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Dean of Faculty of Sciences of Universiy of Santiago de Compostela from 2002 to 2010. President of Spanish Group of Calorimetry and Thermal Analysis from 2010 to 2015. Vocal of Spanish Group of Calorimetry and Thermal Analysis from 2015.<br /><div class="js-profile-less-about u-linkUnstyled u-tcGrayDarker u-textDecorationUnderline u-displayNone">less</div></div></div><div class="ri-section"><div class="ri-section-header"><span>Interests</span></div><div class="ri-tags-container"><a data-click-track="profile-user-info-expand-research-interests" data-has-card-for-ri-list="45089310" href="https://www.academia.edu/Documents/in/Ingeneria_Sistemas_Computacionales"><div id="js-react-on-rails-context" style="display:none" data-rails-context="{"inMailer":false,"i18nLocale":"en","i18nDefaultLocale":"en","href":"https://independent.academia.edu/FragaFrancisco","location":"/FragaFrancisco","scheme":"https","host":"independent.academia.edu","port":null,"pathname":"/FragaFrancisco","search":null,"httpAcceptLanguage":null,"serverSide":false}"></div> <div class="js-react-on-rails-component" style="display:none" data-component-name="Pill" 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class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/117179532/Effect_of_Gold_Nanoparticles_on_the_Physical_Properties_of_an_Epoxy_Resin"><img alt="Research paper thumbnail of Effect of Gold Nanoparticles on the Physical Properties of an Epoxy Resin" class="work-thumbnail" src="https://attachments.academia-assets.com/113104770/thumbnails/1.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/117179532/Effect_of_Gold_Nanoparticles_on_the_Physical_Properties_of_an_Epoxy_Resin">Effect of Gold Nanoparticles on the Physical Properties of an Epoxy Resin</a></div><div class="wp-workCard_item"><span>International Journal of Molecular Sciences</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">The effect of doping the bisphenol A diglycidyl ether (DGEBA)/m-xylylenediamine (mXDA) system wit...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">The effect of doping the bisphenol A diglycidyl ether (DGEBA)/m-xylylenediamine (mXDA) system with gold nanoparticles (AuNP) has been studied with differential scanning calorimetry (DSC), thermogravimetric analysis, dynamic mechanical analysis (DMA), and dielectric analysis (DEA). The evolved heat (ΔHt), the glass transition temperature (Tg), and the associated activation energies of this relaxation process have been determined. Below a certain concentration of AuNPs (=8.5%, in mg AuNP/g epoxy matrix), Tg decreases linearly with the concentration of AuNPs, but above it, Tg is not affected. The degree of conversion α of this epoxy system was analyzed by the semiempirical Kamal’s model, evidencing that diffusion correction is required at high values of α. Activation energy values suggest that AuNPs can cause some impediments at the beginning of the crosslinking process (n-order mechanism). The slight difference between the initial decomposition temperature, as well as the temperature ...</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><a id="b5a9f691d2b089877f43163beb01840e" class="wp-workCard--action" rel="nofollow" data-click-track="profile-work-strip-download" data-download="{"attachment_id":113104770,"asset_id":117179532,"asset_type":"Work","button_location":"profile"}" href="https://www.academia.edu/attachments/113104770/download_file?st=MTczMjUwNjk4Miw4LjIyMi4yMDguMTQ2&s=profile"><span><i class="fa fa-arrow-down"></i></span><span>Download</span></a><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="117179532"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="117179532"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 117179532; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=117179532]").text(description); $(".js-view-count[data-work-id=117179532]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 117179532; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='117179532']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 117179532, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (true){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "b5a9f691d2b089877f43163beb01840e" } } $('.js-work-strip[data-work-id=117179532]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":117179532,"title":"Effect of Gold Nanoparticles on the Physical Properties of an Epoxy Resin","translated_title":"","metadata":{"abstract":"The effect of doping the bisphenol A diglycidyl ether (DGEBA)/m-xylylenediamine (mXDA) system with gold nanoparticles (AuNP) has been studied with differential scanning calorimetry (DSC), thermogravimetric analysis, dynamic mechanical analysis (DMA), and dielectric analysis (DEA). 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data-click-track="profile-work-strip-title" href="https://www.academia.edu/117179531/Simple_route_for_nano_hydroxyapatite_properties_expansion">Simple route for nano-hydroxyapatite properties expansion</a></div><div class="wp-workCard_item"><span>Biomedical Materials</span><span>, 2015</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">Simple surface modification of nano-hydroxyapatite, through acid-basic reactions, allows expandin...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">Simple surface modification of nano-hydroxyapatite, through acid-basic reactions, allows expanding the properties of this material. Introduction of organic groups such as hydrophobic alkyl chains, carboxylic acid, and amide or amine basic groups on the hydroxyapatite surface systematically change the polarity, surface area, and reactivity of hydroxyapatite without modifying its phase. Physical and chemical properties of the new derivative particles were analyzed. The biocompatibility of modified Nano-Hap on Raw 264.7 cells was also assessed.</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="117179531"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="117179531"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 117179531; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=117179531]").text(description); $(".js-view-count[data-work-id=117179531]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 117179531; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='117179531']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 117179531, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=117179531]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":117179531,"title":"Simple route for nano-hydroxyapatite properties expansion","translated_title":"","metadata":{"abstract":"Simple surface modification of nano-hydroxyapatite, through acid-basic reactions, allows expanding the properties of this material. 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Castro-Díaz, C.; Rodríguez-Núñez, E.; Martínez-Ageitos, JM J Appl Polym Sci, to ...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">... 7 Fraga, F.; Castro-Díaz, C.; Rodríguez-Núñez, E.; Martínez-Ageitos, JM J Appl Polym Sci, to appear. 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class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/117179526/Influence_of_water_absorption_on_the_mechanical_properties_of_a_DGEBA_n_0_1_2_DCH_epoxy_system">Influence of water absorption on the mechanical properties of a DGEBA (n = 0)/1, 2 DCH epoxy system</a></div><div class="wp-workCard_item"><span>Journal of Applied Polymer Science</span><span>, 1999</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">... Lisardo Núñez,; M. Villanueva,; F. Fraga,; MR Núñez. Article first published online: 28 JUL 1...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">... Lisardo Núñez,; M. Villanueva,; F. Fraga,; MR Núñez. Article first published online: 28 JUL 1999. DOI: 10.1002/(SICI)1097-4628(19991010)74:2&lt;353::AID-APP17&gt;3.0.CO;2-J. Copyright © 1999John Wiley &amp; Sons, Inc. Issue. 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Determination of the optimum value of the epoxy/curing agent ratio was studied by means of differential scanning calorimetry. The method is based on the search for the maximum enthalpy change'. It was found that this maximum corresponds to a 100/34 value. The glass transition temperature (Tg) has been calculated using dynamic methods. Our values are in good agreement with those in the l i t e r a t~r e~3~ for similar systems. At the same time other kinetic parameters were obtained using an isothermal method and the ratio values previously calculated. 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scanning calorimetry","url":"https://www.academia.edu/Documents/in/Differential_scanning_calorimetry"},{"id":82446,"name":"bisphenol A","url":"https://www.academia.edu/Documents/in/bisphenol_A"},{"id":159672,"name":"Epoxy","url":"https://www.academia.edu/Documents/in/Epoxy"},{"id":260118,"name":"CHEMICAL SCIENCES","url":"https://www.academia.edu/Documents/in/CHEMICAL_SCIENCES"},{"id":335228,"name":"Glass Transition Temperature","url":"https://www.academia.edu/Documents/in/Glass_Transition_Temperature"},{"id":413295,"name":"Kinetic Energy","url":"https://www.academia.edu/Documents/in/Kinetic_Energy"},{"id":632908,"name":"Epoxy Resin","url":"https://www.academia.edu/Documents/in/Epoxy_Resin"},{"id":780855,"name":"Agent Systems","url":"https://www.academia.edu/Documents/in/Agent_Systems"},{"id":1167882,"name":"Kinetic Parameter","url":"https://www.academia.edu/Documents/in/Kinetic_Parameter"},{"id":2711473,"name":"Pure and Applied Chemistry","url":"https://www.academia.edu/Documents/in/Pure_and_Applied_Chemistry"}],"urls":[{"id":38576615,"url":"https://www.degruyter.com/document/doi/10.1351/pac199567071091/pdf"}]}, dispatcherData: dispatcherData }); $(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="113507963"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/113507963/The_influence_of_lixiviates_on_the_thermal_degradation_of_diglycidyl_ether_of_bisphenol_An_0_1_2_diaminecyclohexane_studied_by_dynamic_mechanical_analysis_and_thermogravimetry_fourier_transform_infrared_spectroscopy"><img alt="Research paper thumbnail of The influence of lixiviates on the thermal degradation of diglycidyl ether of bisphenol An=0/1,2-diaminecyclohexane studied by dynamic mechanical analysis and thermogravimetry-fourier transform infrared spectroscopy" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/113507963/The_influence_of_lixiviates_on_the_thermal_degradation_of_diglycidyl_ether_of_bisphenol_An_0_1_2_diaminecyclohexane_studied_by_dynamic_mechanical_analysis_and_thermogravimetry_fourier_transform_infrared_spectroscopy">The influence of lixiviates on the thermal degradation of diglycidyl ether of bisphenol An=0/1,2-diaminecyclohexane studied by dynamic mechanical analysis and thermogravimetry-fourier transform infrared spectroscopy</a></div><div class="wp-workCard_item"><span>Journal of Applied Polymer Science</span><span>, 1999</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">ABSTRACT The influence of the lixiviates originated in a municipal landfill on the thermal degrad...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">ABSTRACT The influence of the lixiviates originated in a municipal landfill on the thermal degradation of a polymeric system composed of a diglycidyl ether of bisphenol A (n = 0) and 1,2-diaminecyclohexane was studied by dynamic mechanical analysis. Storage modulus (E′), loss modulus (E″), and glass transition temperature were measured to make a comparative study between the samples before and after being exposed to the chemical compounds in the lixiviate agents. The different data obtained were analyzed to check the resistance of these materials to chemical attack and the possibility of their use as coating materials in plants where those reagents were present. Thermal stability of the system diglycidyl ether of bisphenol A/1,2-diaminecyclohexane exposed to the attack of lixiviates has also been studied by thermogravimetric analysis. A quantitative study of the gases originated during thermal degradation of the epoxy/diamine system made by infrared spectroscopy. © 1999 John Wiley &amp;amp;amp; Sons, Inc. J Appl Polym Sci 72: 443–453, 1999</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="113507963"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="113507963"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 113507963; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=113507963]").text(description); $(".js-view-count[data-work-id=113507963]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 113507963; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='113507963']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 113507963, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=113507963]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":113507963,"title":"The influence of lixiviates on the thermal degradation of diglycidyl ether of bisphenol An=0/1,2-diaminecyclohexane studied by dynamic mechanical analysis and thermogravimetry-fourier transform infrared spectroscopy","translated_title":"","metadata":{"abstract":"ABSTRACT The influence of the lixiviates originated in a municipal landfill on the thermal degradation of a polymeric system composed of a diglycidyl ether of bisphenol A (n = 0) and 1,2-diaminecyclohexane was studied by dynamic mechanical analysis. Storage modulus (E′), loss modulus (E″), and glass transition temperature were measured to make a comparative study between the samples before and after being exposed to the chemical compounds in the lixiviate agents. The different data obtained were analyzed to check the resistance of these materials to chemical attack and the possibility of their use as coating materials in plants where those reagents were present. Thermal stability