kinetic Analysis of the Curing Process of Biobased Epoxy Resin from Epoxidized Linseed Oil by Dynamic Differential Scanning Calorimetry","attachmentId":85319022,"attachmentType":"pdf","work_url":"https://www.academia.edu/78182275/Kinetic_Analysis_of_the_Curing_Process_of_Biobased_Epoxy_Resin_from_Epoxidized_Linseed_Oil_by_Dynamic_Differential_Scanning_Calorimetry","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/78182275/Kinetic_Analysis_of_the_Curing_Process_of_Biobased_Epoxy_Resin_from_Epoxidized_Linseed_Oil_by_Dynamic_Differential_Scanning_Calorimetry"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="1" data-entity-id="27419199" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/27419199/Cure_kinetics_of_epoxy_resins_studied_by_non_isothermal_DSC_data">Cure kinetics of epoxy resins studied by non-isothermal DSC data</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="51458251" href="https://independent.academia.edu/DanRosu3">Dan Rosu</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Thermochimica Acta, 2002</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Cure kinetics of epoxy resins studied by non-isothermal DSC data","attachmentId":47675852,"attachmentType":"pdf","work_url":"https://www.academia.edu/27419199/Cure_kinetics_of_epoxy_resins_studied_by_non_isothermal_DSC_data","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/27419199/Cure_kinetics_of_epoxy_resins_studied_by_non_isothermal_DSC_data"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="2" data-entity-id="27419200" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/27419200/Investigation_of_the_curing_reactions_of_some_multifunctional_epoxy_resins_using_differential_scanning_calorimetry">Investigation of the curing reactions of some multifunctional epoxy resins using differential scanning calorimetry</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="51458251" href="https://independent.academia.edu/DanRosu3">Dan Rosu</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Thermochimica Acta, 2001</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Investigation of the curing reactions of some multifunctional epoxy resins using differential scanning calorimetry","attachmentId":47675853,"attachmentType":"pdf","work_url":"https://www.academia.edu/27419200/Investigation_of_the_curing_reactions_of_some_multifunctional_epoxy_resins_using_differential_scanning_calorimetry","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/27419200/Investigation_of_the_curing_reactions_of_some_multifunctional_epoxy_resins_using_differential_scanning_calorimetry"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="3" data-entity-id="33928531" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/33928531/Kinetics_of_curing_reaction_of_a_diglycidyl_ether_of_bisphenol_A_1_3_bisaminomethyl_cyclohexane_DGEBA_1_3_BAC_epoxy_resin_system">Kinetics of curing reaction of a diglycidyl ether of bisphenol A/1,3-bisaminomethyl-cyclohexane (DGEBA/1,3-BAC) epoxy resin system</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="39990380" href="https://independent.academia.edu/CamiloRamirez41">Camilo Ramirez</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Thermal Analysis, 1996</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Kinetics of curing reaction of a diglycidyl ether of bisphenol A/1,3-bisaminomethyl-cyclohexane (DGEBA/1,3-BAC) epoxy resin system","attachmentId":53896773,"attachmentType":"pdf","work_url":"https://www.academia.edu/33928531/Kinetics_of_curing_reaction_of_a_diglycidyl_ether_of_bisphenol_A_1_3_bisaminomethyl_cyclohexane_DGEBA_1_3_BAC_epoxy_resin_system","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/33928531/Kinetics_of_curing_reaction_of_a_diglycidyl_ether_of_bisphenol_A_1_3_bisaminomethyl_cyclohexane_DGEBA_1_3_BAC_epoxy_resin_system"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="4" data-entity-id="5305306" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/5305306/Isothermal_cure_kinetics_of_a_diglycidyl_ether_of_bisphenol_A_1_3_bisaminomethylcyclohexane_DGEBA_1_3BAC_epoxy_resin_system">Isothermal cure kinetics of a diglycidyl ether of bisphenol A/1,3-bisaminomethylcyclohexane (DGEBA/1,3BAC) epoxy resin system</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="7312082" href="https://independent.academia.edu/lopezjoaquin">joaquin lopez</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Applied Polymer Science, 1995</p><p class="ds-related-work--abstract ds2-5-body-sm">By employing differential scaning calorimetry, DSC, we have studied, under isothermal conditions, the kinetics of the cure reaction for a system containing a diglycidyl ether of bisphenol A (DGEBA) and 1,3-bisaminomethylcyclohexane (1,3-BAC) as a curing agent, over the temperature range of 60–110°C. We have determined the conversions reached at several cure temperatures and the reaction rates. The experimental data, showing an autocatalytic behavior, were compared with the model proposed by Kamal, which includes two rate constants, k1 and k2, and two reaction orders, m and n. This model gives a good description of cure kinetics up to the onset of vitrification. The activation energies for these rate constants were 44–57 kJ/mol. The reaction orders present a moderate change but their sum is in the range 2.5–3. Diffusion control is incorporated to describe the cure in the latter stages (postivitrification region). By combining the autocatalytic model and a diffusion factor, it was possible to predict the cure kinetics over the whole range of conversion. © 1995 John Wiley & Sons, Inc.