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</a></div></div></div></div><div class="right-panel-container"><div class="user-content-wrapper"><div class="uploads-container" id="social-redesign-work-container"><div class="upload-header"><h2 class="ds2-5-heading-sans-serif-xs">Uploads</h2></div><div class="documents-container backbone-social-profile-documents" style="width: 100%;"><div class="u-taCenter"></div><div class="profile--tab_content_container js-tab-pane tab-pane active" id="all"><div class="profile--tab_heading_container js-section-heading" data-section="Papers" id="Papers"><h3 class="profile--tab_heading_container">Papers by Albert Robbat</h3></div><div class="js-work-strip profile--work_container" data-work-id="114405672"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/114405672/Fast_gas_chromatography_mass_spectrometry_analysis_in_support_of_risk_based_decisions"><img alt="Research paper thumbnail of Fast gas chromatography/mass spectrometry analysis in support of risk‐based decisions" class="work-thumbnail" src="https://attachments.academia-assets.com/111112312/thumbnails/1.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/114405672/Fast_gas_chromatography_mass_spectrometry_analysis_in_support_of_risk_based_decisions">Fast gas chromatography/mass spectrometry analysis in support of risk‐based decisions</a></div><div class="wp-workCard_item"><span>Field Analytical Chemistry and Technology</span><span>, 1999</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><a id="1eb1feff5185e7f2d8fd07eb38643192" class="wp-workCard--action" rel="nofollow" data-click-track="profile-work-strip-download" 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It was found that upon applying a potential to Pt supported on a O2– conducting yttria-stabilized zirconia disk, the decompoition of H2S significantly increased up to a factor of 11 at 600 C. The results appear to verify several aspects of NEMCA including the phenomenon that the electrolyte needs not to conduct reaction-specific species and that the degree of rate enhancement is related to the working electrode polarization. In addition, results indicate that separate chambers are not always required for electrocatalysis.</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="114405670"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="114405670"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 114405670; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=114405670]").text(description); $(".js-view-count[data-work-id=114405670]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 114405670; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='114405670']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 114405670, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=114405670]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":114405670,"title":"Electrocatalytic decomposition of hydrogen sulfide","translated_title":"","metadata":{"abstract":"ABSTRACT The recently discovered phenomenon of nonfaradaic electrochemical modification of catalytic activity (NEMCA) was explored for the electrocatalytic decomposition of H2S to H2 and S2 over Pt electrodes at 600–750 C and 1 atm. 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Independent organizations estimate that the current annual environmental market is $1.8 billion each for environmental engineering firms and commercial laboratory services companies. Clearly, with over 1200 hazardous waste, Superfund sites in EPA`s National Priority LIst (NPL) and with current estimates between 10,000 and 50,000 sites at the NPL funnel awaiting investigation, the nation faces a daunting political, social, and economic challenge. With increasing financial pressures placed on state governments and the recent inclusion of federal facilities into the Superfund process, Congress has finally become aware of the high costs and inefficiencies built into Superfund and in the way EPA conducts the site assessment and cleanup process. Federal funding agencies have focused considerable resources to develop innovative, field-based, analytical technologies that can provide real or near-real time chemical information about the site. Some EPA Regions appear to be out in front of the curve, with major site investigation programs being driven by the integration of innovative technologies. Unfortunately, most of these studies are being conducted on an ad hoc basis and are not universal within the agency. This is also true of DOD and DOE.</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="114405669"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="114405669"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 114405669; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=114405669]").text(description); $(".js-view-count[data-work-id=114405669]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 114405669; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='114405669']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 114405669, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=114405669]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":114405669,"title":"Hazardous Waste Site Investigation and Cleanup: Innovative Technologies, an Alternative Approach","translated_title":"","metadata":{"abstract":"Much has been made about the high costs associated with hazardous waste site investigations and cleanup. 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$(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="114405668"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/114405668/Environmental_applications_of_thermal_extraction_cone_penetrometry_and_ultrafast_gas_chromatography_mass_spectrometry"><img alt="Research paper thumbnail of Environmental applications of thermal extraction cone penetrometry and ultrafast gas chromatography/mass spectrometry" class="work-thumbnail" src="https://attachments.academia-assets.com/111112313/thumbnails/1.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/114405668/Environmental_applications_of_thermal_extraction_cone_penetrometry_and_ultrafast_gas_chromatography_mass_spectrometry">Environmental applications of thermal extraction cone penetrometry and ultrafast gas chromatography/mass spectrometry</a></div><div class="wp-workCard_item"><span>Field Analytical Chemistry and Technology</span><span>, 2001</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><a id="405615589c52bba2bc9be6163dd56f81" class="wp-workCard--action" rel="nofollow" data-click-track="profile-work-strip-download" data-download="{"attachment_id":111112313,"asset_id":114405668,"asset_type":"Work","button_location":"profile"}" href="https://www.academia.edu/attachments/111112313/download_file?st=MTczMjQyMzk5MSw4LjIyMi4yMDguMTQ2&s=profile"><span><i class="fa fa-arrow-down"></i></span><span>Download</span></a><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="114405668"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="114405668"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 114405668; 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A thermal extraction cone penetrometer (TECP) probe was used to extract soil-bound semivolatile organics, transferring them to the surface for analysis by ultrafast gas chromatography/mass spectrometry (GC/MS). Findings showed that polychlorinated biphenyls, polycyclic aromatic hydrocarbons, chlorinated pesticides, and explosives could be collected and analyzed in 5 min when the soil-water content was Ͻ20% and in 15 min when it was between 20 and 35%. When the TECP was directly connected to the GC/MS, trinitrotoluene (TNT) and four of its synthetic precursors were speciated in 20 sec. Moreover, 51 VOCs were detected by membrane-inlet mass spectrometry in ϳ10 sec. Organics were \"sniffed\" from a vial and identified using the Ion Fingerprint Detection TM software. 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$(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="114405667"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" rel="nofollow" href="https://www.academia.edu/114405667/Organic_titanium_in_coal_and_the_deposition_of_titanium_on_direct_liquefaction_catalysts"><img alt="Research paper thumbnail of Organic titanium in coal and the deposition of titanium on direct liquefaction catalysts" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" rel="nofollow" href="https://www.academia.edu/114405667/Organic_titanium_in_coal_and_the_deposition_of_titanium_on_direct_liquefaction_catalysts">Organic titanium in coal and the deposition of titanium on direct liquefaction catalysts</a></div><div class="wp-workCard_item"><span>Fuel</span><span>, Dec 1, 1984</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">Abstract Evidence for the presence of soluble organic titanium species in coals and coal-derived ...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">Abstract Evidence for the presence of soluble organic titanium species in coals and coal-derived materials was sought by the application of dialysis procedures. Dialysates prepared from a heavy direct liquefaction product, an SRC-1, and extracts of the corresponding feed coals contained</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="114405667"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="114405667"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 114405667; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=114405667]").text(description); $(".js-view-count[data-work-id=114405667]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 114405667; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='114405667']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 114405667, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=114405667]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":114405667,"title":"Organic titanium in coal and the deposition of titanium on direct liquefaction catalysts","translated_title":"","metadata":{"abstract":"Abstract Evidence for the presence of soluble organic titanium species in coals and coal-derived materials was sought by the application of dialysis procedures. 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chromatographic retention characteristic of polychlorinated biphenyls</a></div><div class="wp-workCard_item"><span>Analytical Chemistry</span><span>, May 15, 1988</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><a id="2536c583647ab7d14280a1ed0e4b6061" class="wp-workCard--action" rel="nofollow" data-click-track="profile-work-strip-download" data-download="{"attachment_id":111112337,"asset_id":114405666,"asset_type":"Work","button_location":"profile"}" href="https://www.academia.edu/attachments/111112337/download_file?st=MTczMjQyMzk5MSw4LjIyMi4yMDguMTQ2&s=profile"><span><i class="fa fa-arrow-down"></i></span><span>Download</span></a><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="114405666"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i 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}); </script> <div class="js-work-strip profile--work_container" data-work-id="114405664"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/114405664/Pretreatment_and_validation_procedure_for_glassy_carbon_voltammetric_indicator_electrodes"><img alt="Research paper thumbnail of Pretreatment and validation procedure for glassy carbon voltammetric indicator electrodes" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/114405664/Pretreatment_and_validation_procedure_for_glassy_carbon_voltammetric_indicator_electrodes">Pretreatment and validation procedure for glassy carbon voltammetric indicator electrodes</a></div><div class="wp-workCard_item"><span>Analytical Chemistry</span><span>, 1985</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">Metallographic pretreatment procedures are described which yleid surfaces whose eiectrochemlcaiiy...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">Metallographic pretreatment procedures are described which yleid surfaces whose eiectrochemlcaiiy active areas are Identical wlth their geometrlc areas. Glassy carbon indlcator electrodes (GCE) were used successfully in a stationary mode for cycllc ...</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="114405664"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="114405664"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 114405664; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=114405664]").text(description); $(".js-view-count[data-work-id=114405664]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 114405664; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='114405664']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 114405664, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=114405664]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":114405664,"title":"Pretreatment and validation procedure for glassy carbon voltammetric indicator electrodes","translated_title":"","metadata":{"abstract":"Metallographic pretreatment procedures are described which yleid surfaces whose eiectrochemlcaiiy active areas are Identical wlth their geometrlc areas. 