of the system diglycidyl ether of bisphenol A/1,2-diaminecyclohexane exposed to the attack of lixiviates has also been studied by thermogravimetric analysis. A quantitative study of the gases originated during thermal degradation of the epoxy/diamine system made by infrared spectroscopy. © 1999 John Wiley \u0026amp;amp;amp; Sons, Inc. J Appl Polym Sci 72: 443–453, 1999","publisher":"Wiley","publication_date":{"day":null,"month":null,"year":1999,"errors":{}},"publication_name":"Journal of Applied Polymer Science"},"translated_abstract":"ABSTRACT The influence of the lixiviates originated in a municipal landfill on the thermal degradation of a polymeric system composed of a diglycidyl ether of bisphenol A (n = 0) and 1,2-diaminecyclohexane was studied by dynamic mechanical analysis. Storage modulus (E′), loss modulus (E″), and glass transition temperature were measured to make a comparative study between the samples before and after being exposed to the chemical compounds in the lixiviate agents. The different data obtained were analyzed to check the resistance of these materials to chemical attack and the possibility of their use as coating materials in plants where those reagents were present. Thermal stability of the system diglycidyl ether of bisphenol A/1,2-diaminecyclohexane exposed to the attack of lixiviates has also been studied by thermogravimetric analysis. A quantitative study of the gases originated during thermal degradation of the epoxy/diamine system made by infrared spectroscopy. © 1999 John Wiley \u0026amp;amp;amp; Sons, Inc. J Appl Polym Sci 72: 443–453, 1999","internal_url":"https://www.academia.edu/113507963/The_influence_of_lixiviates_on_the_thermal_degradation_of_diglycidyl_ether_of_bisphenol_An_0_1_2_diaminecyclohexane_studied_by_dynamic_mechanical_analysis_and_thermogravimetry_fourier_transform_infrared_spectroscopy","translated_internal_url":"","created_at":"2024-01-14T22:35:13.722-08:00","preview_url":null,"current_user_can_edit":null,"current_user_is_owner":null,"owner_id":45089310,"coauthors_can_edit":true,"document_type":"paper","co_author_tags":[],"downloadable_attachments":[],"slug":"The_influence_of_lixiviates_on_the_thermal_degradation_of_diglycidyl_ether_of_bisphenol_An_0_1_2_diaminecyclohexane_studied_by_dynamic_mechanical_analysis_and_thermogravimetry_fourier_transform_infrared_spectroscopy","translated_slug":"","page_count":null,"language":"en","content_type":"Work","owner":{"id":45089310,"first_name":"Francisco","middle_initials":null,"last_name":"Fraga López","page_name":"FragaFrancisco","domain_name":"independent","created_at":"2016-03-14T09:17:24.694-07:00","display_name":"Francisco Fraga López","url":"https://independent.academia.edu/FragaFrancisco"},"attachments":[],"research_interests":[{"id":48,"name":"Engineering","url":"https://www.academia.edu/Documents/in/Engineering"},{"id":511,"name":"Materials Science","url":"https://www.academia.edu/Documents/in/Materials_Science"},{"id":523,"name":"Chemistry","url":"https://www.academia.edu/Documents/in/Chemistry"},{"id":82446,"name":"bisphenol A","url":"https://www.academia.edu/Documents/in/bisphenol_A"},{"id":159672,"name":"Epoxy","url":"https://www.academia.edu/Documents/in/Epoxy"},{"id":246949,"name":"Thermogravimetry","url":"https://www.academia.edu/Documents/in/Thermogravimetry"},{"id":260118,"name":"CHEMICAL SCIENCES","url":"https://www.academia.edu/Documents/in/CHEMICAL_SCIENCES"},{"id":282351,"name":"Glass Transition","url":"https://www.academia.edu/Documents/in/Glass_Transition"},{"id":389180,"name":"Thermal Stability","url":"https://www.academia.edu/Documents/in/Thermal_Stability"},{"id":398650,"name":"Fourier transform infrared spectroscopy","url":"https://www.academia.edu/Documents/in/Fourier_transform_infrared_spectroscopy"},{"id":398652,"name":"Thermogravimetric Analysis","url":"https://www.academia.edu/Documents/in/Thermogravimetric_Analysis"},{"id":966213,"name":"Journal of Applied Polymer Science","url":"https://www.academia.edu/Documents/in/Journal_of_Applied_Polymer_Science"},{"id":1431635,"name":"Dynamic Mechanical Analysis","url":"https://www.academia.edu/Documents/in/Dynamic_Mechanical_Analysis"}],"urls":[{"id":38576614,"url":"https://api.wiley.com/onlinelibrary/tdm/v1/articles/10.1002%2F(SICI)1097-4628(19990418)72:3%3C443::AID-APP14%3E3.0.CO;2-X"}]}, dispatcherData: dispatcherData }); $(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="113507962"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/113507962/Kinetic_study_and_time_temperature_transformation_cure_diagram_for_an_epoxy_diamine_system"><img alt="Research paper thumbnail of Kinetic study and time‐temperature‐transformation cure diagram for an epoxy‐diamine system" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/113507962/Kinetic_study_and_time_temperature_transformation_cure_diagram_for_an_epoxy_diamine_system">Kinetic study and time‐temperature‐transformation cure diagram for an epoxy‐diamine system</a></div><div class="wp-workCard_item"><span>Journal of Applied Polymer Science</span><span>, 1997</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">... Lisardo Núñez,; J. Taboada,; F. Fraga,; MR Núñez. Article first published online: 7 DEC 1998....</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">... Lisardo Núñez,; J. Taboada,; F. Fraga,; MR Núñez. Article first published online: 7 DEC 1998. DOI: 10.1002/(SICI)1097-4628(19971114)66:7&lt;1377::AID-APP16&gt;3.0.CO;2-#. Copyright © 1997John Wiley &amp; Sons, Inc. Issue. Journal of Applied Polymer Science. ...</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="113507962"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="113507962"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 113507962; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=113507962]").text(description); $(".js-view-count[data-work-id=113507962]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 113507962; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='113507962']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 113507962, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=113507962]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":113507962,"title":"Kinetic study and time‐temperature‐transformation cure diagram for an epoxy‐diamine system","translated_title":"","metadata":{"abstract":"... Lisardo Núñez,; J. Taboada,; F. Fraga,; MR Núñez. Article first published online: 7 DEC 1998. DOI: 10.1002/(SICI)1097-4628(19971114)66:7\u0026lt;1377::AID-APP16\u0026gt;3.0.CO;2-#. Copyright © 1997John Wiley \u0026amp; Sons, Inc. Issue. Journal of Applied Polymer Science. ...","publisher":"Wiley","publication_date":{"day":null,"month":null,"year":1997,"errors":{}},"publication_name":"Journal of Applied Polymer Science"},"translated_abstract":"... Lisardo Núñez,; J. Taboada,; F. Fraga,; MR Núñez. Article first published online: 7 DEC 1998. DOI: 10.1002/(SICI)1097-4628(19971114)66:7\u0026lt;1377::AID-APP16\u0026gt;3.0.CO;2-#. Copyright © 1997John Wiley \u0026amp; Sons, Inc. Issue. Journal of Applied Polymer Science. ...","internal_url":"https://www.academia.edu/113507962/Kinetic_study_and_time_temperature_transformation_cure_diagram_for_an_epoxy_diamine_system","translated_internal_url":"","created_at":"2024-01-14T22:35:13.524-08:00","preview_url":null,"current_user_can_edit":null,"current_user_is_owner":null,"owner_id":45089310,"coauthors_can_edit":true,"document_type":"paper","co_author_tags":[],"downloadable_attachments":[],"slug":"Kinetic_study_and_time_temperature_transformation_cure_diagram_for_an_epoxy_diamine_system","translated_slug":"","page_count":null,"language":"en","content_type":"Work","owner":{"id":45089310,"first_name":"Francisco","middle_initials":null,"last_name":"Fraga López","page_name":"FragaFrancisco","domain_name":"independent","created_at":"2016-03-14T09:17:24.694-07:00","display_name":"Francisco Fraga López","url":"https://independent.academia.edu/FragaFrancisco"},"attachments":[],"research_interests":[{"id":48,"name":"Engineering","url":"https://www.academia.edu/Documents/in/Engineering"},{"id":511,"name":"Materials Science","url":"https://www.academia.edu/Documents/in/Materials_Science"},{"id":523,"name":"Chemistry","url":"https://www.academia.edu/Documents/in/Chemistry"},{"id":4987,"name":"Kinetics","url":"https://www.academia.edu/Documents/in/Kinetics"},{"id":96502,"name":"Applied","url":"https://www.academia.edu/Documents/in/Applied"},{"id":159672,"name":"Epoxy","url":"https://www.academia.edu/Documents/in/Epoxy"},{"id":199746,"name":"Diagram","url":"https://www.academia.edu/Documents/in/Diagram"},{"id":260118,"name":"CHEMICAL SCIENCES","url":"https://www.academia.edu/Documents/in/CHEMICAL_SCIENCES"},{"id":413295,"name":"Kinetic Energy","url":"https://www.academia.edu/Documents/in/Kinetic_Energy"},{"id":966213,"name":"Journal of Applied Polymer Science","url":"https://www.academia.edu/Documents/in/Journal_of_Applied_Polymer_Science"}],"urls":[{"id":38576613,"url":"https://onlinelibrary.wiley.com/doi/pdf/10.1002/(SICI)1097-4628(19971114)66:7%3C1377::AID-APP16%3E3.0.CO;2-%23"}]}, dispatcherData: dispatcherData }); $(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="113507961"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/113507961/Curing_kinetic_of_the_epoxy_system_badge_n_0_1_2_DCH_by_fourier_transform_infrared_spectroscopy_FTIR_"><img alt="Research paper thumbnail of Curing kinetic of the epoxy system badge n = 0/1,2 DCH by fourier transform infrared spectroscopy (FTIR)" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/113507961/Curing_kinetic_of_the_epoxy_system_badge_n_0_1_2_DCH_by_fourier_transform_infrared_spectroscopy_FTIR_">Curing kinetic of the epoxy system badge n = 0/1,2 DCH by fourier transform infrared spectroscopy (FTIR)</a></div><div class="wp-workCard_item"><span>Journal of Applied Polymer Science</span><span>, 2001</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">The curing reaction of an epoxy system consisting of a diglycidyl ether of bisphenol A (BADGE n =...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">The curing reaction of an epoxy system consisting of a diglycidyl ether of bisphenol A (BADGE n = 0) and 1,2‐diaminocyclohexane (DCH) was studied by Fourier Trasform Infrared Spectroscopy (FTIR). From the infrared spectra using a peak‐height method, that was based on the ratio of the height of the characteristic to reference absorbance peak, degree of conversion at different isothermal temperatures were calculated. From a kinetic study, the Horie et al. model was used; parameters such as rate constants and activation energies were determined. The results were compared to those obtained for same epoxy systems using scanning differential calorimetry (DSC). © 2001 John Wiley & Sons, Inc. J Appl Polym Sci 82: 3366–3372, 2001</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="113507961"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="113507961"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 113507961; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=113507961]").text(description); $(".js-view-count[data-work-id=113507961]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 113507961; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='113507961']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 113507961, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=113507961]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":113507961,"title":"Curing kinetic of the epoxy system badge n = 0/1,2 DCH by fourier transform infrared spectroscopy (FTIR)","translated_title":"","metadata":{"abstract":"The curing reaction of an epoxy system consisting of a diglycidyl ether of bisphenol A (BADGE n = 0) and 1,2‐diaminocyclohexane (DCH) was studied by Fourier Trasform Infrared Spectroscopy (FTIR). From the infrared spectra using a peak‐height method, that was based on the ratio of the height of the characteristic to reference absorbance peak, degree of conversion at different isothermal temperatures were calculated. From a kinetic study, the Horie et al. model was used; parameters such as rate constants and activation energies were determined. The results were compared to those obtained for same epoxy systems using scanning differential calorimetry (DSC). © 2001 John Wiley \u0026 Sons, Inc. J Appl Polym Sci 82: 3366–3372, 2001","publisher":"Wiley","publication_date":{"day":null,"month":null,"year":2001,"errors":{}},"publication_name":"Journal of Applied Polymer Science"},"translated_abstract":"The curing reaction of an epoxy system consisting of a diglycidyl ether of bisphenol A (BADGE n = 0) and 1,2‐diaminocyclohexane (DCH) was studied by Fourier Trasform Infrared Spectroscopy (FTIR). From the infrared spectra using a peak‐height method, that was based on the ratio of the height of the characteristic to reference absorbance peak, degree of conversion at different isothermal temperatures were calculated. From a kinetic study, the Horie et al. model was used; parameters such as rate constants and activation energies were determined. The results were compared to those obtained for same epoxy systems using scanning differential calorimetry (DSC). © 2001 John Wiley \u0026 Sons, Inc. J Appl Polym Sci 82: 3366–3372, 2001","internal_url":"https://www.academia.edu/113507961/Curing_kinetic_of_the_epoxy_system_badge_n_0_1_2_DCH_by_fourier_transform_infrared_spectroscopy_FTIR_","translated_internal_url":"","created_at":"2024-01-14T22:35:13.381-08:00","preview_url":null,"current_user_can_edit":null,"current_user_is_owner":null,"owner_id":45089310,"coauthors_can_edit":true,"document_type":"paper","co_author_tags":[],"downloadable_attachments":[],"slug":"Curing_kinetic_of_the_epoxy_system_badge_n_0_1_2_DCH_by_fourier_transform_infrared_spectroscopy_FTIR_","translated_slug":"","page_count":null,"language":"en","content_type":"Work","owner":{"id":45089310,"first_name":"Francisco","middle_initials":null,"last_name":"Fraga