</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Isothermal cure kinetics of a diglycidyl ether of bisphenol A/1,3-bisaminomethylcyclohexane (DGEBA/1,3BAC) epoxy resin system","attachmentId":49355821,"attachmentType":"pdf","work_url":"https://www.academia.edu/5305306/Isothermal_cure_kinetics_of_a_diglycidyl_ether_of_bisphenol_A_1_3_bisaminomethylcyclohexane_DGEBA_1_3BAC_epoxy_resin_system","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/5305306/Isothermal_cure_kinetics_of_a_diglycidyl_ether_of_bisphenol_A_1_3_bisaminomethylcyclohexane_DGEBA_1_3BAC_epoxy_resin_system"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="5" data-entity-id="14955533" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/14955533/Mechanism_and_Kinetics_of_Epoxy_Amine_Cure_Studied_by_Differential_Scanning_Calorimetry">Mechanism and Kinetics of Epoxy−Amine Cure Studied by Differential Scanning Calorimetry</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="33950313" href="https://landaverde.academia.edu/NicolasSbirrazzuoli">Nicolas Sbirrazzuoli</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Macromolecules, 1996</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Mechanism and Kinetics of Epoxy−Amine Cure Studied by Differential Scanning Calorimetry","attachmentId":43703683,"attachmentType":"pdf","work_url":"https://www.academia.edu/14955533/Mechanism_and_Kinetics_of_Epoxy_Amine_Cure_Studied_by_Differential_Scanning_Calorimetry","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/14955533/Mechanism_and_Kinetics_of_Epoxy_Amine_Cure_Studied_by_Differential_Scanning_Calorimetry"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="6" data-entity-id="4285085" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/4285085/Cure_Kinetics_Study_of_Two_Epoxy_Systems_with_Fourier_Tranform_Infrared_Spectroscopy_FTIR_and_Differential_Scanning_Calorimetry_DSC_">Cure Kinetics Study of Two Epoxy Systems with Fourier Tranform Infrared Spectroscopy (FTIR) and Differential Scanning Calorimetry (DSC)</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="5189413" href="https://auth.academia.edu/%CE%95%CE%99%CE%A1%CE%97%CE%9D%CE%97%CE%A3%CE%B9%CE%B4%CE%B5%CF%81%CE%AF%CE%B4%CE%BF%CF%85">Ειρήνη Σιδερίδου-Καραγιαννίδου</a></div><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Cure Kinetics Study of Two Epoxy Systems with Fourier Tranform Infrared Spectroscopy (FTIR) and Differential Scanning Calorimetry (DSC)","attachmentId":31753253,"attachmentType":"pdf","work_url":"https://www.academia.edu/4285085/Cure_Kinetics_Study_of_Two_Epoxy_Systems_with_Fourier_Tranform_Infrared_Spectroscopy_FTIR_and_Differential_Scanning_Calorimetry_DSC_","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/4285085/Cure_Kinetics_Study_of_Two_Epoxy_Systems_with_Fourier_Tranform_Infrared_Spectroscopy_FTIR_and_Differential_Scanning_Calorimetry_DSC_"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="7" data-entity-id="88555489" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/88555489/Alternating_differential_scanning_calorimetry_Isothermal_curing_of_the_epoxy_resin">Alternating differential scanning calorimetry: Isothermal curing of the epoxy resin</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="16092051" href="https://independent.academia.edu/IdaPoljansek">Ida Poljansek</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Acta Chimica Slovenica, 2003</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Alternating differential scanning calorimetry: Isothermal curing of the epoxy resin","attachmentId":92507903,"attachmentType":"pdf","work_url":"https://www.academia.edu/88555489/Alternating_differential_scanning_calorimetry_Isothermal_curing_of_the_epoxy_resin","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/88555489/Alternating_differential_scanning_calorimetry_Isothermal_curing_of_the_epoxy_resin"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="8" data-entity-id="27419197" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/27419197/Cure_kinetics_of_a_liquid_crystalline_epoxy_resin_studied_by_non_isothermal_data">Cure kinetics of a liquid-crystalline epoxy resin studied by non-isothermal data</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="51458251" href="https://independent.academia.edu/DanRosu3">Dan Rosu</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Polymer Testing, 2004</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Cure kinetics of a liquid-crystalline epoxy resin studied by non-isothermal