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$(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="114405663"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/114405663/Author_response_The_diversity_and_function_of_sourdough_starter_microbiomes"><img alt="Research paper thumbnail of Author response: The diversity and function of sourdough starter microbiomes" class="work-thumbnail" src="https://attachments.academia-assets.com/111112310/thumbnails/1.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/114405663/Author_response_The_diversity_and_function_of_sourdough_starter_microbiomes">Author response: The diversity and function of sourdough starter microbiomes</a></div><div class="wp-workCard_item"><span>eLife</span><span>, 2020</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><a id="8ec01a9f873c04337d7bd240d70fb3b8" class="wp-workCard--action" rel="nofollow" data-click-track="profile-work-strip-download" data-download="{"attachment_id":111112310,"asset_id":114405663,"asset_type":"Work","button_location":"profile"}" href="https://www.academia.edu/attachments/111112310/download_file?st=MTczMjQyMzk5MSw4LjIyMi4yMDguMTQ2&s=profile"><span><i class="fa fa-arrow-down"></i></span><span>Download</span></a><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="114405663"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="114405663"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 114405663; 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Working with a community-scientist network of bread bakers, we determined the microbial diversity of 500 sourdough starters from four continents. In sharp contrast with widespread assumptions, we found little evidence for biogeographic patterns in starter communities. Strong co-occurrence patterns observed in situ and recreated in vitro demonstrate that microbial interactions shape sourdough community structure. Variation in dough rise rates and aromas were largely explained by acetic acid bacteria, a mostly overlooked group of sourdough microbes. 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$(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="114405661"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/114405661/Untargeted_approaches_in_food_omics_The_potential_of_comprehensive_two_dimensional_gas_chromatography_mass_spectrometry"><img alt="Research paper thumbnail of Untargeted approaches in food-omics: The potential of comprehensive two-dimensional gas chromatography/mass spectrometry" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/114405661/Untargeted_approaches_in_food_omics_The_potential_of_comprehensive_two_dimensional_gas_chromatography_mass_spectrometry">Untargeted approaches in food-omics: The potential of comprehensive two-dimensional gas chromatography/mass spectrometry</a></div><div class="wp-workCard_item"><span>TrAC Trends in Analytical Chemistry</span><span>, 2021</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">Abstract The contribution focuses on untargeted data processing/analysis approaches that are curr...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">Abstract The contribution focuses on untargeted data processing/analysis approaches that are currently adopted to explore the 4D-data matrices produced by comprehensive two-dimensional gas chromatography-mass spectrometry (GC × GC-MS) in food-omics. Strategies for untargeted explorations are rationalized through the type of features adopted (i.e., visual, datapoint, peak, and peak-regions) at the data processing level, and then discussed through relevant applications and illustrative examples, selected over peer-reviewed literature. The role of MS, including high vs. low resolution MS, as an active probe for specific cross-comparative analysis, is critically discussed also in the context of spectral deconvolution and subtraction, well-established procedures for 1D GC-MS explorations. Moreover, the challenging task of post-targeting aimed at identifying “unknown – knowns”, is examined in its potential, being the key to access a higher level of information. Selected examples emphasize the importance of reliable identification by retention indexing, retention pattern ordering, sensory evaluation (sensory analysis and olfactometry), and data mining.</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="114405661"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="114405661"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 114405661; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=114405661]").text(description); $(".js-view-count[data-work-id=114405661]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 114405661; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='114405661']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 114405661, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=114405661]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":114405661,"title":"Untargeted approaches in food-omics: The potential of comprehensive two-dimensional gas chromatography/mass spectrometry","translated_title":"","metadata":{"abstract":"Abstract The contribution focuses on untargeted data processing/analysis approaches that are currently adopted to explore the 4D-data matrices produced by comprehensive two-dimensional gas chromatography-mass spectrometry (GC × GC-MS) in food-omics. 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class="js-work-strip profile--work_container" data-work-id="114405660"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/114405660/Adding_extra_dimensions_to_Tea_Camellia_sinensis_L_volatiles_profiling_by_GC_GC_TOF_MS_and_soft_electron_ionization_effects_of_climate_changes_on_volatile_metabolome"><img alt="Research paper thumbnail of Adding extra-dimensions to Tea (Camellia sinensis L.) volatiles profiling by GC×GC-TOF-MS and soft electron ionization: effects of climate changes on volatile metabolome" class="work-thumbnail" src="https://attachments.academia-assets.com/111112290/thumbnails/1.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/114405660/Adding_extra_dimensions_to_Tea_Camellia_sinensis_L_volatiles_profiling_by_GC_GC_TOF_MS_and_soft_electron_ionization_effects_of_climate_changes_on_volatile_metabolome">Adding extra-dimensions to Tea (Camellia sinensis L.) volatiles profiling by GC×GC-TOF-MS and soft electron ionization: effects of climate changes on volatile metabolome</a></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">SUBMISSION FORM To be sent by July 31st, 2017 to http://www.spettrometriadimassa.it/Congressi/5MS...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">SUBMISSION FORM To be sent by July 31st, 2017 to <a href="http://www.spettrometriadimassa.it/Congressi/5MS-FoodDay/5MSFoodDay_SubmissionForm.php" rel="nofollow">http://www.spettrometriadimassa.it/Congressi/5MS-FoodDay/5MSFoodDay_SubmissionForm.php</a> Presenting Author Marta Cialiè Rosso Università degli Studi di Torino Dipartimento di Scienza e Tecnologia del Farmaco Via Pietro Giuria 9 10125 Torino Italia 0039 0116707172 Fax <a href="mailto:marta.cialierosso@unito.it" rel="nofollow">marta.cialierosso@unito.it</a> Preference:  Oral presentation X Poster Adding extra-dimensions to Tea (Camellia sinensis L.) volatiles profiling by GC×GC-TOF-MS and soft electron ionization: effects of climate changes on volatile metabolome Marta Cialiè Rosso1, Erica Liberto1, Albert Robbat2, Laura Mc Gregor3, Nick Bukowski3, Carlo Bicchi1 and Chiara Cordero1 1 Dipartimento di Scienza e Tecnologia del Farmaco, Università degli Studi di Torino, Torino, Italy 2 Department of Chemistry, Tufts University, Medford, MA, USA 3 Markes International Ltd, Llantrisant, RCT, UK Adding extra-dimensions to Tea (Camellia sinensis L.) volatiles profiling by 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on metals in tea (Camelia sinensis (L.) Kuntze)" class="work-thumbnail" src="https://attachments.academia-assets.com/111112311/thumbnails/1.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/114405659/2014_2016_seasonal_rainfall_effects_on_metals_in_tea_Camelia_sinensis_L_Kuntze_">2014–2016 seasonal rainfall effects on metals in tea (Camelia sinensis (L.) Kuntze)</a></div><div class="wp-workCard_item"><span>Chemosphere</span><span>, 2018</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><a id="0c0a56094409981b77a3b145bb4e96d5" class="wp-workCard--action" rel="nofollow" data-click-track="profile-work-strip-download" data-download="{"attachment_id":111112311,"asset_id":114405659,"asset_type":"Work","button_location":"profile"}" href="https://www.academia.edu/attachments/111112311/download_file?st=MTczMjQyMzk5MSw4LjIyMi4yMDguMTQ2&s=profile"><span><i class="fa fa-arrow-down"></i></span><span>Download</span></a><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="114405659"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="114405659"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 114405659; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=114405659]").text(description); $(".js-view-count[data-work-id=114405659]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 114405659; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='114405659']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 114405659, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (true){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "0c0a56094409981b77a3b145bb4e96d5" } } $('.js-work-strip[data-work-id=114405659]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":114405659,"title":"2014–2016 seasonal rainfall effects on metals in tea (Camelia sinensis (L.) Kuntze)","translated_title":"","metadata":{"publisher":"Elsevier BV","grobid_abstract":"h i g h l i g h t s Metal nutrient concentrations in tea varied in response to climate changes. Concentrations of Fe, Ca, Mg, Mn, Al and Ba were higher in monsoon tea. Concentrations of Pb, K, Cu, Zn, and Na were higher in pre-and post-monsoon tea. Sensory analysis revealed no metallic taste in environmental and commercial teas.","publication_date":{"day":null,"month":null,"year":2018,"errors":{}},"publication_name":"Chemosphere","grobid_abstract_attachment_id":111112311},"translated_abstract":null,"internal_url":"https://www.academia.edu/114405659/2014_2016_seasonal_rainfall_effects_on_metals_in_tea_Camelia_sinensis_L_Kuntze_","translated_internal_url":"","created_at":"2024-02-02T19:29:30.227-08:00","preview_url":null,"current_user_can_edit":null,"current_user_is_owner":null,"owner_id":35681884,"coauthors_can_edit":true,"document_type":"paper","co_author_tags":[],"downloadable_attachments":[{"id":111112311,"title":"","file_type":"pdf","scribd_thumbnail_url":"https://attachments.academia-assets.com/111112311/thumbnails/1.jpg","file_name":"j.chemosphere.2018.12.07520240203-1-xc7m9t.pdf","download_url":"https://www.academia.edu/attachments/111112311/download_file?st=MTczMjQyMzk5MSw4LjIyMi4yMDguMTQ2&","bulk_download_file_name":"2014_2016_seasonal_rainfall_effects_on_m.pdf","bulk_download_url":"https://d1wqtxts1xzle7.cloudfront.net/111112311/j.chemosphere.2018.12.07520240203-1-xc7m9t-libre.pdf?1706931627=\u0026response-content-disposition=attachment%3B+filename%3D2014_2016_seasonal_rainfall_effects_on_m.pdf\u0026Expires=1732427591\u0026Signature=JJAwq3UMescq8YSUoeKolLdlewQOY6OwQX8L0TICwpZ4EYjiYzBNQZe46WQ7ydFm9sQuSsc9hHv5uG9dNs~y5hPOsSfgwB2wjhB1YZunoSBzpvUVLi3JjKVRBrAuRnJ2Jl3xrqc4xtW3eHL5LUZvbHPJLatsKSFNHpWXBGOA6P6Fti8G~CbskI8sjjBUPP6~m0vViHuMOl4EZH7eSwlR~QMfwt1DdRzPcsuzzRv12cVO5eJWlqqg95~sgmPWTEuLqUov~f~lYwnRjbG3rUthkUFUPWwsVO9XBWDNq9e~IaduIlL88m9s7ItwjvKUwaaFL-5aHZc~3fSa~-Y4NPY8cg__\u0026Key-Pair-Id=APKAJLOHF5GGSLRBV4ZA"}],"slug":"2014_2016_seasonal_rainfall_effects_on_metals_in_tea_Camelia_sinensis_L_Kuntze_","translated_slug":"","page_count":8,"language":"en","content_type":"Work","owner":{"id":35681884,"first_name":"Albert","middle_initials":null,"last_name":"Robbat","page_name":"AlbertRobbat","domain_name":"tufts","created_at":"2015-10-05T06:36:59.544-07:00","display_name":"Albert Robbat","url":"https://tufts.academia.edu/AlbertRobbat"},"attachments":[{"id":111112311,"title":"","file_type":"pdf","scribd_thumbnail_url":"https://attachments.academia-assets.com/111112311/thumbnails/1.jpg","file_name":"j.chemosphere.2018.12.07520240203-1-xc7m9t.pdf","download_url":"https://www.academia.edu/attachments/111112311/download_file?st=MTczMjQyMzk5MSw4LjIyMi4yMDguMTQ2&","bulk_download_file_name":"2014_2016_seasonal_rainfall_effects_on_m.pdf","bulk_download_url":"https://d1wqtxts1xzle7.cloudfront.net/111112311/j.chemosphere.2018.12.07520240203-1-xc7m9t-libre.pdf?1706931627=\u0026response-content-disposition=attachment%3B+filename%3D2014_2016_seasonal_rainfall_effects_on_m.pdf\u0026Expires=1732427591\u0026Signature=JJAwq3UMescq8YSUoeKolLdlewQOY6OwQX8L0TICwpZ4EYjiYzBNQZe46WQ7ydFm9sQuSsc9hHv5uG9dNs~y5hPOsSfgwB2wjhB1YZunoSBzpvUVLi3JjKVRBrAuRnJ2Jl3xrqc4xtW3eHL5LUZvbHPJLatsKSFNHpWXBGOA6P6Fti8G~CbskI8sjjBUPP6~m0vViHuMOl4EZH7eSwlR~QMfwt1DdRzPcsuzzRv12cVO5eJWlqqg95~sgmPWTEuLqUov~f~lYwnRjbG3rUthkUFUPWwsVO9XBWDNq9e~IaduIlL88m9s7ItwjvKUwaaFL-5aHZc~3fSa~-Y4NPY8cg__\u0026Key-Pair-Id=APKAJLOHF5GGSLRBV4ZA"}],"research_interests":[{"id":523,"name":"Chemistry","url":"https://www.academia.edu/Documents/in/Chemistry"},{"id":26327,"name":"Medicine","url":"https://www.academia.edu/Documents/in/Medicine"},{"id":28235,"name":"Multidisciplinary","url":"https://www.academia.edu/Documents/in/Multidisciplinary"},{"id":40032,"name":"Monsoon","url":"https://www.academia.edu/Documents/in/Monsoon"},{"id":540337,"name":"Flavor","url":"https://www.academia.edu/Documents/in/Flavor"},{"id":864424,"name":"Micronutrient","url":"https://www.academia.edu/Documents/in/Micronutrient"}],"urls":[{"id":39145390,"url":"https://api.elsevier.com/content/article/PII:S004565351832397X?httpAccept=text/xml"}]}, dispatcherData: dispatcherData }); $(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="114405658"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/114405658/Electrodeposition_of_Metal_Alloy_and_Mixed_Oxide_Films_Using_a_Single_Precursor_Tetranuclear_Copper_Nickel_Complex"><img alt="Research paper thumbnail of Electrodeposition of Metal Alloy and Mixed Oxide Films Using a Single‐Precursor Tetranuclear Copper‐Nickel Complex" class="work-thumbnail" src="https://attachments.academia-assets.com/111112317/thumbnails/1.