López","page_name":"FragaFrancisco","domain_name":"independent","created_at":"2016-03-14T09:17:24.694-07:00","display_name":"Francisco Fraga López","url":"https://independent.academia.edu/FragaFrancisco"},"attachments":[],"research_interests":[{"id":48,"name":"Engineering","url":"https://www.academia.edu/Documents/in/Engineering"},{"id":511,"name":"Materials Science","url":"https://www.academia.edu/Documents/in/Materials_Science"},{"id":523,"name":"Chemistry","url":"https://www.academia.edu/Documents/in/Chemistry"},{"id":4987,"name":"Kinetics","url":"https://www.academia.edu/Documents/in/Kinetics"},{"id":78753,"name":"Differential scanning calorimetry","url":"https://www.academia.edu/Documents/in/Differential_scanning_calorimetry"},{"id":78842,"name":"Infrared spectroscopy","url":"https://www.academia.edu/Documents/in/Infrared_spectroscopy"},{"id":159672,"name":"Epoxy","url":"https://www.academia.edu/Documents/in/Epoxy"},{"id":260118,"name":"CHEMICAL SCIENCES","url":"https://www.academia.edu/Documents/in/CHEMICAL_SCIENCES"},{"id":398650,"name":"Fourier transform infrared spectroscopy","url":"https://www.academia.edu/Documents/in/Fourier_transform_infrared_spectroscopy"},{"id":753116,"name":"Absorbance","url":"https://www.academia.edu/Documents/in/Absorbance"},{"id":966213,"name":"Journal of Applied Polymer Science","url":"https://www.academia.edu/Documents/in/Journal_of_Applied_Polymer_Science"}],"urls":[{"id":38576612,"url":"https://onlinelibrary.wiley.com/doi/pdf/10.1002/app.2195"}]}, dispatcherData: dispatcherData }); $(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="113507945"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/113507945/Mechanism_and_Activation_Energies_in_Different_Blends_of_Poly_caprolactone_with_Polyethyleneglycol_PEG_and_Polyvinyl_Alcohol_PVA_"><img alt="Research paper thumbnail of Mechanism and Activation Energies in Different Blends of Poly-( -caprolactone) with Polyethyleneglycol (PEG) and Polyvinyl Alcohol (PVA)" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/113507945/Mechanism_and_Activation_Energies_in_Different_Blends_of_Poly_caprolactone_with_Polyethyleneglycol_PEG_and_Polyvinyl_Alcohol_PVA_">Mechanism and Activation Energies in Different Blends of Poly-( -caprolactone) with Polyethyleneglycol (PEG) and Polyvinyl Alcohol (PVA)</a></div><div class="wp-workCard_item"><span>Materials Focus</span><span>, 2014</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">ABSTRACT In this article we study the calorimetric characterization using different differential ...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">ABSTRACT In this article we study the calorimetric characterization using different differential and integral kinetic methods with data from differential scanning calorimeter (DSC). The correlation of activation energies obtained using Kissinger and Flynn–Wall–Ozawa integral methods were lower than 0.99, so it was necessary used the Coats–Redfern Method to determinate the activation energies and the mechanism of fluid-crystalline phase transitionprocess. This mechanisms follows nucleation and growth model (sigmoidal A4 type an Avrami 3 mechanism). This study permits to obtain a tool to predict the disorder of the structure for hydrophobic or hydrophilic samples that could be used to the release of the drugs.</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="113507945"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="113507945"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 113507945; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=113507945]").text(description); $(".js-view-count[data-work-id=113507945]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 113507945; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='113507945']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 113507945, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=113507945]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":113507945,"title":"Mechanism and Activation Energies in Different Blends of Poly-( -caprolactone) with Polyethyleneglycol (PEG) and Polyvinyl Alcohol (PVA)","translated_title":"","metadata":{"abstract":"ABSTRACT In this article we study the calorimetric characterization using different differential and integral kinetic methods with data from differential scanning calorimeter (DSC). The correlation of activation energies obtained using Kissinger and Flynn–Wall–Ozawa integral methods were lower than 0.99, so it was necessary used the Coats–Redfern Method to determinate the activation energies and the mechanism of fluid-crystalline phase transitionprocess. This mechanisms follows nucleation and growth model (sigmoidal A4 type an Avrami 3 mechanism). This study permits to obtain a tool to predict the disorder of the structure for hydrophobic or hydrophilic samples that could be used to the release of the drugs.","publisher":"American Scientific Publishers","publication_date":{"day":null,"month":null,"year":2014,"errors":{}},"publication_name":"Materials Focus"},"translated_abstract":"ABSTRACT In this article we study the calorimetric characterization using different differential and integral kinetic methods with data from differential scanning calorimeter (DSC). The correlation of activation energies obtained using Kissinger and Flynn–Wall–Ozawa integral methods were lower than 0.99, so it was necessary used the Coats–Redfern Method to determinate the activation energies and the mechanism of fluid-crystalline phase transitionprocess. This mechanisms follows nucleation and growth model (sigmoidal A4 type an Avrami 3 mechanism). This study permits to obtain a tool to predict the disorder of the structure for hydrophobic or hydrophilic samples that could be used to the release of the drugs.","internal_url":"https://www.academia.edu/113507945/Mechanism_and_Activation_Energies_in_Different_Blends_of_Poly_caprolactone_with_Polyethyleneglycol_PEG_and_Polyvinyl_Alcohol_PVA_","translated_internal_url":"","created_at":"2024-01-14T22:34:39.131-08:00","preview_url":null,"current_user_can_edit":null,"current_user_is_owner":null,"owner_id":45089310,"coauthors_can_edit":true,"document_type":"paper","co_author_tags":[],"downloadable_attachments":[],"slug":"Mechanism_and_Activation_Energies_in_Different_Blends_of_Poly_caprolactone_with_Polyethyleneglycol_PEG_and_Polyvinyl_Alcohol_PVA_","translated_slug":"","page_count":null,"language":"en","content_type":"Work","owner":{"id":45089310,"first_name":"Francisco","middle_initials":null,"last_name":"Fraga López","page_name":"FragaFrancisco","domain_name":"independent","created_at":"2016-03-14T09:17:24.694-07:00","display_name":"Francisco Fraga López","url":"https://independent.academia.edu/FragaFrancisco"},"attachments":[],"research_interests":[{"id":72,"name":"Chemical Engineering","url":"https://www.academia.edu/Documents/in/Chemical_Engineering"},{"id":511,"name":"Materials Science","url":"https://www.academia.edu/Documents/in/Materials_Science"},{"id":2526,"name":"Polymer Chemistry","url":"https://www.academia.edu/Documents/in/Polymer_Chemistry"},{"id":389153,"name":"Polyvinyl alcohol","url":"https://www.academia.edu/Documents/in/Polyvinyl_alcohol"},{"id":1640042,"name":"PEG Ratio","url":"https://www.academia.edu/Documents/in/PEG_Ratio"},{"id":1947619,"name":"Caprolactone","url":"https://www.academia.edu/Documents/in/Caprolactone"}],"urls":[]}, dispatcherData: dispatcherData }); $(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="107215587"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" rel="nofollow" href="https://www.academia.edu/107215587/Innovaci%C3%B3n_y_desarrollo_en_la_industria_alimentaria"><img alt="Research paper thumbnail of Innovación y desarrollo en la industria alimentaria" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" rel="nofollow" href="https://www.academia.edu/107215587/Innovaci%C3%B3n_y_desarrollo_en_la_industria_alimentaria">Innovación y desarrollo en la industria alimentaria</a></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="107215587"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="107215587"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 107215587; 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$(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="107215584"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/107215584/Physical_aging_for_an_epoxy_network_diglycidyl_ether_of_bisphenol_A_m_xylylenediamine"><img alt="Research paper thumbnail of Physical aging for an epoxy network diglycidyl ether of bisphenol A/m-xylylenediamine" class="work-thumbnail" src="https://attachments.academia-assets.com/105948935/thumbnails/1.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/107215584/Physical_aging_for_an_epoxy_network_diglycidyl_ether_of_bisphenol_A_m_xylylenediamine">Physical aging for an epoxy network diglycidyl ether of bisphenol A/m-xylylenediamine</a></div><div class="wp-workCard_item"><span>Polymer</span><span>, 2003</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><a id="250e9969a04afef26351c8dc6458b58d" class="wp-workCard--action" rel="nofollow" data-click-track="profile-work-strip-download" data-download="{"attachment_id":105948935,"asset_id":107215584,"asset_type":"Work","button_location":"profile"}" href="https://www.academia.edu/attachments/105948935/download_file?st=MTczMjUwNjk4Miw4LjIyMi4yMDguMTQ2&s=profile"><span><i class="fa fa-arrow-down"></i></span><span>Download</span></a><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="107215584"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="107215584"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 107215584; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=107215584]").text(description); $(".js-view-count[data-work-id=107215584]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 107215584; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='107215584']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 107215584, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (true){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "250e9969a04afef26351c8dc6458b58d" } } $('.js-work-strip[data-work-id=107215584]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":107215584,"title":"Physical aging for an epoxy network diglycidyl ether of bisphenol A/m-xylylenediamine","translated_title":"","metadata":{"publisher":"Elsevier BV","grobid_abstract":"The physical aging of the epoxy network consisting of a diglycidyl ether of bisphenol A (BADGE n ¼ 0) and m-xylylenediamine (m-XDA) were studied by differential scanning calorimetry. The following aging temperatures have been used in this work: 60, 70, 80, 90, 100 and 110 8C. The glass transition temperature and the variation of the specific heat capacities have been calculated using the method based on the intersection of both enthalpy-temperature lines for glassy and liquid states. The endothermic aging peak, relaxation enthalpy and fictive temperature were also calculated for each aging temperature and aging time.","publication_date":{"day":null,"month":null,"year":2003,"errors":{}},"publication_name":"Polymer","grobid_abstract_attachment_id":105948935},"translated_abstract":null,"internal_url":"https://www.academia.edu/107215584/Physical_aging_for_an_epoxy_network_diglycidyl_ether_of_bisphenol_A_m_xylylenediamine","translated_internal_url":"","created_at":"2023-09-25T20:19:22.114-07:00","preview_url":null,"current_user_can_edit":null,"current_user_is_owner":null,"owner_id":45089310,"coauthors_can_edit":true,"document_type":"paper","co_author_tags":[],"downloadable_attachments":[{"id":105948935,"title":"","file_type":"pdf","scribd_thumbnail_url":"https://attachments.academia-assets.com/105948935/thumbnails/1.jpg","file_name":"s0032-386128032900624-420230926-1-9aekc7.pdf","download_url":"https://www.academia.edu/attachments/105948935/download_file?st=MTczMjUwNjk4Miw4LjIyMi4yMDguMTQ2&","bulk_download_file_name":"Physical_aging_for_an_epoxy_network_digl.pdf","bulk_download_url":"https://d1wqtxts1xzle7.cloudfront.net/105948935/s0032-386128032900624-420230926-1-9aekc7-libre.pdf?1695699454=\u0026response-content-disposition=attachment%3B+filename%3DPhysical_aging_for_an_epoxy_network_digl.pdf\u0026Expires=1732510582\u0026Signature=M5QyzKxMWSCwl5eL0lqpuyThBhd5HQK43ZgoWLyNszmu6pMjp9gLBR~tVUJyAsNp1Buu4tXMkykqARZ2iG9D2cuFAy8Nc8ceHa5cFqNtOD2vLsSp1JduyPRm5ZTnNyAKxBmpx1wcfV0gDfE--0QRsVZLX4~veYT7DJCDcYb2dUp91yIWkRanTBoUrnzw1N3cysR8pEwtNNkzkrdTOqgMh~GO37TCXrsHdCMw7gFbR1zmpsBv3K3fLQENmXsjmTm03UC6E1Qykfcxcz9YVnDaxyPpZg2qDeFEwV~Opeg6n0BDjUW5EQ6hOFsecdD3qXXotXqfpBtm7DqM7Z0RC6rOuA__\u0026Key-Pair-Id=APKAJLOHF5GGSLRBV4ZA"}],"slug":"Physical_aging_for_an_epoxy_network_diglycidyl_ether_of_bisphenol_A_m_xylylenediamine","translated_slug":"","page_count":6,"language":"en","content_type":"Work","owner":{"id":45089310,"first_name":"Francisco","middle_initials":null,"last_name":"Fraga López","page_name":"FragaFrancisco","domain_name":"independent","created_at":"2016-03-14T09:17:24.694-07:00","display_name":"Francisco Fraga