data","attachmentId":47675861,"attachmentType":"pdf","work_url":"https://www.academia.edu/27419197/Cure_kinetics_of_a_liquid_crystalline_epoxy_resin_studied_by_non_isothermal_data","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/27419197/Cure_kinetics_of_a_liquid_crystalline_epoxy_resin_studied_by_non_isothermal_data"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="9" data-entity-id="4084167" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/4084167/Cure_kinetics_of_ternary_blends_of_epoxy_resins_studied_by_nonisothermal_DSC_data">Cure kinetics of ternary blends of epoxy resins studied by nonisothermal DSC data</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="4924324" href="https://independent.academia.edu/GarimaTripathi">Garima Tripathi</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Applied Polymer Science, 2009</p><p class="ds-related-work--abstract ds2-5-body-sm">The curing kinetics of blends of diglycidyl ether of bisphenol A (DGEBA), cycloaliphatic epoxy resins, and carboxyl-terminated butadiene-acrylonitrile random copolymer (CTBN) in presence of 4,4′-diamino diphenyl sulfone (DDS) as the curing agent was studied by nonisothermal differential scanning calorimetry (DSC) technique at different heating rates. The kinetic parameters of the curing process were determined by isoconversional method given by Malek for the kinetic analysis of the data obtained by the thermal treatment. A two-parameter (m, n) autocatalytic model (Sestak-Berggren equation) was found to be the most adequate selected to describe the cure kinetics of the studied epoxy resins. The values of Ea were found to be 88.6 kJ mol−1 and 61.6 kJ mol−1, respectively, for the studied two sample series. Nonisothermal DSC curves obtained using the experimental data show a good agreement with that theoretically calculated. © 2009 Wiley Periodicals, Inc. J Appl Polym Sci, 2009</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Cure kinetics of ternary blends of epoxy resins studied by nonisothermal DSC data","attachmentId":50042789,"attachmentType":"pdf","work_url":"https://www.academia.edu/4084167/Cure_kinetics_of_ternary_blends_of_epoxy_resins_studied_by_nonisothermal_DSC_data","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/4084167/Cure_kinetics_of_ternary_blends_of_epoxy_resins_studied_by_nonisothermal_DSC_data"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div></div></div><div class="ds-sticky-ctas--wrapper js-loswp-sticky-ctas hidden"><div class="ds-sticky-ctas--grid-container"><div class="ds-sticky-ctas--container"><button class="ds2-5-button js-swp-download-button" data-signup-modal="{"location":"continue-reading-button--sticky-ctas","attachmentId":85319008,"attachmentType":"pdf","workUrl":null}">See full PDF</button><button class="ds2-5-button ds2-5-button--secondary js-swp-download-button" data-signup-modal="{"location":"download-pdf-button--sticky-ctas","attachmentId":85319008,"attachmentType":"pdf","workUrl":null}"><span class="material-symbols-outlined" style="font-size: 20px" translate="no">download</span>Download PDF</button></div></div></div><div class="ds-below-fold--grid-container"><div class="ds-work--container js-loswp-embedded-document"><div class="attachment_preview" data-attachment="Attachment_85319008" style="display: none"><div class="js-scribd-document-container"><div class="scribd--document-loading js-scribd-document-loader" style="display: block;"><img alt="Loading..." src="//a.academia-assets.com/images/loaders/paper-load.gif" /><p>Loading Preview</p></div></div><div style="text-align: center;"><div class="scribd--no-preview-alert js-preview-unavailable"><p>Sorry, preview is currently unavailable. 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href="https://utp-my.academia.edu/ZakariaMan">Zakaria Man</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Applied Polymer Science, 2009</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Reaction kinetics of epoxy resin modified with reactive and nonreactive thermoplastic copolymers","attachmentId":44321040,"attachmentType":"pdf","work_url":"https://www.academia.edu/14322133/Reaction_kinetics_of_epoxy_resin_modified_with_reactive_and_nonreactive_thermoplastic_copolymers","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-related-work-grid-card-view-pdf" href="https://www.academia.edu/14322133/Reaction_kinetics_of_epoxy_resin_modified_with_reactive_and_nonreactive_thermoplastic_copolymers"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-related-work-sidebar-card" data-collection-position="5" data-entity-id="14955541" data-sort-order="default"><a class="ds-related-work--title js-related-work-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/14955541/Isoconversional_kinetic_analysis_of_stoichiometric_and_off_stoichiometric_epoxy_amine_cures">Isoconversional kinetic analysis of stoichiometric and off-stoichiometric epoxy-amine cures</a><div class="ds-related-work--metadata"><a class="js-related-work-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="34129734" href="https://landaverde.academia.edu/LucVincent">Luc Vincent</a><span>, 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