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/114405658/Electrodeposition_of_Metal_Alloy_and_Mixed_Oxide_Films_Using_a_Single_Precursor_Tetranuclear_Copper_Nickel_Complex">Electrodeposition of Metal Alloy and Mixed Oxide Films Using a Single‐Precursor Tetranuclear Copper‐Nickel Complex</a></div><div class="wp-workCard_item"><span>Journal of The Electrochemical Society</span><span>, 1995</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><a id="067aadc124f1f7b34665d3ee11e0a38a" class="wp-workCard--action" rel="nofollow" data-click-track="profile-work-strip-download" data-download="{"attachment_id":111112317,"asset_id":114405658,"asset_type":"Work","button_location":"profile"}" href="https://www.academia.edu/attachments/111112317/download_file?st=MTczMjQyMzk5MSw4LjIyMi4yMDguMTQ2&s=profile"><span><i class="fa fa-arrow-down"></i></span><span>Download</span></a><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="114405658"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="114405658"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 114405658; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=114405658]").text(description); $(".js-view-count[data-work-id=114405658]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 114405658; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='114405658']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 114405658, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (true){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); 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The alloy deposition potential is invariant with complex stoichiometry. Alloy Ni composition, determined by x-ray diffraction (XRD), increases from 12% for x = 1 to 62% for x = 4. The microscopically rough, well-adhering, continuous films have a natural passivation layer formed by air oxidation that consists of Ni(OH)2, NiO, Cu(OH)2, and Cu20. X-ray photoelectron spectroscopy confirmed the bulk film alloy compositions obtained by XRD. The data revealed complex deposit structures consisting of NiO, Ni(OH)2, Cu20, and Cu-Ni alloy giving a mass balance of the metals in the complexes. The Cu20/Cu ~ ratio is close to unity for the deposit made from the Cu4 complex and decreases to zero for the CuNi3 complex. In contrast only half of the Ni(II) centers are deposited as Ni ~ in the Cu-Ni alloy, the balance consisting of 37% NiO and 15% Ni(OH)2. The constant percentage of Ni as Ni(OH)2 in all deposits suggests that it arises from reduction of Ni coordinated water. Mass balance indicates O in Cu20 and NiO originates from the ~4-O. Smooth variations of alloy compositions, metal oxide/metal ratios, and film particle sizes indicate that all the electrode processes involve discrete molecules of the heteropolymetallic complex.","publication_date":{"day":null,"month":null,"year":1995,"errors":{}},"publication_name":"Journal of The Electrochemical Society","grobid_abstract_attachment_id":111112317},"translated_abstract":null,"internal_url":"https://www.academia.edu/114405658/Electrodeposition_of_Metal_Alloy_and_Mixed_Oxide_Films_Using_a_Single_Precursor_Tetranuclear_Copper_Nickel_Complex","translated_internal_url":"","created_at":"2024-02-02T19:29:29.781-08:00","preview_url":null,"current_user_can_edit":null,"current_user_is_owner":null,"owner_id":35681884,"coauthors_can_edit":true,"document_type":"paper","co_author_tags":[],"downloadable_attachments":[{"id":111112317,"title":"","file_type":"pdf","scribd_thumbnail_url":"https://attachments.academia-assets.com/111112317/thumbnails/1.jpg","file_name":"Dube-Workie_Kounaves_20JES_201995v142p3357.pdf","download_url":"https://www.academia.edu/attachments/111112317/download_file?st=MTczMjQyMzk5MSw4LjIyMi4yMDguMTQ2&","bulk_download_file_name":"Electrodeposition_of_Metal_Alloy_and_Mix.pdf","bulk_download_url":"https://d1wqtxts1xzle7.cloudfront.net/111112317/Dube-Workie_Kounaves_20JES_201995v142p3357-libre.pdf?1706931632=\u0026response-content-disposition=attachment%3B+filename%3DElectrodeposition_of_Metal_Alloy_and_Mix.pdf\u0026Expires=1732427591\u0026Signature=PzUEshgrm7bvfyeoQhBKdmkCuSLJKUgf3cFdnENC6qow2kRM9O3UGABN3pLPV-DNXQ4-o5exbevbNrr4tnxZCQXYy09lsgrbtLbOBdr8Yh8yOoKP4LQyUVQkaw0RQcYVCG8IGK0KTI6Oluj3C6-YgjFGKea-ZzHwNNU56LS2zFXAi4xVXwzK8W2eans0Hbz4A0qQa5ZUvN~wF-pRYXhZznSUz~HWk1o4TcH~ONoNlYMLri461zRE1-ppW5abWoIeVlCP3wxyd4mWxBpyr8bTPPD2lKwKj1WmZbRQDdHO4UGE5hqGeDIDgfdoAW1819doCJp7eQwf-m1uSWIOuyS~nA__\u0026Key-Pair-Id=APKAJLOHF5GGSLRBV4ZA"}],"slug":"Electrodeposition_of_Metal_Alloy_and_Mixed_Oxide_Films_Using_a_Single_Precursor_Tetranuclear_Copper_Nickel_Complex","translated_slug":"","page_count":9,"language":"en","content_type":"Work","owner":{"id":35681884,"first_name":"Albert","middle_initials":null,"last_name":"Robbat","page_name":"AlbertRobbat","domain_name":"tufts","created_at":"2015-10-05T06:36:59.544-07:00","display_name":"Albert 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$(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="114405657"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/114405657/Gas_chromatographic_retention_characteristics_of_phenols_with_Superox_20M"><img alt="Research paper thumbnail of Gas chromatographic retention characteristics of phenols with Superox-20M" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/114405657/Gas_chromatographic_retention_characteristics_of_phenols_with_Superox_20M">Gas chromatographic retention characteristics of phenols with Superox-20M</a></div><div class="wp-workCard_item"><span>Analytical Chemistry</span><span>, 1982</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">The gas chromatographic retention characteristics of a variety of underivatized phenols have been...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">The gas chromatographic retention characteristics of a variety of underivatized phenols have been studied by using Superox-20M coated on fused silica. The relative retention times of thes compounds were measured at 160, 150, and 140/sup 0/C in order to determine the effect of operating temperature on relative retention. This information is used to predict relative retention times of phenols for which we had no standards. The linear temperature-programmed retention indexes of the solutes were measured. The retention of phenols on this phase is a function of the compounds vapor pressure, its ability to hydrogen bond with the stationary phase, and the strengths of those hydrogen bonds. These properties are in turn governed by steric, inductive, and resonance effects of the substituents. Linear free-energy relations between the logarithm of the ratio of the activity coefficients of phenol to substituted phenol (calculated from relative retention data) and the chromatographic substituent constant, sigma/sub c/, have been determined for some phenols on Superox-20M. Lastly, it was shown by nuclear magnetic resonance experiments that Superox-20M is apparently a poly(ethylene glycol) (also called a polyoxiran or poly(ethylene oxide)). 5 figures, 3 tables.</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="114405657"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="114405657"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 114405657; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=114405657]").text(description); $(".js-view-count[data-work-id=114405657]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 114405657; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='114405657']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 114405657, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=114405657]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":114405657,"title":"Gas chromatographic retention characteristics of phenols with Superox-20M","translated_title":"","metadata":{"abstract":"The gas chromatographic retention characteristics of a variety of underivatized phenols have been studied by using Superox-20M coated on fused silica. The relative retention times of thes compounds were measured at 160, 150, and 140/sup 0/C in order to determine the effect of operating temperature on relative retention. This information is used to predict relative retention times of phenols for which we had no standards. The linear temperature-programmed retention indexes of the solutes were measured. The retention of phenols on this phase is a function of the compounds vapor pressure, its ability to hydrogen bond with the stationary phase, and the strengths of those hydrogen bonds. These properties are in turn governed by steric, inductive, and resonance effects of the substituents. Linear free-energy relations between the logarithm of the ratio of the activity coefficients of phenol to substituted phenol (calculated from relative retention data) and the chromatographic substituent constant, sigma/sub c/, have been determined for some phenols on Superox-20M. Lastly, it was shown by nuclear magnetic resonance experiments that Superox-20M is apparently a poly(ethylene glycol) (also called a polyoxiran or poly(ethylene oxide)). 5 figures, 3 tables.","publisher":"American Chemical Society (ACS)","publication_date":{"day":null,"month":null,"year":1982,"errors":{}},"publication_name":"Analytical Chemistry"},"translated_abstract":"The gas chromatographic retention characteristics of a variety of underivatized phenols have been studied by using Superox-20M coated on fused silica. The relative retention times of thes compounds were measured at 160, 150, and 140/sup 0/C in order to determine the effect of operating temperature on relative retention. This information is used to predict relative retention times of phenols for which we had no standards. The linear temperature-programmed retention indexes of the solutes were measured. The retention of phenols on this phase is a function of the compounds vapor pressure, its ability to hydrogen bond with the stationary phase, and the strengths of those hydrogen bonds. These properties are in turn governed by steric, inductive, and resonance effects of the substituents. Linear free-energy relations between the logarithm of the ratio of the activity coefficients of phenol to substituted phenol (calculated from relative retention data) and the chromatographic substituent constant, sigma/sub c/, have been determined for some phenols on Superox-20M. Lastly, it was shown by nuclear magnetic resonance experiments that Superox-20M is apparently a poly(ethylene glycol) (also called a polyoxiran or poly(ethylene oxide)). 