López","url":"https://independent.academia.edu/FragaFrancisco"},"attachments":[{"id":105948935,"title":"","file_type":"pdf","scribd_thumbnail_url":"https://attachments.academia-assets.com/105948935/thumbnails/1.jpg","file_name":"s0032-386128032900624-420230926-1-9aekc7.pdf","download_url":"https://www.academia.edu/attachments/105948935/download_file?st=MTczMjUwNjk4Miw4LjIyMi4yMDguMTQ2&","bulk_download_file_name":"Physical_aging_for_an_epoxy_network_digl.pdf","bulk_download_url":"https://d1wqtxts1xzle7.cloudfront.net/105948935/s0032-386128032900624-420230926-1-9aekc7-libre.pdf?1695699454=\u0026response-content-disposition=attachment%3B+filename%3DPhysical_aging_for_an_epoxy_network_digl.pdf\u0026Expires=1732510582\u0026Signature=M5QyzKxMWSCwl5eL0lqpuyThBhd5HQK43ZgoWLyNszmu6pMjp9gLBR~tVUJyAsNp1Buu4tXMkykqARZ2iG9D2cuFAy8Nc8ceHa5cFqNtOD2vLsSp1JduyPRm5ZTnNyAKxBmpx1wcfV0gDfE--0QRsVZLX4~veYT7DJCDcYb2dUp91yIWkRanTBoUrnzw1N3cysR8pEwtNNkzkrdTOqgMh~GO37TCXrsHdCMw7gFbR1zmpsBv3K3fLQENmXsjmTm03UC6E1Qykfcxcz9YVnDaxyPpZg2qDeFEwV~Opeg6n0BDjUW5EQ6hOFsecdD3qXXotXqfpBtm7DqM7Z0RC6rOuA__\u0026Key-Pair-Id=APKAJLOHF5GGSLRBV4ZA"}],"research_interests":[{"id":48,"name":"Engineering","url":"https://www.academia.edu/Documents/in/Engineering"},{"id":511,"name":"Materials Science","url":"https://www.academia.edu/Documents/in/Materials_Science"},{"id":58527,"name":"Polymer","url":"https://www.academia.edu/Documents/in/Polymer"},{"id":78753,"name":"Differential scanning calorimetry","url":"https://www.academia.edu/Documents/in/Differential_scanning_calorimetry"},{"id":82446,"name":"bisphenol A","url":"https://www.academia.edu/Documents/in/bisphenol_A"},{"id":114712,"name":"Enthalpy","url":"https://www.academia.edu/Documents/in/Enthalpy"},{"id":159672,"name":"Epoxy","url":"https://www.academia.edu/Documents/in/Epoxy"},{"id":260118,"name":"CHEMICAL SCIENCES","url":"https://www.academia.edu/Documents/in/CHEMICAL_SCIENCES"},{"id":282351,"name":"Glass Transition","url":"https://www.academia.edu/Documents/in/Glass_Transition"},{"id":335228,"name":"Glass Transition Temperature","url":"https://www.academia.edu/Documents/in/Glass_Transition_Temperature"},{"id":827572,"name":"Specific Heat","url":"https://www.academia.edu/Documents/in/Specific_Heat"}],"urls":[{"id":34074088,"url":"https://api.elsevier.com/content/article/PII:S0032386103006244?httpAccept=text/xml"}]}, dispatcherData: dispatcherData }); $(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="107215582"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/107215582/TTT_cure_diagram_for_an_epoxy_system_diglycidyl_ether_of_bisphenol_A_1_2_diamine_cyclohexane_calcium_carbonate_filler"><img alt="Research paper thumbnail of TTT cure diagram for an epoxy system diglycidyl ether of bisphenol A/1,2 diamine cyclohexane/calcium carbonate filler" class="work-thumbnail" src="https://attachments.academia-assets.com/105948932/thumbnails/1.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/107215582/TTT_cure_diagram_for_an_epoxy_system_diglycidyl_ether_of_bisphenol_A_1_2_diamine_cyclohexane_calcium_carbonate_filler">TTT cure diagram for an epoxy system diglycidyl ether of bisphenol A/1,2 diamine cyclohexane/calcium carbonate filler</a></div><div class="wp-workCard_item"><span>Polymer</span><span>, 2001</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><a id="ef9edf44d0e992699138a40c690b5817" class="wp-workCard--action" rel="nofollow" data-click-track="profile-work-strip-download" data-download="{"attachment_id":105948932,"asset_id":107215582,"asset_type":"Work","button_location":"profile"}" href="https://www.academia.edu/attachments/105948932/download_file?st=MTczMjUwNjk4Miw4LjIyMi4yMDguMTQ2&s=profile"><span><i class="fa fa-arrow-down"></i></span><span>Download</span></a><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="107215582"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="107215582"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 107215582; 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Gel times were measured as a function of temperature using two experimental methods: solubility test and dynamic mechanical analysis (DMA). The results obtained are in fair agreement with that obtained for the two component system BADGE n 0=1; 2 DCH. Vitri®cation times for the three component system was higher than those obtained for the system BADGE n 0=1; 2 DCH and the conversions achieved were very close to maximum values. The activation energy for the overall polymerization reaction was calculated from the gel times obtained using the two above mentioned methods: solubility test (57.12 kJ/mol) and DMA (54.12 kJ/mol). These values are of the same order than those obtained for the two component epoxy system. It was established that the addition of calcium carbonate ®ller avoids the appearance of physical aging, thus making easier both the determination of glass transition temperatures, and the calculation of the TTT diagram.","publication_date":{"day":null,"month":null,"year":2001,"errors":{}},"publication_name":"Polymer","grobid_abstract_attachment_id":105948932},"translated_abstract":null,"internal_url":"https://www.academia.edu/107215582/TTT_cure_diagram_for_an_epoxy_system_diglycidyl_ether_of_bisphenol_A_1_2_diamine_cyclohexane_calcium_carbonate_filler","translated_internal_url":"","created_at":"2023-09-25T20:19:21.816-07:00","preview_url":null,"current_user_can_edit":null,"current_user_is_owner":null,"owner_id":45089310,"coauthors_can_edit":true,"document_type":"paper","co_author_tags":[],"downloadable_attachments":[{"id":105948932,"title":"","file_type":"pdf","scribd_thumbnail_url":"https://attachments.academia-assets.com/105948932/thumbnails/1.jpg","file_name":"s0032-386128002900712-620230926-1-ku9o9q.pdf","download_url":"https://www.academia.edu/attachments/105948932/download_file?st=MTczMjUwNjk4Miw4LjIyMi4yMDguMTQ2&","bulk_download_file_name":"TTT_cure_diagram_for_an_epoxy_system_dig.pdf","bulk_download_url":"https://d1wqtxts1xzle7.cloudfront.net/105948932/s0032-386128002900712-620230926-1-ku9o9q-libre.pdf?1695699455=\u0026response-content-disposition=attachment%3B+filename%3DTTT_cure_diagram_for_an_epoxy_system_dig.pdf\u0026Expires=1732510582\u0026Signature=FIlu~Eveu6j1zHiOPghdzR-D0TGQe~PL3zujzwoSMwY8AmC5jXZi~oNvchG3Lnl1XcKY7uAbuHLLWSPpkRGyV4Q6SWhplSms7qHOabDOp4nYu5wb2tgtqZL6KvxqzYSFD~OV0pSZJl3twAa5P-a2v11du95qeO7eXvAj-jPvGtXsI1816j0LwhZ-QYVNdOpMrPnqGmSOg6eex4VM1SqYUmxzVhQJSGEk8qq5LiCJ6c6TfsD3cR2neaX~b~gyPLCpwbBod6Qu3ygAdjjlHEeQhPV3JBqnlK92k7A-QuwC8Tkvoy1JaHqsPTveSfMJA4V3Ku6YBZnWfbEcrI-vil9VMw__\u0026Key-Pair-Id=APKAJLOHF5GGSLRBV4ZA"}],"slug":"TTT_cure_diagram_for_an_epoxy_system_diglycidyl_ether_of_bisphenol_A_1_2_diamine_cyclohexane_calcium_carbonate_filler","translated_slug":"","page_count":7,"language":"en","content_type":"Work","owner":{"id":45089310,"first_name":"Francisco","middle_initials":null,"last_name":"Fraga López","page_name":"FragaFrancisco","domain_name":"independent","created_at":"2016-03-14T09:17:24.694-07:00","display_name":"Francisco Fraga 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Science","url":"https://www.academia.edu/Documents/in/Materials_Science"},{"id":58527,"name":"Polymer","url":"https://www.academia.edu/Documents/in/Polymer"},{"id":82446,"name":"bisphenol A","url":"https://www.academia.edu/Documents/in/bisphenol_A"},{"id":119665,"name":"Reaction Time","url":"https://www.academia.edu/Documents/in/Reaction_Time"},{"id":147640,"name":"Activation Energy","url":"https://www.academia.edu/Documents/in/Activation_Energy"},{"id":159672,"name":"Epoxy","url":"https://www.academia.edu/Documents/in/Epoxy"},{"id":260118,"name":"CHEMICAL SCIENCES","url":"https://www.academia.edu/Documents/in/CHEMICAL_SCIENCES"},{"id":335228,"name":"Glass Transition Temperature","url":"https://www.academia.edu/Documents/in/Glass_Transition_Temperature"},{"id":630941,"name":"Calcium Carbonate","url":"https://www.academia.edu/Documents/in/Calcium_Carbonate"},{"id":1149150,"name":"Cyclohexane","url":"https://www.academia.edu/Documents/in/Cyclohexane"},{"id":1241878,"name":"Filler Materials","url":"https://www.academia.edu/Documents/in/Filler_Materials"},{"id":1247851,"name":"Experimental Method","url":"https://www.academia.edu/Documents/in/Experimental_Method"},{"id":1431635,"name":"Dynamic Mechanical Analysis","url":"https://www.academia.edu/Documents/in/Dynamic_Mechanical_Analysis"}],"urls":[{"id":34074087,"url":"https://api.elsevier.com/content/article/PII:S0032386100007126?httpAccept=text/xml"}]}, dispatcherData: dispatcherData }); $(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="107215580"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/107215580/Determination_of_physical_and_structural_parameters_by_DMA_and_DSC_application_to_an_epoxidic_formulation"><img alt="Research paper thumbnail of Determination of physical and structural parameters by DMA and DSC application to an epoxidic formulation" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/107215580/Determination_of_physical_and_structural_parameters_by_DMA_and_DSC_application_to_an_epoxidic_formulation">Determination of physical and structural parameters by DMA and DSC application to an epoxidic formulation</a></div><div class="wp-workCard_item"><span>Journal of Thermal Analysis</span><span>, 1994</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper 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epoxy/cure agent reaction" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/107215577/Activation_energies_and_rate_constants_for_an_epoxy_cure_agent_reaction">Activation energies and rate constants for an epoxy/cure agent reaction</a></div><div class="wp-workCard_item"><span>Journal of Thermal Analysis</span><span>, 1996</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">ABSTRACT From the peak reaction temperatures as a function of heating rate, the activation energi...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">ABSTRACT From the peak reaction temperatures as a function of heating rate, the activation energies were obtained for a system consisting of an epoxy resin (Badgen=0) and a curing agent (isophorone diamine), using a Perkin Elmer DSC7 operated in the dynamic mode. At the same time, the Arrhenius law was used to calculate rate constants.</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="107215577"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="107215577"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 107215577; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=107215577]").text(description); $(".js-view-count[data-work-id=107215577]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 107215577; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='107215577']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 107215577, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=107215577]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":107215577,"title":"Activation energies and rate constants for an epoxy/cure agent reaction","translated_title":"","metadata":{"abstract":"ABSTRACT From the peak reaction temperatures as a function of heating rate, the activation energies were obtained for a system consisting of an epoxy resin (Badgen=0) and a curing agent (isophorone diamine), using a Perkin Elmer DSC7 operated in the dynamic mode. 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$(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="106527451"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/106527451/Cure_kinetic_of_the_epoxy_network_diglycidyl_ether_of_bisphenol_A_BADGE_n_0_amantidine"><img alt="Research paper thumbnail of Cure kinetic of the epoxy network diglycidyl ether of bisphenol A (BADGE n=0)/amantidine" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/106527451/Cure_kinetic_of_the_epoxy_network_diglycidyl_ether_of_bisphenol_A_BADGE_n_0_amantidine">Cure kinetic of the epoxy network diglycidyl ether of bisphenol A (BADGE n=0)/amantidine</a></div><div class="wp-workCard_item"><span>Journal of Thermal Analysis and Calorimetry</span><span>, 2007</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="106527451"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="106527451"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 106527451; 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$(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="106527450"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/106527450/Effects_of_diffusion_on_the_kinetic_study_of_the_system_BADGE_n_0_m_xylylenediamine"><img alt="Research paper thumbnail of Effects of diffusion on the kinetic study of the system BADGE n = 0/m-xylylenediamine" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/106527450/Effects_of_diffusion_on_the_kinetic_study_of_the_system_BADGE_n_0_m_xylylenediamine">Effects of diffusion on the kinetic study of the system BADGE n = 0/m-xylylenediamine</a></div><div class="wp-workCard_item"><span>Journal of Applied Polymer Science</span><span>, 1999</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">ABSTRACT The curing reactions of an epoxy system composed of a diglycidyl ether of bisphenol A (B...