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<!DOCTYPE html><html lang="en"><head><meta charset="utf-8"> <meta name="viewport" content="width=device-width, initial-scale=1"> <title>Synthesis and Characterization of Ferroelectrics | MDPI Books</title> <link rel="preconnect" href="https://pub.mdpi-res.com" crossorigin> <script>window.loadTurnstile = new Promise(resolve => { window.onloadTurnstileCallback = function () { resolve(); delete window.onloadTurnstileCallback; delete window.loadTurnstile; } })</script> <script src="https://d1bxh8uas1mnw7.cloudfront.net/assets/embed.js" defer></script> <link rel="preload" as="style" href="https://pub.mdpi-res.com/assets/fonts/suisse/fonts.css"> <link rel="stylesheet" href="https://pub.mdpi-res.com/assets/fonts/suisse/fonts.css" media="all"> <meta name="twitter:image:type" content="image/jpeg"> <meta name="twitter:image:width" content="1200"> <meta name="twitter:image:height" content="630"> <meta property="og:image:type" content="image/jpeg"> <meta property="og:image:width" content="1200"> <meta property="og:image:height" content="630"> <meta name="twitter:card" content="summary_large_image"> <meta name="twitter:site" content="@BooksMDPI"> <meta property="og:site_name" content="MDPI Books"> <meta name="twitter:title" content="Synthesis and Characterization of Ferroelectrics"> <meta property="og:type" content="book"> <meta property="og:title" content="Synthesis and Characterization of Ferroelectrics"> <meta property="og:url" content="https://www.mdpi.com/books/reprint/3336-synthesis-and-characterization-of-ferroelectrics"> <meta name="description" content="The Special Issue on Synthesis and Characterization of Ferroelectrics reports on several physical properties of ferroelectric materials and their technological aspects. Different substitution mechanisms provide ideas toward future improvement of lead-free (Ba,Ca)(Zr,Ti)O3 piezoelectric ceramics, including the electrocaloric effect, fluorescence, and energy storage. It is established that axial and radial element segregation differently influences electrical properties of 0.68Pb(Mg1/3Nb2/3)0.32PbTiO3 (PMN-32PT for short) single crystals. While the electrical properties along the axial direction strongly depend on the PbTiO3 content, the electrical properties along the axial direction are mainly determined by the ratio of Nb and Mg. On the other hand, Fe-substitution of PMN-32PT crystals lead to an enhancement of the coercive field due to wall pinning induced by charged defect dipoles. It is also found, that capacitors based on Pt/Na0.5Bi0.5TiO3/La0.5Sr0.5CoO3 thin films display good fatigue resistance and retention. Another lead-free thin film capacitor fabricated from Ba0.3Sr0.7Zr0.18Ti0.82 features a low leakage current density and high breakdown strength. Such capacitors are essential for energy storage. Furthermore, an enhanced electrocaloric effect on 0.73Pb(Mg1/3Nb2/3)0.27PbTiO3 single crystals is demonstrated. This effect is promising for novel solid-state cooling systems."> <meta name="twitter:description" content="The Special Issue on Synthesis and Characterization of Ferroelectrics reports on several physical properties of ferroelectric materials and their technological aspects. Different substitution mechanisms provide ideas toward future improvement of lead-free (Ba,Ca)(Zr,Ti)O3 piezoelectric ceramics, including the electrocaloric effect, fluorescence, and energy storage. It is established that axial and radial element segregation differently influences electrical properties of 0.68Pb(Mg1/3Nb2/3)0.32PbTiO3 (PMN-32PT for short) single crystals. While the electrical properties along the axial direction strongly depend on the PbTiO3 content, the electrical properties along the axial direction are mainly determined by the ratio of Nb and Mg. On the other hand, Fe-substitution of PMN-32PT crystals lead to an enhancement of the coercive field due to wall pinning induced by charged defect dipoles. It is also found, that capacitors based on Pt/Na0.5Bi0.5TiO3/La0.5Sr0.5CoO3 thin films display good fatigue resistance and retention. Another lead-free thin film capacitor fabricated from Ba0.3Sr0.7Zr0.18Ti0.82 features a low leakage current density and high breakdown strength. Such capacitors are essential for energy storage. Furthermore, an enhanced electrocaloric effect on 0.73Pb(Mg1/3Nb2/3)0.27PbTiO3 single crystals is demonstrated. This effect is promising for novel solid-state cooling systems."