5 figures, 3 tables.","internal_url":"https://www.academia.edu/114405657/Gas_chromatographic_retention_characteristics_of_phenols_with_Superox_20M","translated_internal_url":"","created_at":"2024-02-02T19:29:29.196-08:00","preview_url":null,"current_user_can_edit":null,"current_user_is_owner":null,"owner_id":35681884,"coauthors_can_edit":true,"document_type":"paper","co_author_tags":[],"downloadable_attachments":[],"slug":"Gas_chromatographic_retention_characteristics_of_phenols_with_Superox_20M","translated_slug":"","page_count":null,"language":"en","content_type":"Work","owner":{"id":35681884,"first_name":"Albert","middle_initials":null,"last_name":"Robbat","page_name":"AlbertRobbat","domain_name":"tufts","created_at":"2015-10-05T06:36:59.544-07:00","display_name":"Albert Robbat","url":"https://tufts.academia.edu/AlbertRobbat"},"attachments":[],"research_interests":[{"id":72,"name":"Chemical Engineering","url":"https://www.academia.edu/Documents/in/Chemical_Engineering"},{"id":523,"name":"Chemistry","url":"https://www.academia.edu/Documents/in/Chemistry"},{"id":524,"name":"Analytical Chemistry","url":"https://www.academia.edu/Documents/in/Analytical_Chemistry"},{"id":4656,"name":"Chromatography","url":"https://www.academia.edu/Documents/in/Chromatography"},{"id":7333,"name":"Nuclear Magnetic Resonance","url":"https://www.academia.edu/Documents/in/Nuclear_Magnetic_Resonance"},{"id":114713,"name":"Vapor Pressure","url":"https://www.academia.edu/Documents/in/Vapor_Pressure"},{"id":166448,"name":"Gas Chromatography","url":"https://www.academia.edu/Documents/in/Gas_Chromatography"},{"id":216526,"name":"Free Energy","url":"https://www.academia.edu/Documents/in/Free_Energy"},{"id":347988,"name":"Phenols","url":"https://www.academia.edu/Documents/in/Phenols"},{"id":875404,"name":"Retention Time","url":"https://www.academia.edu/Documents/in/Retention_Time"},{"id":2066593,"name":"Retention Index","url":"https://www.academia.edu/Documents/in/Retention_Index"}],"urls":[{"id":39145388,"url":"https://pubs.acs.org/doi/pdf/10.1021/ac00246a024"}]}, dispatcherData: dispatcherData }); 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$(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="104817529"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" rel="nofollow" href="https://www.academia.edu/104817529/Resource_Development_in_the_Analytical_Chemistry_of_Sulfur_Compounds_for_the_New_Coal_Conversion_Technologies"><img alt="Research paper thumbnail of Resource Development in the Analytical Chemistry of Sulfur Compounds for the New Coal Conversion Technologies" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" rel="nofollow" href="https://www.academia.edu/104817529/Resource_Development_in_the_Analytical_Chemistry_of_Sulfur_Compounds_for_the_New_Coal_Conversion_Technologies">Resource Development in the Analytical Chemistry of Sulfur Compounds for the New Coal Conversion Technologies</a></div><div class="wp-workCard_item"><span>ACS Symposium Series</span><span>, 1981</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="104817529"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="104817529"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 104817529; 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$(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="90409488"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/90409488/The_Chemistry_of_Green_and_Roasted_Coffee_by_Selectable_1D_2D_Gas_Chromatography_Mass_Spectrometry_with_Spectral_Deconvolution"><img alt="Research paper thumbnail of The Chemistry of Green and Roasted Coffee by Selectable 1D/2D Gas Chromatography Mass Spectrometry with Spectral Deconvolution" class="work-thumbnail" src="https://attachments.academia-assets.com/93980698/thumbnails/1.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/90409488/The_Chemistry_of_Green_and_Roasted_Coffee_by_Selectable_1D_2D_Gas_Chromatography_Mass_Spectrometry_with_Spectral_Deconvolution">The Chemistry of Green and Roasted Coffee by Selectable 1D/2D Gas Chromatography Mass Spectrometry with Spectral Deconvolution</a></div><div class="wp-workCard_item"><span>Molecules</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">Gas chromatography/mass spectrometry (GC/MS) is a long-standing technique for the analysis of vol...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">Gas chromatography/mass spectrometry (GC/MS) is a long-standing technique for the analysis of volatile organic compounds (VOCs). When coupled with the Ion Analytics software, GC/MS provides unmatched selectivity in the analysis of complex mixtures and it reduces the reliance on high-resolution chromatography to obtain clean mass spectra. Here, we present an application of spectral deconvolution, with mass spectral subtraction, to identify a wide array of VOCs in green and roasted coffees. Automated sequential, two-dimensional GC-GC/MS of a roasted coffee sample produced the retention index and spectrum of 750 compounds. These initial analytes served as targets for subsequent coffee analysis by GC/MS. The workflow resulted in the quantitation of 511 compounds detected in two different green and roasted coffees. Of these, over 100 compounds serve as candidate differentiators of coffee quality, AAA vs. AA, as designated by the Coopedota cooperative in Costa Rica. Of these, 72 compounds...</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><a id="cde1c36c6300c868ccfd7ef6ab9f2d5b" class="wp-workCard--action" rel="nofollow" data-click-track="profile-work-strip-download" data-download="{"attachment_id":93980698,"asset_id":90409488,"asset_type":"Work","button_location":"profile"}" href="https://www.academia.edu/attachments/93980698/download_file?st=MTczMjQyMzk5MSw4LjIyMi4yMDguMTQ2&s=profile"><span><i class="fa fa-arrow-down"></i></span><span>Download</span></a><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="90409488"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="90409488"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 90409488; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=90409488]").text(description); $(".js-view-count[data-work-id=90409488]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 90409488; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='90409488']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 90409488, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (true){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "cde1c36c6300c868ccfd7ef6ab9f2d5b" } } $('.js-work-strip[data-work-id=90409488]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":90409488,"title":"The Chemistry of Green and Roasted Coffee by Selectable 1D/2D Gas Chromatography Mass Spectrometry with Spectral Deconvolution","translated_title":"","metadata":{"abstract":"Gas chromatography/mass spectrometry (GC/MS) is a long-standing technique for the analysis of volatile organic compounds (VOCs). When coupled with the Ion Analytics software, GC/MS provides unmatched selectivity in the analysis of complex mixtures and it reduces the reliance on high-resolution chromatography to obtain clean mass spectra. Here, we present an application of spectral deconvolution, with mass spectral subtraction, to identify a wide array of VOCs in green and roasted coffees. Automated sequential, two-dimensional GC-GC/MS of a roasted coffee sample produced the retention index and spectrum of 750 compounds. These initial analytes served as targets for subsequent coffee analysis by GC/MS. The workflow resulted in the quantitation of 511 compounds detected in two different green and roasted coffees. Of these, over 100 compounds serve as candidate differentiators of coffee quality, AAA vs. AA, as designated by the Coopedota cooperative in Costa Rica. Of these, 72 compounds...","publisher":"MDPI AG","publication_name":"Molecules"},"translated_abstract":"Gas chromatography/mass spectrometry (GC/MS) is a long-standing technique for the analysis of volatile organic compounds (VOCs). When coupled with the Ion Analytics software, GC/MS provides unmatched selectivity in the analysis of complex mixtures and it reduces the reliance on high-resolution chromatography to obtain clean mass spectra. Here, we present an application of spectral deconvolution, with mass spectral subtraction, to identify a wide array of VOCs in green and roasted coffees. Automated sequential, two-dimensional GC-GC/MS of a roasted coffee sample produced the retention index and spectrum of 750 compounds. These initial analytes served as targets for subsequent coffee analysis by GC/MS. The workflow resulted in the quantitation of 511 compounds detected in two different green and roasted coffees. Of these, over 100 compounds serve as candidate differentiators of coffee quality, AAA vs. AA, as designated by the Coopedota cooperative in Costa Rica. 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$(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="90409485"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/90409485/Electrocatalytic_decomposition_of_hydrogen_sulfide"><img alt="Research paper thumbnail of Electrocatalytic decomposition of hydrogen sulfide" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/90409485/Electrocatalytic_decomposition_of_hydrogen_sulfide">Electrocatalytic decomposition of hydrogen sulfide</a></div><div class="wp-workCard_item"><span>Catalysis Letters</span><span>, 1992</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">ABSTRACT The recently discovered phenomenon of nonfaradaic electrochemical modification of cataly...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">ABSTRACT The recently discovered phenomenon of nonfaradaic electrochemical modification of catalytic activity (NEMCA) was explored for the electrocatalytic decomposition of H2S to H2 and S2 over Pt electrodes at 600–750 C and 1 atm. It was found that upon applying a potential to Pt supported on a O2– conducting yttria-stabilized zirconia disk, the decompoition of H2S significantly increased up to a factor of 11 at 600 C. The results appear to verify several aspects of NEMCA including the phenomenon that the electrolyte needs not to conduct reaction-specific species and that the degree of rate enhancement is related to the working electrode polarization. In addition, results indicate that separate chambers are not always required for electrocatalysis.</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="90409485"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="90409485"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 90409485; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=90409485]").text(description); $(".js-view-count[data-work-id=90409485]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 90409485; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='90409485']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 90409485, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=90409485]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":90409485,"title":"Electrocatalytic decomposition of hydrogen sulfide","translated_title":"","metadata":{"abstract":"ABSTRACT The recently discovered phenomenon of nonfaradaic electrochemical modification of catalytic activity (NEMCA) was explored for the electrocatalytic decomposition of H2S to H2 and S2 over Pt electrodes at 600–750 C and 1 atm. It was found that upon applying a potential to Pt supported on a O2– conducting yttria-stabilized zirconia disk, the decompoition of H2S significantly increased up to a factor of 11 at 600 C. The results appear to verify several aspects of NEMCA including the phenomenon that the electrolyte needs not to conduct reaction-specific species and that the degree of rate enhancement is related to the working electrode polarization. In addition, results indicate that separate chambers are not always required for electrocatalysis.","publisher":"Springer Science and Business Media LLC","publication_date":{"day":null,"month":null,"year":1992,"errors":{}},"publication_name":"Catalysis Letters"},"translated_abstract":"ABSTRACT The recently discovered phenomenon of nonfaradaic electrochemical modification of catalytic activity (NEMCA) was explored for the electrocatalytic decomposition of H2S to H2 and S2 over Pt electrodes at 600–750 C and 1 atm. It was found that upon applying a potential to Pt supported on a O2– conducting yttria-stabilized zirconia disk, the decompoition of H2S significantly increased up to a factor of 11 at 600 C. The results appear to verify several aspects of NEMCA including the phenomenon that the electrolyte needs not to conduct reaction-specific species and that the degree of rate enhancement is related to the working electrode polarization. In addition, results indicate that separate chambers are not always required for electrocatalysis.","internal_url":"https://www.academia.edu/90409485/Electrocatalytic_decomposition_of_hydrogen_sulfide","translated_internal_url":"","created_at":"2022-11-09T17:52:06.386-08:00","preview_url":null,"current_user_can_edit":null,"current_user_is_owner":null,"owner_id":35681884,"coauthors_can_edit":true,"document_type":"paper","co_author_tags":[],"downloadable_attachments":[],"slug":"Electrocatalytic_decomposition_of_hydrogen_sulfide","translated_slug":"","page_count":null,"language":"en","content_type":"Work","owner":{"id":35681884,"first_name":"Albert","middle_initials":null,"last_name":"Robbat","page_name":"AlbertRobbat","domain_name":"tufts","created_at":"2015-10-05T06:36:59.544-07:00","display_name":"Albert Robbat","url":"https://tufts.academia.edu/AlbertRobbat"},"attachments":[],"research_interests":[{"id":72,"name":"Chemical Engineering","url":"https://www.academia.edu/Documents/in/Chemical_Engineering"},{"id":523,"name":"Chemistry","url":"https://www.academia.edu/Documents/in/Chemistry"},{"id":530,"name":"Inorganic Chemistry","url":"https://www.academia.edu/Documents/in/Inorganic_Chemistry"},{"id":4748,"name":"Electrochemistry","url":"https://www.academia.edu/Documents/in/Electrochemistry"},{"id":4749,"name":"Catalysis","url":"https://www.academia.edu/Documents/in/Catalysis"},{"id":6414,"name":"Decomposition","url":"https://www.academia.edu/Documents/in/Decomposition"},{"id":476869,"name":"Hydrogen Sulfide","url":"https://www.academia.edu/Documents/in/Hydrogen_Sulfide"},{"id":1276642,"name":"Electrolyte","url":"https://www.academia.edu/Documents/in/Electrolyte"},{"id":1277798,"name":"Catalytic Activity","url":"https://www.academia.edu/Documents/in/Catalytic_Activity"},{"id":1419009,"name":"Electrocatalyst","url":"https://www.academia.edu/Documents/in/Electrocatalyst"}],"urls":[{"id":25773165,"url":"http://link.springer.com/content/pdf/10.1007/BF00771002.pdf"}]}, dispatcherData: dispatcherData }); $(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> </div><div class="profile--tab_content_container js-tab-pane tab-pane" data-section-id="3681675" id="papers"><div class="js-work-strip profile--work_container" data-work-id="114405672"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/114405672/Fast_gas_chromatography_mass_spectrometry_analysis_in_support_of_risk_based_decisions"><img alt="Research paper thumbnail of Fast gas chromatography/mass spectrometry analysis in support of risk‐based decisions" class="work-thumbnail" src="https://attachments.academia-assets.com/111112312/thumbnails/1.