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id="mood_pagetitle_esbu" class="blue mood_pagetitle_default"><div class="content"><h1>Automated Lab Reactors and In-Situ Analysis</h1><h2>Instruments for Chemical Synthesis, Process Development, and R&D</h2></div></div></div><div class="assistantbox"><link rel="stylesheet" href="/etc/designs/mt/widgets/misc/assistantbox.min-v47.css" type="text/css"><div class="assistant_box"><div class="top"><strong class="assistant_title">How can we assist you?</strong></div><div class="center"><div class="content"><input type="hidden" id="assistantBox_noSearchTermMsg" value="Please provide your search term."/><ul class="expandable_link_list"><li class="assistant_li" id="assistant_DocumentFinder"><a href="/sg/en/home/search/library.tabs.custom2.html" class="exp_link"><em class="assistant_box_slider_arrow"><strong>►</strong></em>Expertise Library </a></li><li class="assistant_li" id="assistant_ProductFinder"><a href="" class="exp_link" data-prodfindertext="Product Finder"><em 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class="esbutabs p5tabs"><link rel="stylesheet" href="/etc/designs/mt/widgets/misc/p5.min-v47.css" type="text/css"><script src="/etc/designs/mt/widgets/misc/p5.min-v47.js"></script> <div class="p5tabs_singlePage"><div id="esbutabs"><div class="introtext_wrapper"><div class="introtext_order_2" style="display:none;"><div class="seopar parsys"><div class="introtext section"><div class="introtext_content"><div class="introtext_col" data-see-more-label="Read more" data-see-less-label="See less"><h2>Automated Lab Reactors & In-Situ Analysis for Chemical Process Development</h2><div class="introtext_collapsible" data-truncate-at="150"><div class="introtext_collapsed"><p>Automated synthesis reactors and <a>controlled laboratory reactors</a> replace traditional round bottom flasks or <a>jacketed lab reactors</a>. This allows&nbs...</p></div><div class="introtext_expanded"><p>Automated synthesis reactors and <a href="/sg/en/home/products/L1_AutochemProducts/chemical-synthesis-reactor-systems.html">controlled laboratory reactors</a> replace traditional round bottom flasks or <a href="/sg/en/home/applications/L1_AutoChem_Applications/L2_ReactionAnalysis/jacketed-reactor.html">jacketed lab reactors</a>. This allows <a target="_blank">chemical synthesis </a>researchers to explore new reaction conditions and develop innovative chemistry. Engineers apply an advanced version of these <a href="/sg/us/en/home/products/L1_AutochemProducts.html">automated laboratory reactor (ALR)</a> systems to measure real-time <a></a><a href="/sg/en/home/products/L1_AutochemProducts/reaction-calorimeters.html">reaction calorimetry</a>, <a href="/sg/en/home/applications/L1_AutoChem_Applications/Process-Safety/heat-of-reaction.html" target="_self">heat of reaction</a>, and thermodynamic data for <a>process safety</a> understanding and control.</p><p>Unattended, fully <a target="_blank"></a><a href="/sg/en/home/products/L1_AutochemProducts/automated-sampling-systems.html">automated sampling of chemical reactions</a>, including slurries, enable chemists and engineers to gain samples throughout the reaction, providing valuable information. With the unique patented sampling probe, <a href="/sg/en/home/products/L1_AutochemProducts/automated-sampling-systems/easysampler-1210.html">EasySampler</a> quenches the sample at the point of sampling and at reaction conditions, proving a truly representative sample for accurate analytical data. </p><p><a href="/sg/en/home/products/L1_AutochemProducts.html">In-situ reaction analysis</a> with <a></a><a href="/sg/en/home/applications/L1_AutoChem_Applications/ftir-spectroscopy/attenuated-total-reflectance-atr.html" target="_blank">Attenuated Total Reflection (ATR)</a> - <a href="/sg/en/home/products/L1_AutochemProducts/ftir-and-raman-spectrometers/ftir-spectrometers.html">Fourier Transform Infrared (FTIR) spectrometers</a> (<a href="/sg/en/home/applications/L1_AutoChem_Applications/ftir-spectroscopy/attenuated-total-reflectance-atr.html">ATR-FTIR spectroscopy</a>) provide real-time monitoring of key reaction species. By following reaction progression, initiation, conversion, intermediate formation, and endpoints, these tools optimize process design and quality. Increased process knowledge from <a href="/sg/en/home/products/L1_AutochemProducts.html">inline reaction analysis</a> supports the development of batch or <a></a><a href="/sg/en/home/applications/L1_AutoChem_Applications/continuous.html">continuous flow chemistry</a> and enables chemical reactions to be scaled-up.