> <meta property="og:description" content="The Special Issue on Synthesis and Characterization of Ferroelectrics reports on several physical properties of ferroelectric materials and their technological aspects. Different substitution mechanisms provide ideas toward future improvement of lead-free (Ba,Ca)(Zr,Ti)O3 piezoelectric ceramics, including the electrocaloric effect, fluorescence, and energy storage. It is established that axial and radial element segregation differently influences electrical properties of 0.68Pb(Mg1/3Nb2/3)0.32PbTiO3 (PMN-32PT for short) single crystals. While the electrical properties along the axial direction strongly depend on the PbTiO3 content, the electrical properties along the axial direction are mainly determined by the ratio of Nb and Mg. On the other hand, Fe-substitution of PMN-32PT crystals lead to an enhancement of the coercive field due to wall pinning induced by charged defect dipoles. It is also found, that capacitors based on Pt/Na0.5Bi0.5TiO3/La0.5Sr0.5CoO3 thin films display good fatigue resistance and retention. Another lead-free thin film capacitor fabricated from Ba0.3Sr0.7Zr0.18Ti0.82 features a low leakage current density and high breakdown strength. Such capacitors are essential for energy storage. Furthermore, an enhanced electrocaloric effect on 0.73Pb(Mg1/3Nb2/3)0.27PbTiO3 single crystals is demonstrated. This effect is promising for novel solid-state cooling systems."> <meta name="twitter:image" content="https://mdpi-res.com/bookfiles/book/3336/Synthesis_and_Characterization_of_Ferroelectrics.jpg?v=1732672922"> <meta name="twitter:image:alt" content="Book cover"> <meta property="og:image" content="https://mdpi-res.com/bookfiles/book/3336/Synthesis_and_Characterization_of_Ferroelectrics.jpg?v=1732672922"> <meta property="og:image:alt" content="Book cover"> <meta name="author" content="Jan Dec"> <link rel="alternate" type="application/pdf" href="https://mdpi-res.com/bookfiles/book/3336/Synthesis_and_Characterization_of_Ferroelectrics.pdf?v=1732672922"> <link rel="canonical" type="text/html" href="https://www.mdpi.com/books/reprint/3336-synthesis-and-characterization-of-ferroelectrics"> <link rel="alternate" type="text/html" href="https://www.mdpi.com/books/reprint/3336"> <meta name content="Materials / States of matter"> <meta name="citation_book_type" content="Reprint"> <meta name="citation_doi" content="10.3390/books978-3-03943-656-9"> <meta name="citation_editor" content="Jan Dec"> <meta name="citation_fulltext_world_readable" content> <meta name="citation_isbn" content="978-3-03943-655-2"> <meta name="citation_isbn" content="978-3-03943-656-9"> <meta name="citation_keywords" content="PMN-32PT; characterization; segregation; Bridgman technique; ferroelectric materials; piezoelectric; ceramic; lead-free; PMN-32PT single crystal; acceptor doping; charged defects; dielectric relaxation; electrical conduction; NBT epitaxial film; ferroelectric properties; ultraviolet light; BSZT thin films; capacitance properties; RF magnetron sputtering; PMN-PT; single crystals; P鈥揈 hysteresis loop; electrocaloric effect; Maxwell relation; n/a"> <meta name="citation_language" content="English"> <meta name="citation_online_date" content="2021/01/21"> <meta name="citation_pages" content="74"> <meta name="citation_pdf_url" content="https://mdpi-res.com/bookfiles/book/3336/Synthesis_and_Characterization_of_Ferroelectrics.pdf?v=1732672922"> <meta name="citation_publication_date" content="2021/01/21"> <meta name="citation_publisher" content="MDPI - Multidisciplinary Digital Publishing Institute"> <meta name="citation_title" content="Synthesis and Characterization of Ferroelectrics"> <meta name="dc.creator" content="Jan Dec"> <meta name="dc.description" content="The Special Issue on “Synthesis and Characterization of Ferroelectrics” reports on several physical properties of ferroelectric materials and their technological aspects. Different substitution mechanisms provide ideas toward future improvement of lead-free (Ba,Ca)(Zr,Ti)O3 piezoelectric ceramics, including the electrocaloric effect, fluorescence, and energy storage. It is established that axial and radial element segregation differently influences electrical properties of 0.68Pb(Mg1/3Nb2/3)0.32PbTiO3 (PMN-32PT for short) single crystals. While the electrical properties along the axial direction strongly depend on the PbTiO3 content, the electrical properties