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[{"id":116089849,"identifier":"Attachment_116089849","shouldShowBulkDownload":false}]; window.loswp.shouldDetectTimezone = true; window.loswp.shouldShowBulkDownload = true; window.loswp.showSignupCaptcha = false window.loswp.willEdgeCache = false; window.loswp.work = {"work":{"id":121124775,"created_at":"2024-06-17T03:33:49.545-07:00","from_world_paper_id":256254525,"updated_at":"2024-11-23T18:44:42.841-08:00","_data":{"publisher":"Springer Science and Business Media LLC","grobid_abstract":"Ultra high-performance liquid chromatographyelectrospray ionization-mass spectrometry (UHPLC/ESI/ MS) methodology was adapted for identification and quantification of tocopherols and tocotrienols in vegetable oils with no derivatization or sample preparation steps. The UHPLC analysis was performed using a C18 column and mobile phase composed of methanol: water: ammonium hydroxide (99:1:0.1 v/v/v) and isopropanol. A single mass spectrometer with electrospray on negative mode was used as a detector for tocopherols and tocotrienols. The samples were diluted in isopropanol. The limit of quantification for tocopherols was 0.006 μg mL −1 , and the linear range was 0.006 to 0.01 μg mL −1 ; for tocotrienols, the limit of quantification was 0.002 μg mL −1 , and the linear range of analysis was 0.002 to 0.003 μg mL −1. The correlation coefficients were higher than 0.99, indicating that the method has suitable linearity. The methodology has proven to be precise, reproducible, and robust for the parameters studied.","publication_date":"2017,,","publication_name":"Food Analytical Methods","grobid_abstract_attachment_id":"116089849"},"document_type":"paper","pre_hit_view_count_baseline":null,"quality":"high","language":"en","title":"Tocopherols and Tocotrienols: an Adapted Methodology by UHPLC/MS Without Sample Pretreatment Steps","broadcastable":false,"draft":null,"has_indexable_attachment":true,"indexable":true}}["work"]; window.loswp.workCoauthors = [104600906]; window.loswp.locale = "en"; window.loswp.countryCode = "SG"; window.loswp.cwvAbTestBucket = ""; window.loswp.designVariant = "ds_vanilla"; window.loswp.fullPageMobileSutdModalVariant = "control"; window.loswp.useOptimizedScribd4genScript = false; window.loswp.appleClientId = 'edu.academia.applesignon';</script><script defer="" src="https://accounts.google.com/gsi/client"></script><div class="ds-loswp-container"><div class="ds-work-card--grid-container"><div class="ds-work-card--container js-loswp-work-card"><div class="ds-work-card--cover"><div class="ds-work-cover--wrapper"><div class="ds-work-cover--container"><button class="ds-work-cover--clickable js-swp-download-button" data-signup-modal="{"location":"swp-splash-paper-cover","attachmentId":116089849,"attachmentType":"pdf"}"><img alt="First page of “Tocopherols and Tocotrienols: an Adapted Methodology by UHPLC/MS Without Sample Pretreatment Steps”" class="ds-work-cover--cover-thumbnail" src="https://0.academia-photos.com/attachment_thumbnails/116089849/mini_magick20240802-1-jiyyna.png?1722558761" /><img alt="PDF Icon" class="ds-work-cover--file-icon" src="//a.academia-assets.com/assets/single_work_splash/adobe.icon-574afd46eb6b03a77a153a647fb47e30546f9215c0ee6a25df597a779717f9ef.svg" /><div class="ds-work-cover--hover-container"><span class="material-symbols-outlined" style="font-size: 20px" translate="no">download</span><p>Download Free PDF</p></div><div class="ds-work-cover--ribbon-container">Download Free PDF</div><div class="ds-work-cover--ribbon-triangle"></div></button></div></div></div><div class="ds-work-card--work-information"><h1 class="ds-work-card--work-title">Tocopherols and Tocotrienols: an Adapted Methodology by UHPLC/MS Without Sample Pretreatment Steps</h1><div class="ds-work-card--work-authors ds-work-card--detail"><a class="ds-work-card--author js-wsj-grid-card-author ds2-5-body-md ds2-5-body-link" data-author-id="104600906" href="https://independent.academia.edu/MarinaAnsolin"><img alt="Profile image of Marina Ansolin" class="ds-work-card--author-avatar" src="//a.academia-assets.com/images/s65_no_pic.png" />Marina Ansolin</a></div><div class="ds-work-card--detail"><p class="ds-work-card--detail ds2-5-body-sm">2017, Food Analytical Methods</p><div class="ds-work-card--work-metadata"><div class="ds-work-card--work-metadata__stat"><span class="material-symbols-outlined" style="font-size: 20px" translate="no">visibility</span><p