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">ABSTRACT The curing reactions of an epoxy system composed of a diglycidyl ether of bisphenol A (BADGE n=0) and m-xylylenediamine (m-XDA) were studied. Two models, the first based solely on chemical kinetics and the second accounting for diffusion, were used and compared to the experimental data. The epoxy resin was used as received in a first series of experiments. In a second series of experiments, the resin was purified in vacuo (180°C and 1 mmHg). The inclusion of a diffusion factor in the second model allowed for the cure kinetics to be predicted over the whole range of conversion covering both pre- and postvitrification stages. The investigation was made in the temperature range 50–110°C, which is considered optimum for the isothermal curing of the epoxy system studied. © 1999 John Wiley &amp;amp;amp; Sons, Inc. J Appl Polym Sci 74: 2997–3005, 1999</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="106527450"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="106527450"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 106527450; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=106527450]").text(description); $(".js-view-count[data-work-id=106527450]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 106527450; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='106527450']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 106527450, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=106527450]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":106527450,"title":"Effects of diffusion on the kinetic study of the system BADGE n = 0/m-xylylenediamine","translated_title":"","metadata":{"abstract":"ABSTRACT The curing reactions of an epoxy system composed of a diglycidyl ether of bisphenol A (BADGE n=0) and m-xylylenediamine (m-XDA) were studied. Two models, the first based solely on chemical kinetics and the second accounting for diffusion, were used and compared to the experimental data. The epoxy resin was used as received in a first series of experiments. In a second series of experiments, the resin was purified in vacuo (180°C and 1 mmHg). The inclusion of a diffusion factor in the second model allowed for the cure kinetics to be predicted over the whole range of conversion covering both pre- and postvitrification stages. The investigation was made in the temperature range 50–110°C, which is considered optimum for the isothermal curing of the epoxy system studied. © 1999 John Wiley \u0026amp;amp;amp; Sons, Inc. J Appl Polym Sci 74: 2997–3005, 1999","publisher":"Wiley-Blackwell","publication_date":{"day":null,"month":null,"year":1999,"errors":{}},"publication_name":"Journal of Applied Polymer Science"},"translated_abstract":"ABSTRACT The curing reactions of an epoxy system composed of a diglycidyl ether of bisphenol A (BADGE n=0) and m-xylylenediamine (m-XDA) were studied. Two models, the first based solely on chemical kinetics and the second accounting for diffusion, were used and compared to the experimental data. The epoxy resin was used as received in a first series of experiments. In a second series of experiments, the resin was purified in vacuo (180°C and 1 mmHg). The inclusion of a diffusion factor in the second model allowed for the cure kinetics to be predicted over the whole range of conversion covering both pre- and postvitrification stages. The investigation was made in the temperature range 50–110°C, which is considered optimum for the isothermal curing of the epoxy system studied. © 1999 John Wiley \u0026amp;amp;amp; Sons, Inc. J Appl Polym Sci 74: 2997–3005, 1999","internal_url":"https://www.academia.edu/106527450/Effects_of_diffusion_on_the_kinetic_study_of_the_system_BADGE_n_0_m_xylylenediamine","translated_internal_url":"","created_at":"2023-09-12T12:04:38.868-07:00","preview_url":null,"current_user_can_edit":null,"current_user_is_owner":null,"owner_id":45089310,"coauthors_can_edit":true,"document_type":"paper","co_author_tags":[],"downloadable_attachments":[],"slug":"Effects_of_diffusion_on_the_kinetic_study_of_the_system_BADGE_n_0_m_xylylenediamine","translated_slug":"","page_count":null,"language":"en","content_type":"Work","owner":{"id":45089310,"first_name":"Francisco","middle_initials":null,"last_name":"Fraga López","page_name":"FragaFrancisco","domain_name":"independent","created_at":"2016-03-14T09:17:24.694-07:00","display_name":"Francisco Fraga López","url":"https://independent.academia.edu/FragaFrancisco"},"attachments":[],"research_interests":[{"id":48,"name":"Engineering","url":"https://www.academia.edu/Documents/in/Engineering"},{"id":511,"name":"Materials Science","url":"https://www.academia.edu/Documents/in/Materials_Science"},{"id":2526,"name":"Polymer Chemistry","url":"https://www.academia.edu/Documents/in/Polymer_Chemistry"},{"id":4987,"name":"Kinetics","url":"https://www.academia.edu/Documents/in/Kinetics"},{"id":82446,"name":"bisphenol A","url":"https://www.academia.edu/Documents/in/bisphenol_A"},{"id":83315,"name":"Diffusion","url":"https://www.academia.edu/Documents/in/Diffusion"},{"id":159672,"name":"Epoxy","url":"https://www.academia.edu/Documents/in/Epoxy"},{"id":260118,"name":"CHEMICAL SCIENCES","url":"https://www.academia.edu/Documents/in/CHEMICAL_SCIENCES"},{"id":413295,"name":"Kinetic Energy","url":"https://www.academia.edu/Documents/in/Kinetic_Energy"},{"id":966213,"name":"Journal of Applied Polymer Science","url":"https://www.academia.edu/Documents/in/Journal_of_Applied_Polymer_Science"}],"urls":[]}, dispatcherData: dispatcherData }); $(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> </div><div class="profile--tab_content_container js-tab-pane tab-pane" data-section-id="12930926" id="papers"><div class="js-work-strip profile--work_container" data-work-id="117179532"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/117179532/Effect_of_Gold_Nanoparticles_on_the_Physical_Properties_of_an_Epoxy_Resin"><img alt="Research paper thumbnail of Effect of Gold Nanoparticles on the Physical Properties of an Epoxy Resin" class="work-thumbnail" src="https://attachments.academia-assets.com/113104770/thumbnails/1.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/117179532/Effect_of_Gold_Nanoparticles_on_the_Physical_Properties_of_an_Epoxy_Resin">Effect of Gold Nanoparticles on the Physical Properties of an Epoxy Resin</a></div><div class="wp-workCard_item"><span>International Journal of Molecular Sciences</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">The effect of doping the bisphenol A diglycidyl ether (DGEBA)/m-xylylenediamine (mXDA) system wit...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">The effect of doping the bisphenol A diglycidyl ether (DGEBA)/m-xylylenediamine (mXDA) system with gold nanoparticles (AuNP) has been studied with differential scanning calorimetry (DSC), thermogravimetric analysis, dynamic mechanical analysis (DMA), and dielectric analysis (DEA). The evolved heat (ΔHt), the glass transition temperature (Tg), and the associated activation energies of this relaxation process have been determined. Below a certain concentration of AuNPs (=8.5%, in mg AuNP/g epoxy matrix), Tg decreases linearly with the concentration of AuNPs, but above it, Tg is not affected. The degree of conversion α of this epoxy system was analyzed by the semiempirical Kamal’s model, evidencing that diffusion correction is required at high values of α. Activation energy values suggest that AuNPs can cause some impediments at the beginning of the crosslinking process (n-order mechanism). The slight difference between the initial decomposition temperature, as well as the temperature ...</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><a id="b5a9f691d2b089877f43163beb01840e" class="wp-workCard--action" rel="nofollow" data-click-track="profile-work-strip-download" data-download="{"attachment_id":113104770,"asset_id":117179532,"asset_type":"Work","button_location":"profile"}" href="https://www.academia.edu/attachments/113104770/download_file?st=MTczMjUwNjk4Myw4LjIyMi4yMDguMTQ2&st=MTczMjUwNjk4Miw4LjIyMi4yMDguMTQ2&s=profile"><span><i class="fa fa-arrow-down"></i></span><span>Download</span></a><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="117179532"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="117179532"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 117179532; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=117179532]").text(description); $(".js-view-count[data-work-id=117179532]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 117179532; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='117179532']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 117179532, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (true){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "b5a9f691d2b089877f43163beb01840e" } } $('.js-work-strip[data-work-id=117179532]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":117179532,"title":"Effect of Gold Nanoparticles on the Physical Properties of an Epoxy Resin","translated_title":"","metadata":{"abstract":"The effect of doping the bisphenol A diglycidyl ether (DGEBA)/m-xylylenediamine (mXDA) system with gold nanoparticles (AuNP) has been studied with differential scanning calorimetry (DSC), thermogravimetric analysis, dynamic mechanical analysis (DMA), and dielectric analysis (DEA). The evolved heat (ΔHt), the glass transition temperature (Tg), and the associated activation energies of this relaxation process have been determined. Below a certain concentration of AuNPs (=8.5%, in mg AuNP/g epoxy matrix), Tg decreases linearly with the concentration of AuNPs, but above it, Tg is not affected. The degree of conversion α of this epoxy system was analyzed by the semiempirical Kamal’s model, evidencing that diffusion correction is required at high values of α. Activation energy values suggest that AuNPs can cause some impediments at the beginning of the crosslinking process (n-order mechanism). The slight difference between the initial decomposition temperature, as well as the temperature ...","publisher":"MDPI AG","publication_name":"International Journal of Molecular Sciences"},"translated_abstract":"The effect of doping the bisphenol A diglycidyl ether (DGEBA)/m-xylylenediamine (mXDA) system with gold nanoparticles (AuNP) has been studied with differential scanning calorimetry (DSC), thermogravimetric analysis, dynamic mechanical analysis (DMA), and dielectric analysis (DEA). The evolved heat (ΔHt), the glass transition temperature (Tg), and the associated activation energies of this relaxation process have been determined. Below a certain concentration of AuNPs (=8.5%, in mg AuNP/g epoxy matrix), Tg decreases linearly with the concentration of AuNPs, but above it, Tg is not affected. The degree of conversion α of this epoxy system was analyzed by the semiempirical Kamal’s model, evidencing that diffusion correction is required at high values of α. Activation energy values suggest that AuNPs can cause some impediments at the beginning of the crosslinking process (n-order mechanism). The slight difference between the initial decomposition temperature, as well as the temperature 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data-click-track="profile-work-strip-title" href="https://www.academia.edu/117179531/Simple_route_for_nano_hydroxyapatite_properties_expansion">Simple route for nano-hydroxyapatite properties expansion</a></div><div class="wp-workCard_item"><span>Biomedical Materials</span><span>, 2015</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">Simple surface modification of nano-hydroxyapatite, through acid-basic reactions, allows expandin...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">Simple surface modification of nano-hydroxyapatite, through acid-basic reactions, allows expanding the properties of this material. Introduction of organic groups such as hydrophobic alkyl chains, carboxylic acid, and amide or amine basic groups on the hydroxyapatite surface systematically change the polarity, surface area, and reactivity of hydroxyapatite without modifying its phase. Physical and chemical properties of the new derivative particles were analyzed. The biocompatibility of modified Nano-Hap on Raw 264.7 cells was also assessed.</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="117179531"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="117179531"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 117179531; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=117179531]").text(description); $(".js-view-count[data-work-id=117179531]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 117179531; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='117179531']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 117179531, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=117179531]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":117179531,"title":"Simple route for nano-hydroxyapatite properties expansion","translated_title":"","metadata":{"abstract":"Simple surface modification of nano-hydroxyapatite, through acid-basic reactions, allows expanding the properties of this material. Introduction of organic groups such as hydrophobic alkyl chains, carboxylic acid, and amide or amine basic groups on the hydroxyapatite surface systematically change the polarity, surface area, and reactivity of hydroxyapatite without modifying its phase. Physical and chemical properties of the new derivative particles were analyzed. The biocompatibility of modified Nano-Hap on Raw 264.7 cells was also assessed.","publisher":"IOP Publishing","publication_date":{"day":null,"month":null,"year":2015,"errors":{}},"publication_name":"Biomedical Materials"},"translated_abstract":"Simple surface modification of nano-hydroxyapatite, through acid-basic reactions, allows expanding the properties of this material. Introduction of organic groups such as hydrophobic alkyl chains, carboxylic acid, and amide or amine basic groups on the hydroxyapatite surface systematically change the polarity, surface area, and reactivity of hydroxyapatite without modifying its phase. Physical and chemical properties of the new derivative particles were analyzed. 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an epoxy network as determined with a peak shift model" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/117179528/Kinetics_of_the_enthalpy_relaxation_process_for_an_epoxy_network_as_determined_with_a_peak_shift_model">Kinetics of the enthalpy relaxation process for an epoxy network as determined with a peak shift model</a></div><div class="wp-workCard_item"><span>Journal of Applied Polymer Science</span><span>, 2005</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">... 7 Fraga, F.; Castro-Díaz, C.; Rodríguez-Núñez, E.; Martínez-Ageitos, JM J Appl Polym Sci, to ...