</p><p><a href="/sg/en/home/products/L1_AutochemProducts/particle-size-analyzers.html">Inline particle size analyzers</a> enable scientists and engineers to track the rate and degree of change to particles, crystals, or droplets as they naturally exist in process. By understanding how particles change in real time, engineers can track batch-to-batch consistency, detect endpoints and optimize downstream throughput and product quality. </p><p><a>Our inline </a><a href="/sg/en/home/applications/L1_AutoChem_Applications/L2_PAT.html">PAT technologies</a> are probe-based instruments that track critical process parameters and quality attributes for <a href="/sg/en/home/applications/L1_AutoChem_Applications/L2_PAT/quality-by-design.html" target="_blank">Quality by Design (QbD)</a> requirements. Lab <a href="/sg/en/home/applications/L1_AutoChem_Applications/L2_PAT.html#pat-tools">PAT instruments</a> help design a quality process. Plant <a href="/sg/en/home/applications/L1_AutoChem_Applications/L2_PAT.html#pat-tools">PAT tools</a> enable monitoring and control of a process.</p><p>Integrated <a href="/sg/en/home/products/L1_AutochemProducts/automated-reactor-in-situ-analysis-software.html">software for chemical reactors and PAT instruments</a> enable researchers to combine all technology in a simple and powerful platform, which captures data, visualizes and interprets experiments, prepares and report results, and compares batches or experiments.<br><br> Key application areas include:</p><ul><li><a title="Chemical Synthesis" href="/sg/en/home/applications/L1_AutoChem_Applications/L2_ReactionAnalysis.html">Chemical Synthesis</a>, including <a href="/sg/en/home/applications/L1_AutoChem_Applications/L2_ReactionAnalysis/design-of-experiments-doe.html">DoE Studies</a>, <a href="/sg/en/home/applications/L1_AutoChem_Applications/L2_ReactionAnalysis/alkylation-reactions.html">Alkylation Reactions</a>, <a 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link_blocks_twoCol"><div class="link_block link_block_twoCol"><div class="link_image"><a href="/sg/en/home/applications/L1_AutoChem_Applications/L2_ReactionAnalysis.html"><picture><img loading="lazy" src="/sg/en/home/applications/L1_AutoChem_Applications/L2_ReactionAnalysis/_jcr_content/thumbnailImage.webImage.file.png" alt="Chemical Synthesis" title="Chemical Synthesis"></picture></a></div><div class="link_info"><h3 class="link_title"><a href="/sg/en/home/applications/L1_AutoChem_Applications/L2_ReactionAnalysis.html">Chemical Synthesis</a></h3><div class="link_description"> Chemical synthesis occurs when two or more molecules are combined to form a product molecule that possesses specific properties. 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Learn more. </div></div></div><div class="link_block link_block_twoCol"><div class="link_image"><a href="/sg/en/home/applications/L1_AutoChem_Applications/L2_Formulation.html"><picture><source srcset="/dam/product_organizations/autochem/Images/Formulations_Thumb.jpg/_jcr_content/renditions/cq5dam.web.240.480.jpeg" media="(min-width: 0px) and (max-width: 320px)" type="image/jpeg"><img loading="lazy" src="/dam/product_organizations/autochem/Images/Formulations_Thumb.jpg/_jcr_content/renditions/cq5dam.web.1280.1280.jpeg" alt="Particle Size Impacts Formulations & Product Development" title="Particle Size Impacts Formulations & Product Development"></picture></a></div><div class="link_info"><h3 class="link_title"><a href="/sg/en/home/applications/L1_AutoChem_Applications/L2_Formulation.html">Particle Size in Formulations</a></h3><div class="link_description"> Solid and liquid formulations are influenced by particle and droplet size. Particles and droplets affect the bioavailability, stability, and manufacturability of formulations incl... </div></div></div><div class="link_block link_block_twoCol"><div class="link_image"><a href="/sg/en/home/applications/L1_AutoChem_Applications/Parallel-Synthesis-Screening-Reaction-Conditions.html"><picture><img loading="lazy" src="/sg/en/home/applications/L1_AutoChem_Applications/Parallel-Synthesis-Screening-Reaction-Conditions/_jcr_content/thumbnailImage.webImage.file.png" alt="Parallel