class="ds2-5-body-sm" id="work-metadata-view-count">…</p></div><div class="ds-work-card--work-metadata__stat"><span class="material-symbols-outlined" style="font-size: 20px" translate="no">description</span><p class="ds2-5-body-sm">10 pages</p></div><div class="ds-work-card--work-metadata__stat"><span class="material-symbols-outlined" style="font-size: 20px" translate="no">link</span><p class="ds2-5-body-sm">1 file</p></div></div><script>(async () => { const workId = 121124775; 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The structure of the compounds was identical, so it could not be separated by reverse phase liquid chromatography. The obtained peaks show an important overlapping and we have used chemometric tools to get a calibration model, which assumes a linear behavior, i.e., the total signal is the sum of individual signals of components. Recovery percentages were between 90.3% and 95.7%. The method has been successfully applied to edible oils and dietary supplements. No pretreatment of the samples was needed.</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Development of an Advance Method for the Determination of Tocopherols in Edible Oils","attachmentId":115676043,"attachmentType":"pdf","work_url":"https://www.academia.edu/120568914/Development_of_an_Advance_Method_for_the_Determination_of_Tocopherols_in_Edible_Oils","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/120568914/Development_of_an_Advance_Method_for_the_Determination_of_Tocopherols_in_Edible_Oils"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="2" data-entity-id="40347682" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/40347682/Extraction_and_quantification_of_tocopherols_from_edible_oils_using_high_performance_liquid_chromatography">Extraction and quantification of tocopherols from edible oils using high performance liquid chromatography</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="126411885" href="https://salu.academia.edu/MSirohi">Muzafar H . Sirohi</a></div><p class="ds-related-work--metadata ds2-5-body-xs">International Journal of Biosciences, 2019</p><p class="ds-related-work--abstract ds2-5-body-sm">Adulteration of Extra Virgin Olive Oil with olive oil and sunflower oil remained major issue in edible oil industry. Herein, rapid, sensitive and precise method for the determination of all type of tocopherols in different vegetable oils includinhg sunflower oil, olive oil and extra virgin olive oil is reported. Reverse Phase High Performance Liquid Chromatography (RP-HPLC) with UV detector was used for tocopherol determination. A simple, quick and sensitive method to estimate the antioxidant quantity is proposed. In this method oils were diluted in methanol and injected directly into column (no saponification procedure). Methanol and water (98:2) mixture was used as mobile phase. Three tocopherols (α, γ and δ) were detected at 292 nm wavelength with UV detector. Method had good limit of detection (LOD) (7ng/g) and reproducibility (C.V% 0.9, 0.8 and 0.4 for α, γ and δ tocopherols, respectively). Result showed the best source for α-tocopherol was sun flower oil (146.65±1.7mg/kg). Oil richest in δ-tocopherol was olive oil and δ-tocopherol was absent in extra virgin olive oil. The current study suggest the new parameter (ratio of α/γ) as first screening indicator of authenticity of purity of extra virgin olive oil for differentiation of various cultivators of same generic source.</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Extraction and quantification of tocopherols from edible oils using high performance liquid chromatography","attachmentId":60593264,"attachmentType":"pdf","work_url":"https://www.academia.edu/40347682/Extraction_and_quantification_of_tocopherols_from_edible_oils_using_high_performance_liquid_chromatography","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/40347682/Extraction_and_quantification_of_tocopherols_from_edible_oils_using_high_performance_liquid_chromatography"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="3" data-entity-id="2297970" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/2297970/Comparison_of_reversed_phase_liquid_chromatography_mass_spectrometry_with_electrospray_and_atmospheric_pressure_chemical_ionization_for_analysis_of_dietary_tocopherols">Comparison of reversed-phase liquid chromatography–mass spectrometry with electrospray and atmospheric pressure chemical ionization for analysis of dietary