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" 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class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/117179526/Influence_of_water_absorption_on_the_mechanical_properties_of_a_DGEBA_n_0_1_2_DCH_epoxy_system">Influence of water absorption on the mechanical properties of a DGEBA (n = 0)/1, 2 DCH epoxy system</a></div><div class="wp-workCard_item"><span>Journal of Applied Polymer Science</span><span>, 1999</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">... Lisardo Núñez,; M. Villanueva,; F. Fraga,; MR Núñez. Article first published online: 28 JUL 1...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">... Lisardo Núñez,; M. Villanueva,; F. Fraga,; MR Núñez. Article first published online: 28 JUL 1999. DOI: 10.1002/(SICI)1097-4628(19991010)74:2&lt;353::AID-APP17&gt;3.0.CO;2-J. Copyright © 1999John Wiley &amp; Sons, Inc. Issue. Journal of Applied Polymer Science. ...</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="117179526"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="117179526"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 117179526; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=117179526]").text(description); $(".js-view-count[data-work-id=117179526]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 117179526; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='117179526']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 117179526, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=117179526]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":117179526,"title":"Influence of water absorption on the mechanical properties of a DGEBA (n = 0)/1, 2 DCH epoxy system","translated_title":"","metadata":{"abstract":"... 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The influence of the crosslinking times on the calorimetric parameters (glass transition temperatures, enthalpy, and endothermic peak) of the system clorhydrate of chitosan/glutaraldehyde (1,5‐pentanedial) was studied using differential scanning calorimetry in dynamic mode. Using Kissinger′s method, the activation energies for the water remaining process were obtained without a precise knowledge of the reaction mechanism from the experimental endothermic peaks. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 100: 3297–3301, 2006</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="117179516"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="117179516"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 117179516; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=117179516]").text(description); $(".js-view-count[data-work-id=117179516]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 117179516; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='117179516']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 117179516, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=117179516]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":117179516,"title":"Calorimetric study of the system clorhydrate of chitosan/glutaraldehyde(1,5‐pentanedial)","translated_title":"","metadata":{"abstract":"The reaction of glutaraldehyde with primary amino groups of chitosan produces covalent crosslinking in a matricial microsphere formulation. The influence of the crosslinking times on the calorimetric parameters (glass transition temperatures, enthalpy, and endothermic peak) of the system clorhydrate of chitosan/glutaraldehyde (1,5‐pentanedial) was studied using differential scanning calorimetry in dynamic mode. Using Kissinger′s method, the activation energies for the water remaining process were obtained without a precise knowledge of the reaction mechanism from the experimental endothermic peaks. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 100: 3297–3301, 2006","publisher":"Wiley","publication_date":{"day":null,"month":null,"year":2006,"errors":{}},"publication_name":"Journal of Applied Polymer Science"},"translated_abstract":"The reaction of glutaraldehyde with primary amino groups of chitosan produces covalent crosslinking in a matricial microsphere formulation. The influence of the crosslinking times on the calorimetric parameters (glass transition temperatures, enthalpy, and endothermic peak) of the system clorhydrate of chitosan/glutaraldehyde (1,5‐pentanedial) was studied using differential scanning calorimetry in dynamic mode. Using Kissinger′s method, the activation energies for the water remaining process were obtained without a precise knowledge of the reaction mechanism from the experimental endothermic peaks. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 100: 3297–3301, 2006","internal_url":"https://www.academia.edu/117179516/Calorimetric_study_of_the_system_clorhydrate_of_chitosan_glutaraldehyde_1_5_pentanedial_","translated_internal_url":"","created_at":"2024-04-07T05:00:40.907-07:00","preview_url":null,"current_user_can_edit":null,"current_user_is_owner":null,"owner_id":45089310,"coauthors_can_edit":true,"document_type":"paper","co_author_tags":[],"downloadable_attachments":[],"slug":"Calorimetric_study_of_the_system_clorhydrate_of_chitosan_glutaraldehyde_1_5_pentanedial_","translated_slug":"","page_count":null,"language":"en","content_type":"Work","owner":{"id":45089310,"first_name":"Francisco","middle_initials":null,"last_name":"Fraga López","page_name":"FragaFrancisco","domain_name":"independent","created_at":"2016-03-14T09:17:24.694-07:00","display_name":"Francisco Fraga López","url":"https://independent.academia.edu/FragaFrancisco"},"attachments":[],"research_interests":[{"id":48,"name":"Engineering","url":"https://www.academia.edu/Documents/in/Engineering"},{"id":523,"name":"Chemistry","url":"https://www.academia.edu/Documents/in/Chemistry"},{"id":9130,"name":"Chitosan","url":"https://www.academia.edu/Documents/in/Chitosan"},{"id":260118,"name":"CHEMICAL SCIENCES","url":"https://www.academia.edu/Documents/in/CHEMICAL_SCIENCES"},{"id":966213,"name":"Journal of Applied Polymer Science","url":"https://www.academia.edu/Documents/in/Journal_of_Applied_Polymer_Science"},{"id":2687106,"name":"glutaraldehyde","url":"https://www.academia.edu/Documents/in/glutaraldehyde"}],"urls":[{"id":40908077,"url":"https://onlinelibrary.wiley.com/doi/pdf/10.1002/app.23150"}]}, dispatcherData: dispatcherData }); $(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="113507964"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/113507964/Determination_of_the_optimum_epoxy_curing_agent_ratio_A_study_of_different_kinetic_parameters"><img alt="Research paper thumbnail of Determination of the optimum epoxy/curing agent ratio: A study of different kinetic parameters" class="work-thumbnail" src="https://attachments.academia-assets.com/110449283/thumbnails/1.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/113507964/Determination_of_the_optimum_epoxy_curing_agent_ratio_A_study_of_different_kinetic_parameters">Determination of the optimum epoxy/curing agent ratio: A study of different kinetic parameters</a></div><div class="wp-workCard_item"><span>Pure and Applied Chemistry</span><span>, 1995</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><a id="65275047ec1cce08a1b0f7a482cccb34" class="wp-workCard--action" rel="nofollow" data-click-track="profile-work-strip-download" data-download="{"attachment_id":110449283,"asset_id":113507964,"asset_type":"Work","button_location":"profile"}" href="https://www.academia.edu/attachments/110449283/download_file?st=MTczMjUwNjk4Myw4LjIyMi4yMDguMTQ2&st=MTczMjUwNjk4Miw4LjIyMi4yMDguMTQ2&s=profile"><span><i class="fa fa-arrow-down"></i></span><span>Download</span></a><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="113507964"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="113507964"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 113507964; 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Determination of the optimum value of the epoxy/curing agent ratio was studied by means of differential scanning calorimetry. The method is based on the search for the maximum enthalpy change'. It was found that this maximum corresponds to a 100/34 value. The glass transition temperature (Tg) has been calculated using dynamic methods. Our values are in good agreement with those in the l i t e r a t~r e~3~ for similar systems. At the same time other kinetic parameters were obtained using an isothermal method and the ratio values previously calculated. 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analysis and thermogravimetry-fourier transform infrared spectroscopy" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/113507963/The_influence_of_lixiviates_on_the_thermal_degradation_of_diglycidyl_ether_of_bisphenol_An_0_1_2_diaminecyclohexane_studied_by_dynamic_mechanical_analysis_and_thermogravimetry_fourier_transform_infrared_spectroscopy">The influence of lixiviates on the thermal degradation of diglycidyl ether of bisphenol An=0/1,2-diaminecyclohexane studied by dynamic mechanical analysis and thermogravimetry-fourier transform infrared spectroscopy</a></div><div class="wp-workCard_item"><span>Journal of Applied Polymer Science</span><span>, 1999</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">ABSTRACT The influence of the lixiviates originated in a municipal landfill on the thermal degrad...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">ABSTRACT The influence of the lixiviates originated in a municipal landfill on the thermal degradation of a polymeric system composed of a diglycidyl ether of bisphenol A (n = 0) and 1,2-diaminecyclohexane was studied by dynamic mechanical analysis. Storage modulus (E′), loss modulus (E″), and glass transition temperature were measured to make a comparative study between the samples before and after being exposed to the chemical compounds in the lixiviate agents. The different data obtained were analyzed to check the resistance of these materials to chemical attack and the possibility of their use as coating materials in plants where those reagents were present. Thermal stability of the system diglycidyl ether of bisphenol A/1,2-diaminecyclohexane exposed to the attack of lixiviates has also been studied by thermogravimetric analysis. A quantitative study of the gases originated during thermal degradation of the epoxy/diamine system made by infrared spectroscopy. © 1999 John Wiley &amp;amp;amp; Sons, Inc. J Appl Polym Sci 72: 443–453, 1999</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="113507963"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="113507963"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 113507963; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=113507963]").text(description); $(".js-view-count[data-work-id=113507963]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 113507963; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='113507963']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 113507963, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=113507963]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":113507963,"title":"The influence of lixiviates on the thermal degradation of diglycidyl ether of bisphenol An=0/1,2-diaminecyclohexane studied by dynamic mechanical analysis and thermogravimetry-fourier transform infrared spectroscopy","translated_title":"","metadata":{"abstract":"ABSTRACT The influence of the lixiviates originated in a municipal landfill on the thermal degradation of a polymeric system composed of a diglycidyl ether of bisphenol A (n = 0) and 1,2-diaminecyclohexane was studied by dynamic mechanical analysis. Storage modulus (E′), loss modulus (E″), and glass transition temperature were measured to make a comparative study between the samples before and after being exposed to the chemical compounds in the lixiviate agents. The different data obtained were analyzed to check the resistance of these materials to chemical attack and the possibility of their use as coating materials in plants where those reagents were present. Thermal stability of the system diglycidyl ether of bisphenol A/1,2-diaminecyclohexane exposed to the attack of lixiviates has also been studied by thermogravimetric analysis. A quantitative study of the gases originated during thermal degradation of the epoxy/diamine system made by infrared spectroscopy. © 1999 John Wiley \u0026amp;amp;amp; Sons, Inc. J Appl Polym Sci 72: 443–453, 1999","publisher":"Wiley","publication_date":{"day":null,"month":null,"year":1999,"errors":{}},"publication_name":"Journal of Applied Polymer Science"},"translated_abstract":"ABSTRACT The influence of the lixiviates originated in a municipal landfill on the thermal degradation of a polymeric system composed of a diglycidyl ether of bisphenol A (n = 0) and 1,2-diaminecyclohexane was studied by dynamic mechanical analysis. Storage modulus (E′), loss modulus (E″), and glass transition temperature were measured to make a comparative study between the samples before and after being exposed to the chemical compounds in the lixiviate agents. The different data obtained were analyzed to check the resistance of these materials to chemical attack and the possibility of their use as coating materials in plants where those reagents were present. Thermal stability of the system diglycidyl ether of bisphenol A/1,2-diaminecyclohexane exposed to the attack of lixiviates has also been studied by thermogravimetric analysis. A quantitative study of the gases originated during thermal degradation of the epoxy/diamine system made by infrared spectroscopy. © 1999 John Wiley \u0026amp;amp;amp; Sons, Inc. J Appl Polym Sci 72: 443–453, 