Synthesis" title="Parallel Synthesis"></picture></a></div><div class="link_info"><h3 class="link_title"><a href="/sg/en/home/applications/L1_AutoChem_Applications/Parallel-Synthesis-Screening-Reaction-Conditions.html">Parallel Synthesis</a></h3><div class="link_description"> Parallel Synthesis accelerates the discovery of potential drug candidates and screen for optimal process conditions as the molecule proceeds through development phases. Instead of... </div></div></div><div class="link_block link_block_twoCol"><div class="link_image"><a href="/sg/en/home/applications/L1_AutoChem_Applications/fermentation.html"><picture><img loading="lazy" src="/sg/en/home/applications/L1_AutoChem_Applications/fermentation/_jcr_content/thumbnailImage.webImage.file.png" alt="Fermentation and Bioprocessing" title="Fermentation and Bioprocessing"></picture></a></div><div class="link_info"><h3 class="link_title"><a href="/sg/en/home/applications/L1_AutoChem_Applications/fermentation.html">Fermentation and Bioprocessing</a></h3><div class="link_description"> Characterize & Optimize Fermentation & Bioprocesses in Real Time to Maximize Production </div></div></div><div class="link_block link_block_twoCol"><div class="link_image"><a href="/sg/en/home/applications/L1_AutoChem_Applications/continuous.html"><picture><img loading="lazy" src="/sg/en/home/applications/L1_AutoChem_Applications/continuous/_jcr_content/thumbnailImage.webImage.file.png" alt="Flow Chemistry" title="Flow Chemistry"></picture></a></div><div class="link_info"><h3 class="link_title"><a href="/sg/en/home/applications/L1_AutoChem_Applications/continuous.html">Flow Chemistry</a></h3><div class="link_description"> Continuous flow chemistry opens options with exothermic synthetic steps that are not possible in batch reactors, and new developments in flow reactor design provide alternatives fo... </div></div></div><div class="link_block link_block_twoCol"><div class="link_image"><a href="/sg/en/home/applications/L1_AutoChem_Applications/Raman-Spectroscopy.html"><picture><source srcset="/dam/autochem/applications/raman-spectroscopy/what-is-raman-spectroscopy-thumbnail-300x185.jpg/_jcr_content/renditions/cq5dam.web.240.240.webp" media="(min-width: 0px) and (max-width: 320px)" type="image/webp"><source srcset="/dam/autochem/applications/raman-spectroscopy/what-is-raman-spectroscopy-thumbnail-300x185.jpg/_jcr_content/renditions/cq5dam.web.240.480.jpeg" media="(min-width: 0px) and (max-width: 320px)" type="image/jpeg"><source srcset="/dam/autochem/applications/raman-spectroscopy/what-is-raman-spectroscopy-thumbnail-300x185.jpg/_jcr_content/renditions/original.webp" media="(min-width: 321px) and (max-width: 480px)" type="image/webp"><source srcset="/dam/autochem/applications/raman-spectroscopy/what-is-raman-spectroscopy-thumbnail-300x185.jpg/_jcr_content/renditions/original.webp" media="(min-width: 481px) and (max-width: 640px)" type="image/webp"><source srcset="/dam/autochem/applications/raman-spectroscopy/what-is-raman-spectroscopy-thumbnail-300x185.jpg/_jcr_content/renditions/original.webp" media="(min-width: 641px) and (max-width: 800px)" type="image/webp"><source srcset="/dam/autochem/applications/raman-spectroscopy/what-is-raman-spectroscopy-thumbnail-300x185.jpg/_jcr_content/renditions/original.webp" media="(min-width: 801px)" type="image/webp"><img loading="lazy" src="/dam/autochem/applications/raman-spectroscopy/what-is-raman-spectroscopy-thumbnail-300x185.jpg/_jcr_content/renditions/cq5dam.web.1280.1280.jpeg" alt="Raman Spectroscopy" title="Raman Spectroscopy"></picture></a></div><div class="link_info"><h3 class="link_title"><a href="/sg/en/home/applications/L1_AutoChem_Applications/Raman-Spectroscopy.html">Raman Spectroscopy</a></h3><div class="link_description"> Raman spectroscopy fundamentals. Learn about Raman vs IR, Raman scattering principle, the Raman shift, Rayleigh scattering and more. </div></div></div><div class="link_block link_block_twoCol"><div class="link_image"><a href="/sg/en/home/applications/L1_AutoChem_Applications/ftir-spectroscopy.html"><picture><source srcset="/dam/autochem/applications/ftir-spectroscopy/ftir-spectroscopy-thumbnail-300x185.png/_jcr_content/renditions/cq5dam.web.240.240.webp" media="(min-width: 0px) and (max-width: 320px)" type="image/webp"><source