tocopherols</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="2389241" href="https://independent.academia.edu/JelenaJastrebova">Jelena Jastrebova</a></div><p class="ds-related-work--metadata ds2-5-body-xs">2007</p><p class="ds-related-work--abstract ds2-5-body-sm">ESI and APCI ionization techniques in both negative and positive ion modes were evaluated for simultaneous LC–MS analysis of the four tocopherol homologues (α, β, γ and δ). The ESI and APCI ionization of tocopherols in positive ion mode was not efficient and proceeded via two competitive mechanisms, with the formation of protonated pseudo-molecular ions and molecular ions, which adversely influenced the repeatability of MS signal. Ionization in negative ion mode in both ESI and APCI was more efficient as it only produced target deprotonated pseudo-molecular ions. The APCI in negative ion mode showed larger linearity range, lower detection limits and was less sensitive to the differences in chemical structure of analytes and nature of applied solvents than negative ion ESI. Negative ion APCI was, therefore, chosen for the development of LC–MS method for simultaneous determination of the four tocopherols in foods. A baseline separation of the tocopherols was achieved on novel pentafluorophenyl silica-based column Fluophase PFP. The use of methanol–water (95:5, v/v) as a mobile phase was preferable to the use of acetonitrile–water due to considerable gain in MS signal. The limits of quantifications were 9 ng/mL for α-tocopherol, 8 ng/mL for β- and γ- and 7.5 ng/mL for δ-tocopherol when 2 μL was injected. This method was successfully applied to determination of tocopherols in sunflower oil and milk.</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Comparison of reversed-phase liquid chromatography–mass spectrometry with electrospray and atmospheric pressure chemical ionization for analysis of dietary tocopherols","attachmentId":31635986,"attachmentType":"pdf","work_url":"https://www.academia.edu/2297970/Comparison_of_reversed_phase_liquid_chromatography_mass_spectrometry_with_electrospray_and_atmospheric_pressure_chemical_ionization_for_analysis_of_dietary_tocopherols","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/2297970/Comparison_of_reversed_phase_liquid_chromatography_mass_spectrometry_with_electrospray_and_atmospheric_pressure_chemical_ionization_for_analysis_of_dietary_tocopherols"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="4" data-entity-id="14942654" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/14942654/Determination_of_Tocopherols_and_Tocotrienols_in_Vegetable_Oils_by_Nanoliquid_Chromatography_with_Ultraviolet_Visible_Detection_Using_a_Silica_Monolithic_Column">Determination of Tocopherols and Tocotrienols in Vegetable Oils by Nanoliquid Chromatography with Ultraviolet−Visible Detection Using a Silica Monolithic Column</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="34101217" href="https://independent.academia.edu/ESim%C3%B3alfonso">E. Simó-alfonso</a><span>, </span><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="33933893" href="https://independent.academia.edu/LorenzoCerretani">Lorenzo Cerretani</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Agricultural and Food Chemistry, 2010</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Determination of Tocopherols and Tocotrienols in Vegetable Oils by Nanoliquid Chromatography with Ultraviolet−Visible Detection Using a Silica Monolithic Column","attachmentId":43722755,"attachmentType":"pdf","work_url":"https://www.academia.edu/14942654/Determination_of_Tocopherols_and_Tocotrienols_in_Vegetable_Oils_by_Nanoliquid_Chromatography_with_Ultraviolet_Visible_Detection_Using_a_Silica_Monolithic_Column","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/14942654/Determination_of_Tocopherols_and_Tocotrienols_in_Vegetable_Oils_by_Nanoliquid_Chromatography_with_Ultraviolet_Visible_Detection_Using_a_Silica_Monolithic_Column"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="5" data-entity-id="78676861" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/78676861/Development_and_Validation_of_Simple_Reversed_Phase_Method_for_Separation_and_Quantification_of_Tocopherols_in_Edible_Oils">Development and Validation of Simple Reversed Phase Method for Separation and Quantification of Tocopherols in Edible Oils</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="131411281" href="https://independent.academia.edu/AdelShehata4">Adel