1999","internal_url":"https://www.academia.edu/113507963/The_influence_of_lixiviates_on_the_thermal_degradation_of_diglycidyl_ether_of_bisphenol_An_0_1_2_diaminecyclohexane_studied_by_dynamic_mechanical_analysis_and_thermogravimetry_fourier_transform_infrared_spectroscopy","translated_internal_url":"","created_at":"2024-01-14T22:35:13.722-08:00","preview_url":null,"current_user_can_edit":null,"current_user_is_owner":null,"owner_id":45089310,"coauthors_can_edit":true,"document_type":"paper","co_author_tags":[],"downloadable_attachments":[],"slug":"The_influence_of_lixiviates_on_the_thermal_degradation_of_diglycidyl_ether_of_bisphenol_An_0_1_2_diaminecyclohexane_studied_by_dynamic_mechanical_analysis_and_thermogravimetry_fourier_transform_infrared_spectroscopy","translated_slug":"","page_count":null,"language":"en","content_type":"Work","owner":{"id":45089310,"first_name":"Francisco","middle_initials":null,"last_name":"Fraga López","page_name":"FragaFrancisco","domain_name":"independent","created_at":"2016-03-14T09:17:24.694-07:00","display_name":"Francisco Fraga López","url":"https://independent.academia.edu/FragaFrancisco"},"attachments":[],"research_interests":[{"id":48,"name":"Engineering","url":"https://www.academia.edu/Documents/in/Engineering"},{"id":511,"name":"Materials Science","url":"https://www.academia.edu/Documents/in/Materials_Science"},{"id":523,"name":"Chemistry","url":"https://www.academia.edu/Documents/in/Chemistry"},{"id":82446,"name":"bisphenol A","url":"https://www.academia.edu/Documents/in/bisphenol_A"},{"id":159672,"name":"Epoxy","url":"https://www.academia.edu/Documents/in/Epoxy"},{"id":246949,"name":"Thermogravimetry","url":"https://www.academia.edu/Documents/in/Thermogravimetry"},{"id":260118,"name":"CHEMICAL SCIENCES","url":"https://www.academia.edu/Documents/in/CHEMICAL_SCIENCES"},{"id":282351,"name":"Glass Transition","url":"https://www.academia.edu/Documents/in/Glass_Transition"},{"id":389180,"name":"Thermal Stability","url":"https://www.academia.edu/Documents/in/Thermal_Stability"},{"id":398650,"name":"Fourier transform infrared spectroscopy","url":"https://www.academia.edu/Documents/in/Fourier_transform_infrared_spectroscopy"},{"id":398652,"name":"Thermogravimetric Analysis","url":"https://www.academia.edu/Documents/in/Thermogravimetric_Analysis"},{"id":966213,"name":"Journal of Applied Polymer Science","url":"https://www.academia.edu/Documents/in/Journal_of_Applied_Polymer_Science"},{"id":1431635,"name":"Dynamic Mechanical Analysis","url":"https://www.academia.edu/Documents/in/Dynamic_Mechanical_Analysis"}],"urls":[{"id":38576614,"url":"https://api.wiley.com/onlinelibrary/tdm/v1/articles/10.1002%2F(SICI)1097-4628(19990418)72:3%3C443::AID-APP14%3E3.0.CO;2-X"}]}, dispatcherData: dispatcherData }); $(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="113507962"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/113507962/Kinetic_study_and_time_temperature_transformation_cure_diagram_for_an_epoxy_diamine_system"><img alt="Research paper thumbnail of Kinetic study and time‐temperature‐transformation cure diagram for an epoxy‐diamine system" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/113507962/Kinetic_study_and_time_temperature_transformation_cure_diagram_for_an_epoxy_diamine_system">Kinetic study and time‐temperature‐transformation cure diagram for an epoxy‐diamine system</a></div><div class="wp-workCard_item"><span>Journal of Applied Polymer Science</span><span>, 1997</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">... Lisardo Núñez,; J. Taboada,; F. Fraga,; MR Núñez. Article first published online: 7 DEC 1998....</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">... Lisardo Núñez,; J. Taboada,; F. Fraga,; MR Núñez. Article first published online: 7 DEC 1998. DOI: 10.1002/(SICI)1097-4628(19971114)66:7&lt;1377::AID-APP16&gt;3.0.CO;2-#. Copyright © 1997John Wiley &amp; Sons, Inc. Issue. Journal of Applied Polymer Science. ...</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="113507962"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="113507962"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 113507962; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=113507962]").text(description); $(".js-view-count[data-work-id=113507962]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 113507962; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='113507962']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 113507962, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=113507962]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":113507962,"title":"Kinetic study and time‐temperature‐transformation cure diagram for an epoxy‐diamine system","translated_title":"","metadata":{"abstract":"... Lisardo Núñez,; J. Taboada,; F. Fraga,; MR Núñez. Article first published online: 7 DEC 1998. DOI: 10.1002/(SICI)1097-4628(19971114)66:7\u0026lt;1377::AID-APP16\u0026gt;3.0.CO;2-#. Copyright © 1997John Wiley \u0026amp; Sons, Inc. Issue. Journal of Applied Polymer Science. ...","publisher":"Wiley","publication_date":{"day":null,"month":null,"year":1997,"errors":{}},"publication_name":"Journal of Applied Polymer Science"},"translated_abstract":"... Lisardo Núñez,; J. Taboada,; F. Fraga,; MR Núñez. Article first published online: 7 DEC 1998. DOI: 10.1002/(SICI)1097-4628(19971114)66:7\u0026lt;1377::AID-APP16\u0026gt;3.0.CO;2-#. Copyright © 1997John Wiley \u0026amp; Sons, Inc. Issue. Journal of Applied Polymer Science. ...","internal_url":"https://www.academia.edu/113507962/Kinetic_study_and_time_temperature_transformation_cure_diagram_for_an_epoxy_diamine_system","translated_internal_url":"","created_at":"2024-01-14T22:35:13.524-08:00","preview_url":null,"current_user_can_edit":null,"current_user_is_owner":null,"owner_id":45089310,"coauthors_can_edit":true,"document_type":"paper","co_author_tags":[],"downloadable_attachments":[],"slug":"Kinetic_study_and_time_temperature_transformation_cure_diagram_for_an_epoxy_diamine_system","translated_slug":"","page_count":null,"language":"en","content_type":"Work","owner":{"id":45089310,"first_name":"Francisco","middle_initials":null,"last_name":"Fraga López","page_name":"FragaFrancisco","domain_name":"independent","created_at":"2016-03-14T09:17:24.694-07:00","display_name":"Francisco Fraga López","url":"https://independent.academia.edu/FragaFrancisco"},"attachments":[],"research_interests":[{"id":48,"name":"Engineering","url":"https://www.academia.edu/Documents/in/Engineering"},{"id":511,"name":"Materials Science","url":"https://www.academia.edu/Documents/in/Materials_Science"},{"id":523,"name":"Chemistry","url":"https://www.academia.edu/Documents/in/Chemistry"},{"id":4987,"name":"Kinetics","url":"https://www.academia.edu/Documents/in/Kinetics"},{"id":96502,"name":"Applied","url":"https://www.academia.edu/Documents/in/Applied"},{"id":159672,"name":"Epoxy","url":"https://www.academia.edu/Documents/in/Epoxy"},{"id":199746,"name":"Diagram","url":"https://www.academia.edu/Documents/in/Diagram"},{"id":260118,"name":"CHEMICAL SCIENCES","url":"https://www.academia.edu/Documents/in/CHEMICAL_SCIENCES"},{"id":413295,"name":"Kinetic Energy","url":"https://www.academia.edu/Documents/in/Kinetic_Energy"},{"id":966213,"name":"Journal of Applied Polymer Science","url":"https://www.academia.edu/Documents/in/Journal_of_Applied_Polymer_Science"}],"urls":[{"id":38576613,"url":"https://onlinelibrary.wiley.com/doi/pdf/10.1002/(SICI)1097-4628(19971114)66:7%3C1377::AID-APP16%3E3.0.CO;2-%23"}]}, dispatcherData: dispatcherData }); $(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="113507961"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/113507961/Curing_kinetic_of_the_epoxy_system_badge_n_0_1_2_DCH_by_fourier_transform_infrared_spectroscopy_FTIR_"><img alt="Research paper thumbnail of Curing kinetic of the epoxy system badge n = 0/1,2 DCH by fourier transform infrared spectroscopy (FTIR)" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/113507961/Curing_kinetic_of_the_epoxy_system_badge_n_0_1_2_DCH_by_fourier_transform_infrared_spectroscopy_FTIR_">Curing kinetic of the epoxy system badge n = 0/1,2 DCH by fourier transform infrared spectroscopy (FTIR)</a></div><div class="wp-workCard_item"><span>Journal of Applied Polymer Science</span><span>, 2001</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">The curing reaction of an epoxy system consisting of a diglycidyl ether of bisphenol A (BADGE n =...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">The curing reaction of an epoxy system consisting of a diglycidyl ether of bisphenol A (BADGE n = 0) and 1,2‐diaminocyclohexane (DCH) was studied by Fourier Trasform Infrared Spectroscopy (FTIR). From the infrared spectra using a peak‐height method, that was based on the ratio of the height of the characteristic to reference absorbance peak, degree of conversion at different isothermal temperatures were calculated. From a kinetic study, the Horie et al. model was used; parameters such as rate constants and activation energies were determined. The results were compared to those obtained for same epoxy systems using scanning differential calorimetry (DSC). © 2001 John Wiley & Sons, Inc. J Appl Polym Sci 82: 3366–3372, 2001</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="113507961"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="113507961"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 113507961; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=113507961]").text(description); $(".js-view-count[data-work-id=113507961]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 113507961; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='113507961']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 113507961, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=113507961]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":113507961,"title":"Curing kinetic of the epoxy system badge n = 0/1,2 DCH by fourier transform infrared spectroscopy (FTIR)","translated_title":"","metadata":{"abstract":"The curing reaction of an epoxy system consisting of a diglycidyl ether of bisphenol A (BADGE n = 0) and 1,2‐diaminocyclohexane (DCH) was studied by Fourier Trasform Infrared Spectroscopy (FTIR). 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The correlation of activation energies obtained using Kissinger and Flynn–Wall–Ozawa integral methods were lower than 0.99, so it was necessary used the Coats–Redfern Method to determinate the activation energies and the mechanism of fluid-crystalline phase transitionprocess. This mechanisms follows nucleation and growth model (sigmoidal A4 type an Avrami 3 mechanism). 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$(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="107215584"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/107215584/Physical_aging_for_an_epoxy_network_diglycidyl_ether_of_bisphenol_A_m_xylylenediamine"><img alt="Research paper thumbnail of Physical aging for an epoxy network diglycidyl ether of bisphenol A/m-xylylenediamine" class="work-thumbnail" src="https://attachments.academia-assets.com/105948935/thumbnails/1.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/107215584/Physical_aging_for_an_epoxy_network_diglycidyl_ether_of_bisphenol_A_m_xylylenediamine">Physical aging for an epoxy network diglycidyl ether of bisphenol A/m-xylylenediamine</a></div><div class="wp-workCard_item"><span>Polymer</span><span>, 2003</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><a id="250e9969a04afef26351c8dc6458b58d" class="wp-workCard--action" rel="nofollow" data-click-track="profile-work-strip-download" data-download="{"attachment_id":105948935,"asset_id":107215584,"asset_type":"Work","button_location":"profile"}" href="https://www.academia.edu/attachments/105948935/download_file?st=MTczMjUwNjk4Myw4LjIyMi4yMDguMTQ2&st=MTczMjUwNjk4Miw4LjIyMi4yMDguMTQ2&s=profile"><span><i class="fa fa-arrow-down"></i></span><span>Download</span></a><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="107215584"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="107215584"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 107215584; 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dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "250e9969a04afef26351c8dc6458b58d" } } $('.js-work-strip[data-work-id=107215584]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":107215584,"title":"Physical aging for an epoxy network diglycidyl ether of bisphenol A/m-xylylenediamine","translated_title":"","metadata":{"publisher":"Elsevier BV","grobid_abstract":"The physical aging of the epoxy network consisting of a diglycidyl ether of bisphenol A (BADGE n ¼ 0) and m-xylylenediamine (m-XDA) were studied by differential scanning calorimetry. The following aging temperatures have been used in this work: 60, 70, 80, 90, 100 and 110 8C. The glass transition temperature and the variation of the specific heat capacities have been calculated using the method based on the intersection of both enthalpy-temperature lines for glassy and liquid states. The endothermic aging peak, relaxation enthalpy and fictive temperature were also calculated for each aging temperature and aging time.","publication_date":{"day":null,"month":null,"year":2003,"errors":{}},"publication_name":"Polymer","grobid_abstract_attachment_id":105948935},"translated_abstract":null,"internal_url":"https://www.academia.edu/107215584/Physical_aging_for_an_epoxy_network_diglycidyl_ether_of_bisphenol_A_m_xylylenediamine","translated_internal_url":"","created_at":"2023-09-25T20:19:22.114-07:00","preview_url":null,"current_user_can_edit":null,"current_user_is_owner":null,"owner_id":45089310,"coauthors_can_edit":true,"document_type":"paper","co_author_tags":[],"downloadable_attachments":[{"id":105948935,"title":"","file_type":"pdf","scribd_thumbnail_url":"https://attachments.academia-assets.com/105948935/thumbnails/1.jpg","file_name":"s0032-386128032900624-420230926-1-9aekc7.pdf","download_url":"https://www.academia.edu/attachments/105948935/download_file?st=MTczMjUwNjk4Myw4LjIyMi4yMDguMTQ2&st=MTczMjUwNjk4Miw4LjIyMi4yMDguMTQ2&","bulk_download_file_name":"Physical_aging_for_an_epoxy_network_digl.pdf","bulk_download_url":"https://d1wqtxts1xzle7.cloudfront.net/105948935/s0032-386128032900624-420230926-1-9aekc7-libre.pdf?1695699454=\u0026response-content-disposition=attachment%3B+filename%3DPhysical_aging_for_an_epoxy_network_digl.pdf\u0026Expires=1732510582\u0026Signature=M5QyzKxMWSCwl5eL0lqpuyThBhd5HQK43ZgoWLyNszmu6pMjp9gLBR~tVUJyAsNp1Buu4tXMkykqARZ2iG9D2cuFAy8Nc8ceHa5cFqNtOD2vLsSp1JduyPRm5ZTnNyAKxBmpx1wcfV0gDfE--0QRsVZLX4~veYT7DJCDcYb2dUp91yIWkRanTBoUrnzw1N3cysR8pEwtNNkzkrdTOqgMh~GO37TCXrsHdCMw7gFbR1zmpsBv3K3fLQENmXsjmTm03UC6E1Qykfcxcz9YVnDaxyPpZg2qDeFEwV~Opeg6n0BDjUW5EQ6hOFsecdD3qXXotXqfpBtm7DqM7Z0RC6rOuA__\u0026Key-Pair-Id=APKAJLOHF5GGSLRBV4ZA"}],"slug":"Physical_aging_for_an_epoxy_network_diglycidyl_ether_of_bisphenol_A_m_xylylenediamine","translated_slug":"","page_count":6,"language":"en","content_type":"Work","owner":{"id":45089310,"first_name":"Francisco","middle_initials":null,"last_name":"Fraga