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/114405672/Fast_gas_chromatography_mass_spectrometry_analysis_in_support_of_risk_based_decisions">Fast gas chromatography/mass spectrometry analysis in support of risk‐based decisions</a></div><div class="wp-workCard_item"><span>Field Analytical Chemistry and Technology</span><span>, 1999</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><a id="1eb1feff5185e7f2d8fd07eb38643192" class="wp-workCard--action" rel="nofollow" data-click-track="profile-work-strip-download" data-download="{"attachment_id":111112312,"asset_id":114405672,"asset_type":"Work","button_location":"profile"}" href="https://www.academia.edu/attachments/111112312/download_file?st=MTczMjQyMzk5MSw4LjIyMi4yMDguMTQ2&st=MTczMjQyMzk5MCw4LjIyMi4yMDguMTQ2&s=profile"><span><i class="fa fa-arrow-down"></i></span><span>Download</span></a><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="114405672"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="114405672"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 114405672; 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$(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="114405670"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/114405670/Electrocatalytic_decomposition_of_hydrogen_sulfide"><img alt="Research paper thumbnail of Electrocatalytic decomposition of hydrogen sulfide" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/114405670/Electrocatalytic_decomposition_of_hydrogen_sulfide">Electrocatalytic decomposition of hydrogen sulfide</a></div><div class="wp-workCard_item"><span>Catalysis Letters</span><span>, Sep 1, 1992</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">ABSTRACT The recently discovered phenomenon of nonfaradaic electrochemical modification of cataly...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">ABSTRACT The recently discovered phenomenon of nonfaradaic electrochemical modification of catalytic activity (NEMCA) was explored for the electrocatalytic decomposition of H2S to H2 and S2 over Pt electrodes at 600–750 C and 1 atm. It was found that upon applying a potential to Pt supported on a O2– conducting yttria-stabilized zirconia disk, the decompoition of H2S significantly increased up to a factor of 11 at 600 C. The results appear to verify several aspects of NEMCA including the phenomenon that the electrolyte needs not to conduct reaction-specific species and that the degree of rate enhancement is related to the working electrode polarization. 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It was found that upon applying a potential to Pt supported on a O2– conducting yttria-stabilized zirconia disk, the decompoition of H2S significantly increased up to a factor of 11 at 600 C. The results appear to verify several aspects of NEMCA including the phenomenon that the electrolyte needs not to conduct reaction-specific species and that the degree of rate enhancement is related to the working electrode polarization. In addition, results indicate that separate chambers are not always required for electrocatalysis.","publisher":"Springer Science+Business Media","publication_date":{"day":1,"month":9,"year":1992,"errors":{}},"publication_name":"Catalysis Letters"},"translated_abstract":"ABSTRACT The recently discovered phenomenon of nonfaradaic electrochemical modification of catalytic activity (NEMCA) was explored for the electrocatalytic decomposition of H2S to H2 and S2 over Pt electrodes at 600–750 C and 1 atm. It was found that upon applying a potential to Pt supported on a O2– conducting yttria-stabilized zirconia disk, the decompoition of H2S significantly increased up to a factor of 11 at 600 C. The results appear to verify several aspects of NEMCA including the phenomenon that the electrolyte needs not to conduct reaction-specific species and that the degree of rate enhancement is related to the working electrode polarization. In addition, results indicate that separate chambers are not always required for electrocatalysis.","internal_url":"https://www.academia.edu/114405670/Electrocatalytic_decomposition_of_hydrogen_sulfide","translated_internal_url":"","created_at":"2024-02-02T19:29:33.131-08:00","preview_url":null,"current_user_can_edit":null,"current_user_is_owner":null,"owner_id":35681884,"coauthors_can_edit":true,"document_type":"paper","co_author_tags":[],"downloadable_attachments":[],"slug":"Electrocatalytic_decomposition_of_hydrogen_sulfide","translated_slug":"","page_count":null,"language":"en","content_type":"Work","owner":{"id":35681884,"first_name":"Albert","middle_initials":null,"last_name":"Robbat","page_name":"AlbertRobbat","domain_name":"tufts","created_at":"2015-10-05T06:36:59.544-07:00","display_name":"Albert Robbat","url":"https://tufts.academia.edu/AlbertRobbat"},"attachments":[],"research_interests":[{"id":72,"name":"Chemical Engineering","url":"https://www.academia.edu/Documents/in/Chemical_Engineering"},{"id":523,"name":"Chemistry","url":"https://www.academia.edu/Documents/in/Chemistry"},{"id":530,"name":"Inorganic Chemistry","url":"https://www.academia.edu/Documents/in/Inorganic_Chemistry"},{"id":4748,"name":"Electrochemistry","url":"https://www.academia.edu/Documents/in/Electrochemistry"},{"id":4749,"name":"Catalysis","url":"https://www.academia.edu/Documents/in/Catalysis"},{"id":6414,"name":"Decomposition","url":"https://www.academia.edu/Documents/in/Decomposition"},{"id":11648,"name":"Organometallic Chemistry","url":"https://www.academia.edu/Documents/in/Organometallic_Chemistry"},{"id":476869,"name":"Hydrogen Sulfide","url":"https://www.academia.edu/Documents/in/Hydrogen_Sulfide"},{"id":1276642,"name":"Electrolyte","url":"https://www.academia.edu/Documents/in/Electrolyte"},{"id":1277798,"name":"Catalytic Activity","url":"https://www.academia.edu/Documents/in/Catalytic_Activity"},{"id":1419009,"name":"Electrocatalyst","url":"https://www.academia.edu/Documents/in/Electrocatalyst"}],"urls":[{"id":39145399,"url":"https://doi.org/10.1007/bf00771002"}]}, dispatcherData: dispatcherData }); $(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="114405669"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/114405669/Hazardous_Waste_Site_Investigation_and_Cleanup_Innovative_Technologies_an_Alternative_Approach"><img alt="Research paper thumbnail of Hazardous Waste Site Investigation and Cleanup: Innovative Technologies, an Alternative Approach" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/114405669/Hazardous_Waste_Site_Investigation_and_Cleanup_Innovative_Technologies_an_Alternative_Approach">Hazardous Waste Site Investigation and Cleanup: Innovative Technologies, an Alternative Approach</a></div><div class="wp-workCard_item"><span>Hazardous waste and hazardous materials</span><span>, 1994</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">Much has been made about the high costs associated with hazardous waste site investigations and c...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">Much has been made about the high costs associated with hazardous waste site investigations and cleanup. Independent organizations estimate that the current annual environmental market is $1.8 billion each for environmental engineering firms and commercial laboratory services companies. Clearly, with over 1200 hazardous waste, Superfund sites in EPA`s National Priority LIst (NPL) and with current estimates between 10,000 and 50,000 sites at the NPL funnel awaiting investigation, the nation faces a daunting political, social, and economic challenge. With increasing financial pressures placed on state governments and the recent inclusion of federal facilities into the Superfund process, Congress has finally become aware of the high costs and inefficiencies built into Superfund and in the way EPA conducts the site assessment and cleanup process. Federal funding agencies have focused considerable resources to develop innovative, field-based, analytical technologies that can provide real or near-real time chemical information about the site. Some EPA Regions appear to be out in front of the curve, with major site investigation programs being driven by the integration of innovative technologies. Unfortunately, most of these studies are being conducted on an ad hoc basis and are not universal within the agency. This is also true of DOD and DOE.</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="114405669"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="114405669"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 114405669; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=114405669]").text(description); $(".js-view-count[data-work-id=114405669]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 114405669; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='114405669']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 114405669, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=114405669]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":114405669,"title":"Hazardous Waste Site Investigation and Cleanup: Innovative Technologies, an Alternative Approach","translated_title":"","metadata":{"abstract":"Much has been made about the high costs associated with hazardous waste site investigations and cleanup. Independent organizations estimate that the current annual environmental market is $1.8 billion each for environmental engineering firms and commercial laboratory services companies. Clearly, with over 1200 hazardous waste, Superfund sites in EPA`s National Priority LIst (NPL) and with current estimates between 10,000 and 50,000 sites at the NPL funnel awaiting investigation, the nation faces a daunting political, social, and economic challenge. With increasing financial pressures placed on state governments and the recent inclusion of federal facilities into the Superfund process, Congress has finally become aware of the high costs and inefficiencies built into Superfund and in the way EPA conducts the site assessment and cleanup process. Federal funding agencies have focused considerable resources to develop innovative, field-based, analytical technologies that can provide real or near-real time chemical information about the site. Some EPA Regions appear to be out in front of the curve, with major site investigation programs being driven by the integration of innovative technologies. Unfortunately, most of these studies are being conducted on an ad hoc basis and are not universal within the agency. This is also true of DOD and DOE.","publisher":"Mary Ann Liebert, Inc.","publication_date":{"day":null,"month":null,"year":1994,"errors":{}},"publication_name":"Hazardous waste and hazardous materials"},"translated_abstract":"Much has been made about the high costs associated with hazardous waste site investigations and cleanup. Independent organizations estimate that the current annual environmental market is $1.8 billion each for environmental engineering firms and commercial laboratory services companies. Clearly, with over 1200 hazardous waste, Superfund sites in EPA`s National Priority LIst (NPL) and with current estimates between 10,000 and 50,000 sites at the NPL funnel awaiting investigation, the nation faces a daunting political, social, and economic challenge. With increasing financial pressures placed on state governments and the recent inclusion of federal facilities into the Superfund process, Congress has finally become aware of the high costs and inefficiencies built into Superfund and in the way EPA conducts the site assessment and cleanup process. Federal funding agencies have focused considerable resources to develop innovative, field-based, analytical technologies that can provide real or near-real time chemical information about the site. Some EPA Regions appear to be out in front of the curve, with major site investigation programs being driven by the integration of innovative technologies. Unfortunately, most of these studies are being conducted on an ad hoc basis and are not universal within the agency. This is also true of DOD and