Shehata</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Egyptian Journal of Chemistry, 2018</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Development and Validation of Simple Reversed Phase Method for Separation and Quantification of Tocopherols in Edible Oils","attachmentId":85640981,"attachmentType":"pdf","work_url":"https://www.academia.edu/78676861/Development_and_Validation_of_Simple_Reversed_Phase_Method_for_Separation_and_Quantification_of_Tocopherols_in_Edible_Oils","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/78676861/Development_and_Validation_of_Simple_Reversed_Phase_Method_for_Separation_and_Quantification_of_Tocopherols_in_Edible_Oils"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="6" data-entity-id="34385558" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/34385558/Analysis_of_tocopherols_in_vegetable_oils_by_high_performance_liquid_chromatography_Comparison_of_fluorescence_and_evaporative_light_scattering_detection">Analysis of tocopherols in vegetable oils by high-performance liquid chromatography: Comparison of fluorescence and evaporative light-scattering detection</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="34694729" href="https://uga.academia.edu/wwwcaesugaedudepartmentsfstLBCAP">Casimir C Akoh</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of the American Oil Chemists’ Society, 1994</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Analysis of tocopherols in vegetable oils by high-performance liquid chromatography: Comparison of fluorescence and evaporative light-scattering detection","attachmentId":54270951,"attachmentType":"pdf","work_url":"https://www.academia.edu/34385558/Analysis_of_tocopherols_in_vegetable_oils_by_high_performance_liquid_chromatography_Comparison_of_fluorescence_and_evaporative_light_scattering_detection","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/34385558/Analysis_of_tocopherols_in_vegetable_oils_by_high_performance_liquid_chromatography_Comparison_of_fluorescence_and_evaporative_light_scattering_detection"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="7" data-entity-id="72899932" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/72899932/Determination_of_tocopherols_and_tocotrienols_in_cereals_by_pressurized_liquid_extraction_liquid_chromatography_mass_spectrometry">Determination of tocopherols and tocotrienols in cereals by pressurized liquid extraction–liquid chromatography–mass spectrometry</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="101889434" href="https://independent.academia.edu/MYRIAMBUSTAMANTERANGEL">MYRIAM BUSTAMANTE RANGEL</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Analytica Chimica Acta, 2007</p><p class="ds-related-work--abstract ds2-5-body-sm">A rapid analytical method including pressurized liquid extraction (PLE) and liquid chromatography-electrospray ionisation-mass spectrometry (LC-ESI-MS) has been developed for the determination of tocopherols and tocotrienols in cereals. The pressurized liquid extraction parameters were optimized in order to maximize the extraction efficiency. The use of methanol as extraction solvent at a temperature of 50 degrees C and a pressure of 110 bar, using one cycle of extraction with a static time of 5 min, provided the best results. A good LC separation was achieved using a C(18) column and a solution of 6.0 mM ammonia in methanol/water (97:3, v/v) as the mobile phase at a flow rate of 0.2 mL min(-1). MS coupling with an ESI interface in the negative ion mode was used as the detection technique. In the present work, it is shown that the addition of a base to the mobile phase is required to enhance the ionization of tocopherols and tocotrienols in negative ion mode electrospray ionization....</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Determination of tocopherols and tocotrienols in cereals by pressurized liquid extraction–liquid chromatography–mass spectrometry","attachmentId":83898407,"attachmentType":"pdf","work_url":"https://www.academia.edu/72899932/Determination_of_tocopherols_and_tocotrienols_in_cereals_by_pressurized_liquid_extraction_liquid_chromatography_mass_spectrometry","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/72899932/Determination_of_tocopherols_and_tocotrienols_in_cereals_by_pressurized_liquid_extraction_liquid_chromatography_mass_spectrometry"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="8" data-entity-id="23202164" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/23202164/Quantification_of_Tocopherols_and_Tocotrienols_in_Portuguese_Olive_Oils_Using_HPLC_with_Three_Different_Detection_Systems">Quantification