López","page_name":"FragaFrancisco","domain_name":"independent","created_at":"2016-03-14T09:17:24.694-07:00","display_name":"Francisco Fraga López","url":"https://independent.academia.edu/FragaFrancisco"},"attachments":[{"id":105948935,"title":"","file_type":"pdf","scribd_thumbnail_url":"https://attachments.academia-assets.com/105948935/thumbnails/1.jpg","file_name":"s0032-386128032900624-420230926-1-9aekc7.pdf","download_url":"https://www.academia.edu/attachments/105948935/download_file?st=MTczMjUwNjk4Myw4LjIyMi4yMDguMTQ2&st=MTczMjUwNjk4Miw4LjIyMi4yMDguMTQ2&","bulk_download_file_name":"Physical_aging_for_an_epoxy_network_digl.pdf","bulk_download_url":"https://d1wqtxts1xzle7.cloudfront.net/105948935/s0032-386128032900624-420230926-1-9aekc7-libre.pdf?1695699454=\u0026response-content-disposition=attachment%3B+filename%3DPhysical_aging_for_an_epoxy_network_digl.pdf\u0026Expires=1732510582\u0026Signature=M5QyzKxMWSCwl5eL0lqpuyThBhd5HQK43ZgoWLyNszmu6pMjp9gLBR~tVUJyAsNp1Buu4tXMkykqARZ2iG9D2cuFAy8Nc8ceHa5cFqNtOD2vLsSp1JduyPRm5ZTnNyAKxBmpx1wcfV0gDfE--0QRsVZLX4~veYT7DJCDcYb2dUp91yIWkRanTBoUrnzw1N3cysR8pEwtNNkzkrdTOqgMh~GO37TCXrsHdCMw7gFbR1zmpsBv3K3fLQENmXsjmTm03UC6E1Qykfcxcz9YVnDaxyPpZg2qDeFEwV~Opeg6n0BDjUW5EQ6hOFsecdD3qXXotXqfpBtm7DqM7Z0RC6rOuA__\u0026Key-Pair-Id=APKAJLOHF5GGSLRBV4ZA"}],"research_interests":[{"id":48,"name":"Engineering","url":"https://www.academia.edu/Documents/in/Engineering"},{"id":511,"name":"Materials Science","url":"https://www.academia.edu/Documents/in/Materials_Science"},{"id":58527,"name":"Polymer","url":"https://www.academia.edu/Documents/in/Polymer"},{"id":78753,"name":"Differential scanning calorimetry","url":"https://www.academia.edu/Documents/in/Differential_scanning_calorimetry"},{"id":82446,"name":"bisphenol A","url":"https://www.academia.edu/Documents/in/bisphenol_A"},{"id":114712,"name":"Enthalpy","url":"https://www.academia.edu/Documents/in/Enthalpy"},{"id":159672,"name":"Epoxy","url":"https://www.academia.edu/Documents/in/Epoxy"},{"id":260118,"name":"CHEMICAL SCIENCES","url":"https://www.academia.edu/Documents/in/CHEMICAL_SCIENCES"},{"id":282351,"name":"Glass Transition","url":"https://www.academia.edu/Documents/in/Glass_Transition"},{"id":335228,"name":"Glass Transition Temperature","url":"https://www.academia.edu/Documents/in/Glass_Transition_Temperature"},{"id":827572,"name":"Specific Heat","url":"https://www.academia.edu/Documents/in/Specific_Heat"}],"urls":[{"id":34074088,"url":"https://api.elsevier.com/content/article/PII:S0032386103006244?httpAccept=text/xml"}]}, dispatcherData: dispatcherData }); $(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="107215582"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/107215582/TTT_cure_diagram_for_an_epoxy_system_diglycidyl_ether_of_bisphenol_A_1_2_diamine_cyclohexane_calcium_carbonate_filler"><img alt="Research paper thumbnail of TTT cure diagram for an epoxy system diglycidyl ether of bisphenol A/1,2 diamine cyclohexane/calcium carbonate filler" class="work-thumbnail" src="https://attachments.academia-assets.com/105948932/thumbnails/1.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/107215582/TTT_cure_diagram_for_an_epoxy_system_diglycidyl_ether_of_bisphenol_A_1_2_diamine_cyclohexane_calcium_carbonate_filler">TTT cure diagram for an epoxy system diglycidyl ether of bisphenol A/1,2 diamine cyclohexane/calcium carbonate filler</a></div><div class="wp-workCard_item"><span>Polymer</span><span>, 2001</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><a id="ef9edf44d0e992699138a40c690b5817" class="wp-workCard--action" rel="nofollow" data-click-track="profile-work-strip-download" data-download="{"attachment_id":105948932,"asset_id":107215582,"asset_type":"Work","button_location":"profile"}" href="https://www.academia.edu/attachments/105948932/download_file?st=MTczMjUwNjk4Myw4LjIyMi4yMDguMTQ2&st=MTczMjUwNjk4Miw4LjIyMi4yMDguMTQ2&s=profile"><span><i class="fa fa-arrow-down"></i></span><span>Download</span></a><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="107215582"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="107215582"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 107215582; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=107215582]").text(description); $(".js-view-count[data-work-id=107215582]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 107215582; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='107215582']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 107215582, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (true){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "ef9edf44d0e992699138a40c690b5817" } } $('.js-work-strip[data-work-id=107215582]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":107215582,"title":"TTT cure diagram for an epoxy system diglycidyl ether of bisphenol A/1,2 diamine cyclohexane/calcium carbonate filler","translated_title":"","metadata":{"publisher":"Elsevier BV","grobid_abstract":"Curing reactions of the epoxy system consisting of a diglycidyl ether of bisphenol A (BADGE n 0; 1,2 diaminecyclohexane (DCH); and calcium carbonate ®ller were studied to calculate a time±temperature-transformation (TTT) isothermal cure diagram for this system. Gel times were measured as a function of temperature using two experimental methods: solubility test and dynamic mechanical analysis (DMA). The results obtained are in fair agreement with that obtained for the two component system BADGE n 0=1; 2 DCH. Vitri®cation times for the three component system was higher than those obtained for the system BADGE n 0=1; 2 DCH and the conversions achieved were very close to maximum values. The activation energy for the overall polymerization reaction was calculated from the gel times obtained using the two above mentioned methods: solubility test (57.12 kJ/mol) and DMA (54.12 kJ/mol). These values are of the same order than those obtained for the two component epoxy system. It was established that the addition of calcium carbonate ®ller avoids the appearance of physical aging, thus making easier both the determination of glass transition temperatures, and the calculation of the TTT diagram.","publication_date":{"day":null,"month":null,"year":2001,"errors":{}},"publication_name":"Polymer","grobid_abstract_attachment_id":105948932},"translated_abstract":null,"internal_url":"https://www.academia.edu/107215582/TTT_cure_diagram_for_an_epoxy_system_diglycidyl_ether_of_bisphenol_A_1_2_diamine_cyclohexane_calcium_carbonate_filler","translated_internal_url":"","created_at":"2023-09-25T20:19:21.816-07:00","preview_url":null,"current_user_can_edit":null,"current_user_is_owner":null,"owner_id":45089310,"coauthors_can_edit":true,"document_type":"paper","co_author_tags":[],"downloadable_attachments":[{"id":105948932,"title":"","file_type":"pdf","scribd_thumbnail_url":"https://attachments.academia-assets.com/105948932/thumbnails/1.jpg","file_name":"s0032-386128002900712-620230926-1-ku9o9q.pdf","download_url":"https://www.academia.edu/attachments/105948932/download_file?st=MTczMjUwNjk4Myw4LjIyMi4yMDguMTQ2&st=MTczMjUwNjk4Miw4LjIyMi4yMDguMTQ2&","bulk_download_file_name":"TTT_cure_diagram_for_an_epoxy_system_dig.pdf","bulk_download_url":"https://d1wqtxts1xzle7.cloudfront.net/105948932/s0032-386128002900712-620230926-1-ku9o9q-libre.pdf?1695699455=\u0026response-content-disposition=attachment%3B+filename%3DTTT_cure_diagram_for_an_epoxy_system_dig.pdf\u0026Expires=1732510582\u0026Signature=FIlu~Eveu6j1zHiOPghdzR-D0TGQe~PL3zujzwoSMwY8AmC5jXZi~oNvchG3Lnl1XcKY7uAbuHLLWSPpkRGyV4Q6SWhplSms7qHOabDOp4nYu5wb2tgtqZL6KvxqzYSFD~OV0pSZJl3twAa5P-a2v11du95qeO7eXvAj-jPvGtXsI1816j0LwhZ-QYVNdOpMrPnqGmSOg6eex4VM1SqYUmxzVhQJSGEk8qq5LiCJ6c6TfsD3cR2neaX~b~gyPLCpwbBod6Qu3ygAdjjlHEeQhPV3JBqnlK92k7A-QuwC8Tkvoy1JaHqsPTveSfMJA4V3Ku6YBZnWfbEcrI-vil9VMw__\u0026Key-Pair-Id=APKAJLOHF5GGSLRBV4ZA"}],"slug":"TTT_cure_diagram_for_an_epoxy_system_diglycidyl_ether_of_bisphenol_A_1_2_diamine_cyclohexane_calcium_carbonate_filler","translated_slug":"","page_count":7,"language":"en","content_type":"Work","owner":{"id":45089310,"first_name":"Francisco","middle_initials":null,"last_name":"Fraga 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epoxy/cure agent reaction" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/107215577/Activation_energies_and_rate_constants_for_an_epoxy_cure_agent_reaction">Activation energies and rate constants for an epoxy/cure agent reaction</a></div><div class="wp-workCard_item"><span>Journal of Thermal Analysis</span><span>, 1996</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">ABSTRACT From the peak reaction temperatures as a function of heating rate, the activation energi...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">ABSTRACT From the peak reaction temperatures as a function of heating rate, the activation energies were obtained for a system consisting of an epoxy resin (Badgen=0) and a curing agent (isophorone diamine), using a Perkin Elmer DSC7 operated in the dynamic mode. At the same time, the Arrhenius law was used to calculate rate constants.</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="107215577"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="107215577"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 107215577; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=107215577]").text(description); $(".js-view-count[data-work-id=107215577]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 107215577; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='107215577']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 107215577, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=107215577]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":107215577,"title":"Activation energies and rate constants for an epoxy/cure agent reaction","translated_title":"","metadata":{"abstract":"ABSTRACT From the peak reaction temperatures as a function of heating rate, the activation energies were obtained for a system consisting of an epoxy resin (Badgen=0) and a curing agent (isophorone diamine), using a Perkin Elmer DSC7 operated in the dynamic mode. 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$(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="106527450"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/106527450/Effects_of_diffusion_on_the_kinetic_study_of_the_system_BADGE_n_0_m_xylylenediamine"><img alt="Research paper thumbnail of Effects of diffusion on the kinetic study of the system BADGE n = 0/m-xylylenediamine" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/106527450/Effects_of_diffusion_on_the_kinetic_study_of_the_system_BADGE_n_0_m_xylylenediamine">Effects of diffusion on the kinetic study of the system BADGE n = 0/m-xylylenediamine</a></div><div class="wp-workCard_item"><span>Journal of Applied Polymer Science</span><span>, 1999</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">ABSTRACT The curing reactions of an epoxy system composed of a diglycidyl ether of bisphenol A (B...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">ABSTRACT The curing reactions of an epoxy system composed of a diglycidyl ether of bisphenol A (BADGE n=0) and m-xylylenediamine (m-XDA) were studied. Two models, the first based solely on chemical kinetics and the second accounting for diffusion, were used and compared to the experimental data. The epoxy resin was used as received in a first series of experiments. In a second series of experiments, the resin was purified in vacuo (180°C and 1 mmHg). The inclusion of a diffusion factor in the second model allowed for the cure kinetics to be predicted over the whole range of conversion covering both pre- and postvitrification stages. The investigation was made in the temperature range 50–110°C, which is considered optimum for the isothermal curing of the epoxy system studied. © 1999 John Wiley &amp;amp;amp; Sons, Inc. J Appl Polym Sci 74: 2997–3005, 1999</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="106527450"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="106527450"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 106527450; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=106527450]").text(description); $(".js-view-count[data-work-id=106527450]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 106527450; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='106527450']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 106527450, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=106527450]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":106527450,"title":"Effects of diffusion on the kinetic study of the system BADGE n = 0/m-xylylenediamine","translated_title":"","metadata":{"abstract":"ABSTRACT The curing reactions of an epoxy system composed of a diglycidyl ether of bisphenol A (BADGE n=0) and m-xylylenediamine (m-XDA) were studied. 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