DOE.","internal_url":"https://www.academia.edu/114405669/Hazardous_Waste_Site_Investigation_and_Cleanup_Innovative_Technologies_an_Alternative_Approach","translated_internal_url":"","created_at":"2024-02-02T19:29:32.877-08:00","preview_url":null,"current_user_can_edit":null,"current_user_is_owner":null,"owner_id":35681884,"coauthors_can_edit":true,"document_type":"paper","co_author_tags":[],"downloadable_attachments":[],"slug":"Hazardous_Waste_Site_Investigation_and_Cleanup_Innovative_Technologies_an_Alternative_Approach","translated_slug":"","page_count":null,"language":"en","content_type":"Work","owner":{"id":35681884,"first_name":"Albert","middle_initials":null,"last_name":"Robbat","page_name":"AlbertRobbat","domain_name":"tufts","created_at":"2015-10-05T06:36:59.544-07:00","display_name":"Albert Robbat","url":"https://tufts.academia.edu/AlbertRobbat"},"attachments":[],"research_interests":[{"id":48,"name":"Engineering","url":"https://www.academia.edu/Documents/in/Engineering"},{"id":55,"name":"Environmental Engineering","url":"https://www.academia.edu/Documents/in/Environmental_Engineering"},{"id":402,"name":"Environmental Science","url":"https://www.academia.edu/Documents/in/Environmental_Science"},{"id":14085,"name":"Waste Management","url":"https://www.academia.edu/Documents/in/Waste_Management"},{"id":21885,"name":"Hazardous Waste","url":"https://www.academia.edu/Documents/in/Hazardous_Waste"},{"id":74630,"name":"Site Investigation","url":"https://www.academia.edu/Documents/in/Site_Investigation"},{"id":146385,"name":"Land Reclamation","url":"https://www.academia.edu/Documents/in/Land_Reclamation"},{"id":457859,"name":"Cost Benefit Analysis","url":"https://www.academia.edu/Documents/in/Cost_Benefit_Analysis"},{"id":1957240,"name":"ENVIRONMENTAL SCIENCE AND MANAGEMENT","url":"https://www.academia.edu/Documents/in/ENVIRONMENTAL_SCIENCE_AND_MANAGEMENT"}],"urls":[{"id":39145398,"url":"https://doi.org/10.1089/hwm.1994.11.249"}]}, dispatcherData: dispatcherData }); $(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="114405668"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/114405668/Environmental_applications_of_thermal_extraction_cone_penetrometry_and_ultrafast_gas_chromatography_mass_spectrometry"><img alt="Research paper thumbnail of Environmental applications of thermal extraction cone penetrometry and ultrafast gas chromatography/mass spectrometry" class="work-thumbnail" src="https://attachments.academia-assets.com/111112313/thumbnails/1.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/114405668/Environmental_applications_of_thermal_extraction_cone_penetrometry_and_ultrafast_gas_chromatography_mass_spectrometry">Environmental applications of thermal extraction cone penetrometry and ultrafast gas chromatography/mass spectrometry</a></div><div class="wp-workCard_item"><span>Field Analytical Chemistry and Technology</span><span>, 2001</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><a id="405615589c52bba2bc9be6163dd56f81" class="wp-workCard--action" rel="nofollow" data-click-track="profile-work-strip-download" data-download="{"attachment_id":111112313,"asset_id":114405668,"asset_type":"Work","button_location":"profile"}" href="https://www.academia.edu/attachments/111112313/download_file?st=MTczMjQyMzk5MSw4LjIyMi4yMDguMTQ2&st=MTczMjQyMzk5MSw4LjIyMi4yMDguMTQ2&s=profile"><span><i class="fa fa-arrow-down"></i></span><span>Download</span></a><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="114405668"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="114405668"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 114405668; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=114405668]").text(description); $(".js-view-count[data-work-id=114405668]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 114405668; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='114405668']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 114405668, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (true){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "405615589c52bba2bc9be6163dd56f81" } } $('.js-work-strip[data-work-id=114405668]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":114405668,"title":"Environmental applications of thermal extraction cone penetrometry and ultrafast gas chromatography/mass spectrometry","translated_title":"","metadata":{"publisher":"Wiley","grobid_abstract":"This article describes the collection and analysis of organic contaminants at depth without bringing soil to the surface. A thermal extraction cone penetrometer (TECP) probe was used to extract soil-bound semivolatile organics, transferring them to the surface for analysis by ultrafast gas chromatography/mass spectrometry (GC/MS). Findings showed that polychlorinated biphenyls, polycyclic aromatic hydrocarbons, chlorinated pesticides, and explosives could be collected and analyzed in 5 min when the soil-water content was Ͻ20% and in 15 min when it was between 20 and 35%. When the TECP was directly connected to the GC/MS, trinitrotoluene (TNT) and four of its synthetic precursors were speciated in 20 sec. Moreover, 51 VOCs were detected by membrane-inlet mass spectrometry in ϳ10 sec. Organics were \"sniffed\" from a vial and identified using the Ion Fingerprint Detection TM software. 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$(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="114405667"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" rel="nofollow" href="https://www.academia.edu/114405667/Organic_titanium_in_coal_and_the_deposition_of_titanium_on_direct_liquefaction_catalysts"><img alt="Research paper thumbnail of Organic titanium in coal and the deposition of titanium on direct liquefaction catalysts" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" rel="nofollow" href="https://www.academia.edu/114405667/Organic_titanium_in_coal_and_the_deposition_of_titanium_on_direct_liquefaction_catalysts">Organic titanium in coal and the deposition of titanium on direct liquefaction catalysts</a></div><div class="wp-workCard_item"><span>Fuel</span><span>, Dec 1, 1984</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">Abstract Evidence for the presence of soluble organic titanium species in coals and coal-derived ...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">Abstract Evidence for the presence of soluble organic titanium species in coals and coal-derived materials was sought by the application of dialysis procedures. 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chromatographic retention characteristic of polychlorinated biphenyls</a></div><div class="wp-workCard_item"><span>Analytical Chemistry</span><span>, May 15, 1988</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><a id="2536c583647ab7d14280a1ed0e4b6061" class="wp-workCard--action" rel="nofollow" data-click-track="profile-work-strip-download" data-download="{"attachment_id":111112337,"asset_id":114405666,"asset_type":"Work","button_location":"profile"}" href="https://www.academia.edu/attachments/111112337/download_file?st=MTczMjQyMzk5MSw4LjIyMi4yMDguMTQ2&st=MTczMjQyMzk5MSw4LjIyMi4yMDguMTQ2&s=profile"><span><i class="fa fa-arrow-down"></i></span><span>Download</span></a><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="114405666"><a 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electrodes</a></div><div class="wp-workCard_item"><span>Analytical Chemistry</span><span>, 1985</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">Metallographic pretreatment procedures are described which yleid surfaces whose eiectrochemlcaiiy...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">Metallographic pretreatment procedures are described which yleid surfaces whose eiectrochemlcaiiy active areas are Identical wlth their geometrlc areas. 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$(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="114405661"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/114405661/Untargeted_approaches_in_food_omics_The_potential_of_comprehensive_two_dimensional_gas_chromatography_mass_spectrometry"><img alt="Research paper thumbnail of Untargeted approaches in food-omics: The potential of comprehensive two-dimensional gas chromatography/mass spectrometry" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/114405661/Untargeted_approaches_in_food_omics_The_potential_of_comprehensive_two_dimensional_gas_chromatography_mass_spectrometry">Untargeted approaches in food-omics: The potential of comprehensive two-dimensional gas chromatography/mass spectrometry</a></div><div class="wp-workCard_item"><span>TrAC Trends in Analytical Chemistry</span><span>, 2021</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">Abstract The contribution focuses on untargeted data processing/analysis approaches that are curr...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">Abstract The contribution focuses on untargeted data processing/analysis approaches that are currently adopted to explore the 4D-data matrices produced by comprehensive two-dimensional gas chromatography-mass spectrometry (GC × GC-MS) in food-omics. Strategies for untargeted explorations are rationalized through the type of features adopted (i.e., visual, datapoint, peak, and peak-regions) at the data processing level, and then discussed through relevant applications and illustrative examples, selected over peer-reviewed literature. The role of MS, including high vs. low resolution MS, as an active probe for specific cross-comparative analysis, is critically discussed also in the context of spectral deconvolution and subtraction, well-established procedures for 1D GC-MS explorations. Moreover, the challenging task of post-targeting aimed at identifying “unknown – knowns”, is examined in its potential, being the key to access a higher level of information. Selected examples emphasize the importance of reliable identification by retention indexing, retention pattern ordering, sensory evaluation (sensory analysis and olfactometry), and data mining.</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="114405661"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="114405661"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 114405661; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=114405661]").text(description); $(".js-view-count[data-work-id=114405661]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 114405661; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='114405661']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 114405661, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=114405661]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":114405661,"title":"Untargeted approaches in food-omics: The potential of comprehensive two-dimensional gas chromatography/mass spectrometry","translated_title":"","metadata":{"abstract":"Abstract The contribution focuses on untargeted data processing/analysis approaches that are currently adopted to explore the 4D-data matrices produced by comprehensive two-dimensional gas chromatography-mass spectrometry (GC × GC-MS) in food-omics. Strategies for untargeted explorations are rationalized through the type of features adopted (i.e., visual, datapoint, peak, and peak-regions) at the data processing level, and then discussed through relevant applications and illustrative examples, selected over peer-reviewed literature. The role of MS, including high vs. low resolution MS, as an active probe for specific cross-comparative analysis, is critically discussed also in the context of spectral deconvolution and subtraction, well-established procedures for 1D GC-MS explorations. Moreover, the challenging task of post-targeting aimed at identifying “unknown – knowns”, is examined in its potential, being the key to access a higher level of information. Selected examples emphasize the importance of reliable identification by retention indexing, retention pattern ordering, sensory evaluation (sensory analysis and olfactometry), and data mining.","publisher":"Elsevier BV","publication_date":{"day":null,"month":null,"year":2021,"errors":{}},"publication_name":"TrAC Trends in Analytical Chemistry"},"translated_abstract":"Abstract The contribution focuses on untargeted data processing/analysis approaches that are currently adopted to explore the 4D-data matrices produced by comprehensive two-dimensional gas chromatography-mass spectrometry (GC × GC-MS) in food-omics. Strategies for untargeted explorations are rationalized through the type of features adopted (i.e., visual, datapoint, peak, and peak-regions) at the data processing level, and then discussed through relevant applications and illustrative examples, selected over peer-reviewed literature. 