of Tocopherols and Tocotrienols in Portuguese Olive Oils Using HPLC with Three Different Detection Systems</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="45011450" href="https://independent.academia.edu/PatriciaOliveira116">Patricia Oliveira</a></div><p class="ds-related-work--metadata ds2-5-body-xs">J Agr Food Chem, 2006</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Quantification of Tocopherols and Tocotrienols in Portuguese Olive Oils Using HPLC with Three Different Detection Systems","attachmentId":43690954,"attachmentType":"pdf","work_url":"https://www.academia.edu/23202164/Quantification_of_Tocopherols_and_Tocotrienols_in_Portuguese_Olive_Oils_Using_HPLC_with_Three_Different_Detection_Systems","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/23202164/Quantification_of_Tocopherols_and_Tocotrienols_in_Portuguese_Olive_Oils_Using_HPLC_with_Three_Different_Detection_Systems"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="9" data-entity-id="54235652" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/54235652/Simultaneous_extraction_of_tocotrienols_and_tocopherols_from_cereals_using_pressurized_liquid_extraction_prior_to_LC_determination">Simultaneous extraction of tocotrienols and tocopherols from cereals using pressurized liquid extraction prior to LC determination</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="101889434" href="https://independent.academia.edu/MYRIAMBUSTAMANTERANGEL">MYRIAM BUSTAMANTE RANGEL</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Separation Science, 2009</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Simultaneous extraction of tocotrienols and tocopherols from cereals using pressurized liquid extraction prior to LC determination","attachmentId":70696702,"attachmentType":"pdf","work_url":"https://www.academia.edu/54235652/Simultaneous_extraction_of_tocotrienols_and_tocopherols_from_cereals_using_pressurized_liquid_extraction_prior_to_LC_determination","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline 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class="ds-related-work--container js-related-work-sidebar-card" data-collection-position="3" data-entity-id="113563004" data-sort-order="default"><a class="ds-related-work--title js-related-work-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/113563004/Rapid_Estimation_of_Tocopherol_Content_in_Linseed_and_Sunflower_Oils_Reactivity_and_Assay">Rapid Estimation of Tocopherol Content in Linseed and Sunflower Oils-Reactivity and Assay</a><div class="ds-related-work--metadata"><a class="js-related-work-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="277533442" href="https://uni-lj.academia.edu/IrenaKraljCigic">Irena Kralj Cigic</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Molecules, 2015</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Rapid Estimation of Tocopherol Content in Linseed 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Marketed in Nigeria","attachmentId":70591840,"attachmentType":"pdf","work_url":"https://www.academia.edu/54031424/Physicochemical_Characteristics_and_HPLC_Determination_of_Alpha_Tocopherol_in_Eighteen_Edible_Vegetable_Oils_Marketed_in_Nigeria","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-related-work-grid-card-view-pdf" href="https://www.academia.edu/54031424/Physicochemical_Characteristics_and_HPLC_Determination_of_Alpha_Tocopherol_in_Eighteen_Edible_Vegetable_Oils_Marketed_in_Nigeria"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-related-work-sidebar-card" data-collection-position="5" data-entity-id="63880756" data-sort-order="default"><a class="ds-related-work--title js-related-work-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/63880756/Tocopherol_content_in_vegetable_oils_using_a_rapid_HPLC_fluorescence_detection_method">Tocopherol content in vegetable oils using a rapid HPLC fluorescence detection method</a><div class="ds-related-work--metadata"><a class="js-related-work-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="179288064" href="https://independent.academia.edu/RaducuCamelia">Camelia Raducu</a></div><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Tocopherol content in vegetable oils using a rapid HPLC fluorescence detection 