srcset="/dam/autochem/applications/ftir-spectroscopy/ftir-spectroscopy-thumbnail-300x185.png/_jcr_content/renditions/original.webp" media="(min-width: 321px) and (max-width: 480px)" type="image/webp"><source srcset="/dam/autochem/applications/ftir-spectroscopy/ftir-spectroscopy-thumbnail-300x185.png/_jcr_content/renditions/original.webp" media="(min-width: 481px) and (max-width: 640px)" type="image/webp"><source srcset="/dam/autochem/applications/ftir-spectroscopy/ftir-spectroscopy-thumbnail-300x185.png/_jcr_content/renditions/original.webp" media="(min-width: 641px) and (max-width: 800px)" type="image/webp"><source srcset="/dam/autochem/applications/ftir-spectroscopy/ftir-spectroscopy-thumbnail-300x185.png/_jcr_content/renditions/original.webp" media="(min-width: 801px)" type="image/webp"><img loading="lazy" src="/dam/autochem/applications/ftir-spectroscopy/ftir-spectroscopy-thumbnail-300x185.png/_jcr_content/renditions/cq5dam.web.1280.1280.png" alt="FTIR Spectroscopy" title="FTIR Spectroscopy"></picture></a></div><div class="link_info"><h3 class="link_title"><a href="/sg/en/home/applications/L1_AutoChem_Applications/ftir-spectroscopy.html">FTIR Spectroscopy</a></h3><div class="link_description"> Discover how FTIR spectroscopy utilizes infrared energy to provide a unique fingerprint for identification and analysis. Enhance your research with our comprehensive FTIR spectrosc... </div></div></div></div></div></div></div></div><div class="ptab-content publications" data-tab-name="publications" id="publications"><h3 class="ptabs_accordion_header simple-accordion_header simple-accordion_header-large"><span class="accordion_expander simple-accordion_icon"></span>Publications</h3><div class="ptab-content-body"><h3>Publications on Crystallization, Organic Synthesis, Process Development, Safety and PAT</h3><div class="mask"></div><div class="publicationsblockpar parsys"><div class="matchingblockpush section"><link rel="stylesheet" href="/etc/designs/mt/widgets/misc/tabnavigation.min-v47.css" type="text/css"><div id="mb_esbutabspublicationsblockparmatchingblockpush" class="matching_block_wrapper matching_box mb_gridLayout" data-swiftype-index="false"><input type="hidden" name="mbTabItemsCount" value="1"/><div class="tab_navigation_mb title">White Papers</div><div class="center"><div class="content accordion_blue_grey layout_ mb_gridLayout"><div class="mbItemGrid"><div class="mbItemWrapper rowLevel_2"><div class="mbItem"><div class="image"><a href="/sg/en/home/library/white-papers/automated-reactors/green-chemistry.html"><img loading="lazy" src="/dam/autochem/library/whitepaper/green-sustainable-chemistry/advancing-green-sustainable-chemistry-wp-thumb-300x300.png/_jcr_content/renditions/cq5dam.web.1280.1280.png" align="right" alt="Reaction Analysis Modeling to Drive Green Chemistry and Sustainable Development" title="Reaction Analysis Modeling to Drive Green Chemistry and Sustainable Development"/></a><div class="itemInfo"><div class="mbItemTitle"><a href="/sg/en/home/library/white-papers/automated-reactors/green-chemistry.html"> Advancing Green and Sustainable Chemistry </a></div><div class="description hyphenate"><a class="noStyle" href="/sg/en/home/library/white-papers/automated-reactors/green-chemistry.html"> Drive sustainable development through green chemistry practices by 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class="description hyphenate"><a class="noStyle" href="/sg/en/home/library/white-papers/automated-reactors/Crystallization-Process-Design.html"> Three world-class crystallization researchers present how to deliver significant improvements in crystallization process design. </a></div><div class="feedback_wrapper"><form method="get" action="/sg/en/home/library/white-papers/automated-reactors/Crystallization-Process-Design.fb.mainpar.feedbackb.html"><button class="fb-button-p5a btn-action btn-primary" aria-label="Get the White Paper Now"><span>Get the White Paper Now</span></button></form></div></div></div></div></div><div class="mbItemWrapper rowLevel_3"><div class="mbItem"><div class="mbItemTitle"><a href="/sg/en/home/library/white-papers/automated-reactors/pat-academic-research.html"> The Role of Process Analytical Technology in Academic Research </a></div><div class="image"><a href="/sg/en/home/library/white-papers/automated-reactors/pat-academic-research.html"><img loading="lazy" 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