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mining.","internal_url":"https://www.academia.edu/114405661/Untargeted_approaches_in_food_omics_The_potential_of_comprehensive_two_dimensional_gas_chromatography_mass_spectrometry","translated_internal_url":"","created_at":"2024-02-02T19:29:31.031-08:00","preview_url":null,"current_user_can_edit":null,"current_user_is_owner":null,"owner_id":35681884,"coauthors_can_edit":true,"document_type":"paper","co_author_tags":[],"downloadable_attachments":[],"slug":"Untargeted_approaches_in_food_omics_The_potential_of_comprehensive_two_dimensional_gas_chromatography_mass_spectrometry","translated_slug":"","page_count":null,"language":"en","content_type":"Work","owner":{"id":35681884,"first_name":"Albert","middle_initials":null,"last_name":"Robbat","page_name":"AlbertRobbat","domain_name":"tufts","created_at":"2015-10-05T06:36:59.544-07:00","display_name":"Albert Robbat","url":"https://tufts.academia.edu/AlbertRobbat"},"attachments":[],"research_interests":[{"id":422,"name":"Computer 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class="js-work-strip profile--work_container" data-work-id="114405660"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/114405660/Adding_extra_dimensions_to_Tea_Camellia_sinensis_L_volatiles_profiling_by_GC_GC_TOF_MS_and_soft_electron_ionization_effects_of_climate_changes_on_volatile_metabolome"><img alt="Research paper thumbnail of Adding extra-dimensions to Tea (Camellia sinensis L.) volatiles profiling by GC×GC-TOF-MS and soft electron ionization: effects of climate changes on volatile metabolome" class="work-thumbnail" src="https://attachments.academia-assets.com/111112290/thumbnails/1.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/114405660/Adding_extra_dimensions_to_Tea_Camellia_sinensis_L_volatiles_profiling_by_GC_GC_TOF_MS_and_soft_electron_ionization_effects_of_climate_changes_on_volatile_metabolome">Adding extra-dimensions to Tea (Camellia sinensis L.) volatiles profiling by GC×GC-TOF-MS and soft electron ionization: effects of climate changes on volatile metabolome</a></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">SUBMISSION FORM To be sent by July 31st, 2017 to http://www.spettrometriadimassa.it/Congressi/5MS...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">SUBMISSION FORM To be sent by July 31st, 2017 to <a href="http://www.spettrometriadimassa.it/Congressi/5MS-FoodDay/5MSFoodDay_SubmissionForm.php" rel="nofollow">http://www.spettrometriadimassa.it/Congressi/5MS-FoodDay/5MSFoodDay_SubmissionForm.php</a> Presenting Author Marta Cialiè Rosso Università degli Studi di Torino Dipartimento di Scienza e Tecnologia del Farmaco Via Pietro Giuria 9 10125 Torino Italia 0039 0116707172 Fax <a href="mailto:marta.cialierosso@unito.it" rel="nofollow">marta.cialierosso@unito.it</a> Preference:  Oral presentation X Poster Adding extra-dimensions to Tea (Camellia sinensis L.) volatiles profiling by GC×GC-TOF-MS and soft electron ionization: effects of climate changes on volatile metabolome Marta Cialiè Rosso1, Erica Liberto1, Albert Robbat2, Laura Mc Gregor3, Nick Bukowski3, Carlo Bicchi1 and Chiara Cordero1 1 Dipartimento di Scienza e Tecnologia del Farmaco, Università degli Studi di Torino, Torino, Italy 2 Department of Chemistry, Tufts University, Medford, MA, USA 3 Markes International Ltd, Llantrisant, RCT, UK Adding extra-dimensions to Tea (Camellia sinensis L.) volatiles profiling by GC×GC-TOF-MS and soft electron ioni...</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><a id="5a5411b359173c6364fe4fb405454e91" class="wp-workCard--action" rel="nofollow" data-click-track="profile-work-strip-download" data-download="{"attachment_id":111112290,"asset_id":114405660,"asset_type":"Work","button_location":"profile"}" href="https://www.academia.edu/attachments/111112290/download_file?st=MTczMjQyMzk5MSw4LjIyMi4yMDguMTQ2&st=MTczMjQyMzk5MSw4LjIyMi4yMDguMTQ2&s=profile"><span><i class="fa fa-arrow-down"></i></span><span>Download</span></a><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="114405660"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span 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on metals in tea (Camelia sinensis (L.) Kuntze)" class="work-thumbnail" src="https://attachments.academia-assets.com/111112311/thumbnails/1.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/114405659/2014_2016_seasonal_rainfall_effects_on_metals_in_tea_Camelia_sinensis_L_Kuntze_">2014–2016 seasonal rainfall effects on metals in tea (Camelia sinensis (L.) Kuntze)</a></div><div class="wp-workCard_item"><span>Chemosphere</span><span>, 2018</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><a id="0c0a56094409981b77a3b145bb4e96d5" class="wp-workCard--action" rel="nofollow" data-click-track="profile-work-strip-download" data-download="{"attachment_id":111112311,"asset_id":114405659,"asset_type":"Work","button_location":"profile"}" href="https://www.academia.edu/attachments/111112311/download_file?st=MTczMjQyMzk5MSw4LjIyMi4yMDguMTQ2&st=MTczMjQyMzk5MSw4LjIyMi4yMDguMTQ2&s=profile"><span><i class="fa fa-arrow-down"></i></span><span>Download</span></a><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="114405659"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="114405659"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 114405659; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=114405659]").text(description); $(".js-view-count[data-work-id=114405659]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 114405659; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='114405659']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 114405659, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (true){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "0c0a56094409981b77a3b145bb4e96d5" } } $('.js-work-strip[data-work-id=114405659]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":114405659,"title":"2014–2016 seasonal rainfall effects on metals in tea (Camelia sinensis (L.) 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$(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="114405658"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/114405658/Electrodeposition_of_Metal_Alloy_and_Mixed_Oxide_Films_Using_a_Single_Precursor_Tetranuclear_Copper_Nickel_Complex"><img alt="Research paper thumbnail of Electrodeposition of Metal Alloy and Mixed Oxide Films Using a Single‐Precursor Tetranuclear Copper‐Nickel Complex" class="work-thumbnail" src="https://attachments.academia-assets.com/111112317/thumbnails/1.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/114405658/Electrodeposition_of_Metal_Alloy_and_Mixed_Oxide_Films_Using_a_Single_Precursor_Tetranuclear_Copper_Nickel_Complex">Electrodeposition of Metal Alloy and Mixed Oxide Films Using a Single‐Precursor Tetranuclear Copper‐Nickel Complex</a></div><div class="wp-workCard_item"><span>Journal of The Electrochemical Society</span><span>, 1995</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><a id="067aadc124f1f7b34665d3ee11e0a38a" class="wp-workCard--action" rel="nofollow" data-click-track="profile-work-strip-download" data-download="{"attachment_id":111112317,"asset_id":114405658,"asset_type":"Work","button_location":"profile"}" href="https://www.academia.edu/attachments/111112317/download_file?st=MTczMjQyMzk5MSw4LjIyMi4yMDguMTQ2&st=MTczMjQyMzk5MSw4LjIyMi4yMDguMTQ2&s=profile"><span><i class="fa fa-arrow-down"></i></span><span>Download</span></a><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="114405658"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="114405658"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 114405658; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=114405658]").text(description); $(".js-view-count[data-work-id=114405658]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 114405658; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='114405658']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 114405658, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (true){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); 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The alloy deposition potential is invariant with complex stoichiometry. Alloy Ni composition, determined by x-ray diffraction (XRD), increases from 12% for x = 1 to 62% for x = 4. The microscopically rough, well-adhering, continuous films have a natural passivation layer formed by air oxidation that consists of Ni(OH)2, NiO, Cu(OH)2, and Cu20. X-ray photoelectron spectroscopy confirmed the bulk film alloy compositions obtained by XRD. The data revealed complex deposit structures consisting of NiO, Ni(OH)2, Cu20, and Cu-Ni alloy giving a mass balance of the metals in the complexes. The Cu20/Cu ~ ratio is close to unity for the deposit made from the Cu4 complex and decreases to zero for the CuNi3 complex. In contrast only half of the Ni(II) centers are deposited as Ni ~ in the Cu-Ni alloy, the balance consisting of 37% NiO and 15% Ni(OH)2. The constant percentage of Ni as Ni(OH)2 in all deposits suggests that it arises from reduction of Ni coordinated water. Mass balance indicates O in Cu20 and NiO originates from the ~4-O. Smooth variations of alloy compositions, metal oxide/metal ratios, and film particle sizes indicate that all the electrode processes involve discrete molecules of the heteropolymetallic complex.","publication_date":{"day":null,"month":null,"year":1995,"errors":{}},"publication_name":"Journal of The Electrochemical 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$(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="114405657"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/114405657/Gas_chromatographic_retention_characteristics_of_phenols_with_Superox_20M"><img alt="Research paper thumbnail of Gas chromatographic retention characteristics of phenols with Superox-20M" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/114405657/Gas_chromatographic_retention_characteristics_of_phenols_with_Superox_20M">Gas chromatographic retention characteristics of phenols with Superox-20M</a></div><div class="wp-workCard_item"><span>Analytical Chemistry</span><span>, 1982</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">The gas chromatographic retention characteristics of a variety of underivatized phenols have been...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">The gas chromatographic retention characteristics of a variety of underivatized phenols have been studied by using Superox-20M coated on fused silica. The relative retention times of thes compounds were measured at 160, 150, and 140/sup 0/C in order to determine the effect of operating temperature on relative retention. This information is used to predict relative retention times of phenols for which we had no standards. The linear temperature-programmed retention indexes of the solutes were measured. The retention of phenols on this phase is a function of the compounds vapor pressure, its ability to hydrogen bond with the stationary phase, and the strengths of those hydrogen bonds. These properties are in turn governed by steric, inductive, and resonance effects of the substituents. Linear free-energy relations between the logarithm of the ratio of the activity coefficients of phenol to substituted phenol (calculated from relative retention data) and the chromatographic substituent constant, sigma/sub c/, have been determined for some phenols on Superox-20M. Lastly, it was shown by nuclear magnetic resonance experiments that Superox-20M is apparently a poly(ethylene glycol) (also called a polyoxiran or poly(ethylene oxide)). 5 figures, 3 tables.</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="114405657"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="114405657"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 114405657; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=114405657]").text(description); $(".js-view-count[data-work-id=114405657]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 114405657; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='114405657']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 114405657, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (false){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "-1" } } $('.js-work-strip[data-work-id=114405657]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":114405657,"title":"Gas chromatographic retention characteristics of phenols with Superox-20M","translated_title":"","metadata":{"abstract":"The gas chromatographic retention characteristics of a variety of underivatized phenols have been studied by using Superox-20M coated on fused silica. The relative retention times of thes compounds were measured at 160, 150, and 140/sup 0/C in order to determine the effect of operating temperature on relative retention. This information is used to predict relative retention times of phenols for which we had no standards. The linear temperature-programmed retention indexes of the solutes were measured. The retention of phenols on this phase is a function of the compounds vapor pressure, its ability to hydrogen bond with the stationary phase, and the strengths of those hydrogen bonds. These properties are in turn governed by steric, inductive, and resonance effects of the substituents. Linear free-energy relations between the logarithm of the ratio of the activity coefficients of phenol to substituted phenol (calculated from relative retention data) and the chromatographic substituent constant, sigma/sub c/, have been determined for some phenols on Superox-20M. Lastly, it was shown by nuclear magnetic resonance experiments that Superox-20M is apparently a poly(ethylene glycol) (also called a polyoxiran or poly(ethylene oxide)). 