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data-author-id="6306154" href="https://independent.academia.edu/FernandezHector">Hector Fernandez</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Talanta, 2013</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Quantitative determination of tocopherols in edible vegetable oils using electrochemical ultra-microsensors combined with chemometric tools","attachmentId":43201232,"attachmentType":"pdf","work_url":"https://www.academia.edu/22599527/Quantitative_determination_of_tocopherols_in_edible_vegetable_oils_using_electrochemical_ultra_microsensors_combined_with_chemometric_tools","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline 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data-author-id="7910954" href="https://sbkwomenuni.academia.edu/DrAyeshaMushtaq">Dr. Ayesha Mushtaq</a></div><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Extraction and Estimation of Alpha-Tocopherol from Commercially Available Vegetable Cooking Oils by HPLC","attachmentId":37387168,"attachmentType":"pdf","work_url":"https://www.academia.edu/12062577/Extraction_and_Estimation_of_Alpha_Tocopherol_from_Commercially_Available_Vegetable_Cooking_Oils_by_HPLC","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-related-work-grid-card-view-pdf" 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ds2-5-body-link" data-author-id="43383257" href="https://independent.academia.edu/TGaleanod%C3%ADaz">T. Galeano-díaz</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Food Chemistry, 2007</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Chemometrics for the resolution of co-eluting peaks of β- and γ-tocopherols in RP-HPLC: Determination in edible oils and dietary supplements","attachmentId":67123669,"attachmentType":"pdf","work_url":"https://www.academia.edu/48590591/Chemometrics_for_the_resolution_of_co_eluting_peaks_of_%CE%B2_and_%CE%B3_tocopherols_in_RP_HPLC_Determination_in_edible_oils_and_dietary_supplements","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-related-work-grid-card-view-pdf" href="https://www.academia.edu/48590591/Chemometrics_for_the_resolution_of_co_eluting_peaks_of_%CE%B2_and_%CE%B3_tocopherols_in_RP_HPLC_Determination_in_edible_oils_and_dietary_supplements"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-related-work-sidebar-card" data-collection-position="13" data-entity-id="14679832" data-sort-order="default"><a class="ds-related-work--title js-related-work-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/14679832/A_small_scale_sample_preparation_method_with_HPLC_analysis_for_determination_of_tocopherols_and_tocotrienols_in_cereals">A small-scale sample preparation method with HPLC analysis for determination of tocopherols and tocotrienols in cereals</a><div class="ds-related-work--metadata"><a class="js-related-work-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="33627626" href="https://helsinki.academia.edu/VelimattiOllilainen">Velimatti Ollilainen</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Food Composition and Analysis, 2004</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"A small-scale sample preparation method with HPLC analysis for determination of tocopherols and tocotrienols in cereals","attachmentId":46120635,"attachmentType":"pdf","work_url":"https://www.academia.edu/14679832/A_small_scale_sample_preparation_method_with_HPLC_analysis_for_determination_of_tocopherols_and_tocotrienols_in_cereals","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link 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analysis</a><div class="ds-related-work--metadata"><a class="js-related-work-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="222176624" href="https://independent.academia.edu/ComanVirginia">Virginia Coman</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Open Chemistry, 2010</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Separation and determination of tocopherols in vegetable oils by solid phase extraction on porous polymers SPE cartridges and capillary gas chromatography analysis","attachmentId":103619052,"attachmentType":"pdf","work_url":"https://www.academia.edu/103674194/Separation_and_determination_of_tocopherols_in_vegetable_oils_by_solid_phase_extraction_on_porous_polymers_SPE_cartridges_and_capillary_gas_chromatography_analysis","alternativeTracking":true}"><span class="material-symbols-outlined" 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