5 figures, 3 tables.","publisher":"American Chemical Society (ACS)","publication_date":{"day":null,"month":null,"year":1982,"errors":{}},"publication_name":"Analytical Chemistry"},"translated_abstract":"The gas chromatographic retention characteristics of a variety of underivatized phenols have been studied by using Superox-20M coated on fused silica. The relative retention times of thes compounds were measured at 160, 150, and 140/sup 0/C in order to determine the effect of operating temperature on relative retention. This information is used to predict relative retention times of phenols for which we had no standards. The linear temperature-programmed retention indexes of the solutes were measured. The retention of phenols on this phase is a function of the compounds vapor pressure, its ability to hydrogen bond with the stationary phase, and the strengths of those hydrogen bonds. These properties are in turn governed by steric, inductive, and resonance effects of the substituents. Linear free-energy relations between the logarithm of the ratio of the activity coefficients of phenol to substituted phenol (calculated from relative retention data) and the chromatographic substituent constant, sigma/sub c/, have been determined for some phenols on Superox-20M. Lastly, it was shown by nuclear magnetic resonance experiments that Superox-20M is apparently a poly(ethylene glycol) (also called a polyoxiran or poly(ethylene oxide)). 5 figures, 3 tables.","internal_url":"https://www.academia.edu/114405657/Gas_chromatographic_retention_characteristics_of_phenols_with_Superox_20M","translated_internal_url":"","created_at":"2024-02-02T19:29:29.196-08:00","preview_url":null,"current_user_can_edit":null,"current_user_is_owner":null,"owner_id":35681884,"coauthors_can_edit":true,"document_type":"paper","co_author_tags":[],"downloadable_attachments":[],"slug":"Gas_chromatographic_retention_characteristics_of_phenols_with_Superox_20M","translated_slug":"","page_count":null,"language":"en","content_type":"Work","owner":{"id":35681884,"first_name":"Albert","middle_initials":null,"last_name":"Robbat","page_name":"AlbertRobbat","domain_name":"tufts","created_at":"2015-10-05T06:36:59.544-07:00","display_name":"Albert Robbat","url":"https://tufts.academia.edu/AlbertRobbat"},"attachments":[],"research_interests":[{"id":72,"name":"Chemical Engineering","url":"https://www.academia.edu/Documents/in/Chemical_Engineering"},{"id":523,"name":"Chemistry","url":"https://www.academia.edu/Documents/in/Chemistry"},{"id":524,"name":"Analytical Chemistry","url":"https://www.academia.edu/Documents/in/Analytical_Chemistry"},{"id":4656,"name":"Chromatography","url":"https://www.academia.edu/Documents/in/Chromatography"},{"id":7333,"name":"Nuclear Magnetic Resonance","url":"https://www.academia.edu/Documents/in/Nuclear_Magnetic_Resonance"},{"id":114713,"name":"Vapor Pressure","url":"https://www.academia.edu/Documents/in/Vapor_Pressure"},{"id":166448,"name":"Gas Chromatography","url":"https://www.academia.edu/Documents/in/Gas_Chromatography"},{"id":216526,"name":"Free Energy","url":"https://www.academia.edu/Documents/in/Free_Energy"},{"id":347988,"name":"Phenols","url":"https://www.academia.edu/Documents/in/Phenols"},{"id":875404,"name":"Retention Time","url":"https://www.academia.edu/Documents/in/Retention_Time"},{"id":2066593,"name":"Retention Index","url":"https://www.academia.edu/Documents/in/Retention_Index"}],"urls":[{"id":39145388,"url":"https://pubs.acs.org/doi/pdf/10.1021/ac00246a024"}]}, dispatcherData: dispatcherData }); 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$(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="90409488"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/90409488/The_Chemistry_of_Green_and_Roasted_Coffee_by_Selectable_1D_2D_Gas_Chromatography_Mass_Spectrometry_with_Spectral_Deconvolution"><img alt="Research paper thumbnail of The Chemistry of Green and Roasted Coffee by Selectable 1D/2D Gas Chromatography Mass Spectrometry with Spectral Deconvolution" class="work-thumbnail" src="https://attachments.academia-assets.com/93980698/thumbnails/1.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/90409488/The_Chemistry_of_Green_and_Roasted_Coffee_by_Selectable_1D_2D_Gas_Chromatography_Mass_Spectrometry_with_Spectral_Deconvolution">The Chemistry of Green and Roasted Coffee by Selectable 1D/2D Gas Chromatography Mass Spectrometry with Spectral Deconvolution</a></div><div class="wp-workCard_item"><span>Molecules</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">Gas chromatography/mass spectrometry (GC/MS) is a long-standing technique for the analysis of vol...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">Gas chromatography/mass spectrometry (GC/MS) is a long-standing technique for the analysis of volatile organic compounds (VOCs). When coupled with the Ion Analytics software, GC/MS provides unmatched selectivity in the analysis of complex mixtures and it reduces the reliance on high-resolution chromatography to obtain clean mass spectra. Here, we present an application of spectral deconvolution, with mass spectral subtraction, to identify a wide array of VOCs in green and roasted coffees. Automated sequential, two-dimensional GC-GC/MS of a roasted coffee sample produced the retention index and spectrum of 750 compounds. These initial analytes served as targets for subsequent coffee analysis by GC/MS. The workflow resulted in the quantitation of 511 compounds detected in two different green and roasted coffees. Of these, over 100 compounds serve as candidate differentiators of coffee quality, AAA vs. AA, as designated by the Coopedota cooperative in Costa Rica. Of these, 72 compounds...</span></div><div class="wp-workCard_item wp-workCard--actions"><span class="work-strip-bookmark-button-container"></span><a id="cde1c36c6300c868ccfd7ef6ab9f2d5b" class="wp-workCard--action" rel="nofollow" data-click-track="profile-work-strip-download" data-download="{"attachment_id":93980698,"asset_id":90409488,"asset_type":"Work","button_location":"profile"}" href="https://www.academia.edu/attachments/93980698/download_file?st=MTczMjQyMzk5MSw4LjIyMi4yMDguMTQ2&st=MTczMjQyMzk5MSw4LjIyMi4yMDguMTQ2&s=profile"><span><i class="fa fa-arrow-down"></i></span><span>Download</span></a><span class="wp-workCard--action visible-if-viewed-by-owner inline-block" style="display: none;"><span class="js-profile-work-strip-edit-button-wrapper profile-work-strip-edit-button-wrapper" data-work-id="90409488"><a class="js-profile-work-strip-edit-button" tabindex="0"><span><i class="fa fa-pencil"></i></span><span>Edit</span></a></span></span><span id="work-strip-rankings-button-container"></span></div><div class="wp-workCard_item wp-workCard--stats"><span><span><span class="js-view-count view-count u-mr2x" data-work-id="90409488"><i class="fa fa-spinner fa-spin"></i></span><script>$(function () { var workId = 90409488; window.Academia.workViewCountsFetcher.queue(workId, function (count) { var description = window.$h.commaizeInt(count) + " " + window.$h.pluralize(count, 'View'); $(".js-view-count[data-work-id=90409488]").text(description); $(".js-view-count[data-work-id=90409488]").attr('title', description).tooltip(); }); });</script></span></span><span><span class="percentile-widget hidden"><span class="u-mr2x work-percentile"></span></span><script>$(function () { var workId = 90409488; window.Academia.workPercentilesFetcher.queue(workId, function (percentileText) { var container = $(".js-work-strip[data-work-id='90409488']"); container.find('.work-percentile').text(percentileText.charAt(0).toUpperCase() + percentileText.slice(1)); container.find('.percentile-widget').show(); container.find('.percentile-widget').removeClass('hidden'); }); });</script></span><span><script>$(function() { new Works.PaperRankView({ workId: 90409488, container: "", }); });</script></span></div><div id="work-strip-premium-row-container"></div></div></div><script> require.config({ waitSeconds: 90 })(["https://a.academia-assets.com/assets/wow_profile-f77ea15d77ce96025a6048a514272ad8becbad23c641fc2b3bd6e24ca6ff1932.js","https://a.academia-assets.com/assets/work_edit-ad038b8c047c1a8d4fa01b402d530ff93c45fee2137a149a4a5398bc8ad67560.js"], function() { // from javascript_helper.rb var dispatcherData = {} if (true){ window.WowProfile.dispatcher = window.WowProfile.dispatcher || _.clone(Backbone.Events); dispatcherData = { dispatcher: window.WowProfile.dispatcher, downloadLinkId: "cde1c36c6300c868ccfd7ef6ab9f2d5b" } } $('.js-work-strip[data-work-id=90409488]').each(function() { if (!$(this).data('initialized')) { new WowProfile.WorkStripView({ el: this, workJSON: {"id":90409488,"title":"The Chemistry of Green and Roasted Coffee by Selectable 1D/2D Gas Chromatography Mass Spectrometry with Spectral Deconvolution","translated_title":"","metadata":{"abstract":"Gas chromatography/mass spectrometry (GC/MS) is a long-standing technique for the analysis of volatile organic compounds (VOCs). When coupled with the Ion Analytics software, GC/MS provides unmatched selectivity in the analysis of complex mixtures and it reduces the reliance on high-resolution chromatography to obtain clean mass spectra. Here, we present an application of spectral deconvolution, with mass spectral subtraction, to identify a wide array of VOCs in green and roasted coffees. Automated sequential, two-dimensional GC-GC/MS of a roasted coffee sample produced the retention index and spectrum of 750 compounds. These initial analytes served as targets for subsequent coffee analysis by GC/MS. The workflow resulted in the quantitation of 511 compounds detected in two different green and roasted coffees. Of these, over 100 compounds serve as candidate differentiators of coffee quality, AAA vs. AA, as designated by the Coopedota cooperative in Costa Rica. Of these, 72 compounds...","publisher":"MDPI AG","publication_name":"Molecules"},"translated_abstract":"Gas chromatography/mass spectrometry (GC/MS) is a long-standing technique for the analysis of volatile organic compounds (VOCs). When coupled with the Ion Analytics software, GC/MS provides unmatched selectivity in the analysis of complex mixtures and it reduces the reliance on high-resolution chromatography to obtain clean mass spectra. Here, we present an application of spectral deconvolution, with mass spectral subtraction, to identify a wide array of VOCs in green and roasted coffees. Automated sequential, two-dimensional GC-GC/MS of a roasted coffee sample produced the retention index and spectrum of 750 compounds. These initial analytes served as targets for subsequent coffee analysis by GC/MS. The workflow resulted in the quantitation of 511 compounds detected in two different green and roasted coffees. Of these, over 100 compounds serve as candidate differentiators of coffee quality, AAA vs. AA, as designated by the Coopedota cooperative in Costa Rica. 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$(this).data('initialized', true); } }); $a.trackClickSource(".js-work-strip-work-link", "profile_work_strip") }); </script> <div class="js-work-strip profile--work_container" data-work-id="90409485"><div class="profile--work_thumbnail hidden-xs"><a class="js-work-strip-work-link" data-click-track="profile-work-strip-thumbnail" href="https://www.academia.edu/90409485/Electrocatalytic_decomposition_of_hydrogen_sulfide"><img alt="Research paper thumbnail of Electrocatalytic decomposition of hydrogen sulfide" class="work-thumbnail" src="https://a.academia-assets.com/images/blank-paper.jpg" /></a></div><div class="wp-workCard wp-workCard_itemContainer"><div class="wp-workCard_item wp-workCard--title"><a class="js-work-strip-work-link text-gray-darker" data-click-track="profile-work-strip-title" href="https://www.academia.edu/90409485/Electrocatalytic_decomposition_of_hydrogen_sulfide">Electrocatalytic decomposition of hydrogen sulfide</a></div><div class="wp-workCard_item"><span>Catalysis Letters</span><span>, 1992</span></div><div class="wp-workCard_item"><span class="js-work-more-abstract-truncated">ABSTRACT The recently discovered phenomenon of nonfaradaic electrochemical modification of cataly...</span><a class="js-work-more-abstract" data-broccoli-component="work_strip.more_abstract" data-click-track="profile-work-strip-more-abstract" href="javascript:;"><span> more </span><span><i class="fa fa-caret-down"></i></span></a><span class="js-work-more-abstract-untruncated hidden">ABSTRACT The recently discovered phenomenon of nonfaradaic electrochemical modification of catalytic activity (NEMCA) was explored for the electrocatalytic decomposition of H2S to H2 and S2 over Pt electrodes at 600–750 C and 1 atm. It was found that upon applying a potential to Pt supported on a O2– conducting yttria-stabilized zirconia disk, the decompoition of H2S significantly increased up to a factor of 11 at 600 C. The results appear to verify several aspects of NEMCA including the phenomenon that the electrolyte needs not to conduct reaction-specific species and that the degree of rate enhancement is related to the working electrode polarization. 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