along the axial direction are mainly determined by the ratio of Nb and Mg. On the other hand, Fe-substitution of PMN-32PT crystals lead to an enhancement of the coercive field due to wall pinning induced by charged defect dipoles. It is also found, that capacitors based on Pt/Na0.5Bi0.5TiO3/La0.5Sr0.5CoO3 thin films display good fatigue resistance and retention. Another lead-free thin film capacitor fabricated from Ba0.3Sr0.7Zr0.18Ti0.82 features a low leakage current density and high breakdown strength. Such capacitors are essential for energy storage. Furthermore, an enhanced electrocaloric effect on 0.73Pb(Mg1/3Nb2/3)0.27PbTiO3 single crystals is demonstrated. This effect is promising for novel solid-state cooling systems."> <meta name="dc.identifier" content="10.3390/books978-3-03943-656-9"> <meta name="dc.identifier" content="https://doi.org/10.3390/books978-3-03943-656-9" scheme="dcterms.uri"> <meta name="dc.language" content="English" xml:lang="en_US"> <meta name="dc.subject" content="Chemistry & Materials Science"> <meta name="dc.subject" content="Engineering"> <meta name="dc.subject" content="Environmental & Earth Sciences"> <meta name="dc.title" content="Synthesis and Characterization of Ferroelectrics"> <meta name="dc.type" content="book"> <style>body{overflow-x:hidden}:root{color-scheme:only light}@media screen and (min-width:2500px){html{font-size:105%}}html body{--tw-text-opacity:1;color:#172b4d;color:rgba(var(--color-text-default),var(--tw-text-opacity))}@font-face{font-family:swiper-icons;font-style:normal;font-weight:400;src:url("data:application/font-woff;charset=utf-8;base64, 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.slider-origin>.merge-h\:left-auto{left:auto}.slider-horizontal .slider-origin>.merge-h\:top-5{top:1.25rem}.slider-horizontal .slider-origin>.merge-h\:translate-x-1\/2{--tw-translate-x:50%;transform:translate(50%,var(--tw-translate-y)) rotate(var(--tw-rotate)) skewX(var(--tw-skew-x)) skewY(var(--tw-skew-y)) scaleX(var(--tw-scale-x)) scaleY(var(--tw-scale-y));transform:translate(var(--tw-translate-x),var(--tw-translate-y)) rotate(var(--tw-rotate)) skewX(var(--tw-skew-x)) skewY(var(--tw-skew-y)) scaleX(var(--tw-scale-x)) scaleY(var(--tw-scale-y))}.slider-vertical .slider-origin>.merge-v\:left-7{left:1.75rem}.slider-vertical .slider-origin>.merge-v\:right-1{right:.25rem}.slider-vertical .slider-origin>.merge-v\:top-auto{top:auto}.slider-vertical .slider-origin>.merge-v\:-translate-x-4{--tw-translate-x:-1rem;transform:translate(-1rem,var(--tw-translate-y)) rotate(var(--tw-rotate)) skewX(var(--tw-skew-x)) skewY(var(--tw-skew-y)) scaleX(var(--tw-scale-x)) scaleY(var(--tw-scale-y));transform:translate(var(--tw-translate-x),var(--tw-translate-y)) rotate(var(--tw-rotate)) skewX(var(--tw-skew-x)) skewY(var(--tw-skew-y)) scaleX(var(--tw-scale-x)) scaleY(var(--tw-scale-y))}.slider-horizontal.slider-txt-rtl .txt-rtl-h\:-left-2{left:-.5rem}.slider-horizontal.slider-txt-rtl .txt-rtl-h\:left-0{left:0}.slider-horizontal.slider-txt-rtl .txt-rtl-h\:right-auto{right:auto}.slider-tap .tap\:transition-transform{transition-duration:.15s;transition-property:transform;transition-timing-function:cubic-bezier(.4,0,.2,1)}.slider-tap .tap\:duration-300{transition-duration:.3s}.slider-tooltip-focus:not(.slider-focused) .tt-focus\:hidden{display:none!important}.slider-tooltip-focus.slider-focused:not(.slider-tooltip-hidden) .tt-focused\:block{display:block!important}.slider-tooltip-drag:not(.slider-state-drag) .tt-drag\:hidden{display:none!important}.slider-tooltip-drag.slider-state-drag .tt-dragging\:block\:not$\.slider-tooltip-hidden${display:block!important}@media not all and (min-width:1024px){.max-lg\:mb-lg{margin-bottom:1.5rem;margin-bottom:var(--spacing-lg)}.max-lg\:mt-xl{margin-top:2rem;margin-top:var(--spacing-xl)}.max-lg\:block{display:block}.max-lg\:hidden{display:none}.max-lg\:\!w-full{width:100%!important}.max-lg\:w-full{width:100%}.max-lg\:items-center{align-items:center}.max-lg\:gap-x-6{-moz-column-gap:1.5rem;column-gap:1.5rem}.max-lg\:border-b{border-bottom-width:1px}.max-lg\:border-t-\[1px\]{border-top-width:1px}.max-lg\:border-t-color-default{--tw-border-opacity:1;border-top-color:#dcdfe4;border-top-color:rgba(var(--color-border-default),var(--tw-border-opacity))}.max-lg\:pt-lg{padding-top:1.5rem;padding-top:var(--spacing-lg)}.max-lg\:pt-md{padding-top:1rem;padding-top:var(--spacing-md)}.max-lg\:\!text-xl{font-size:1.25rem!important;line-height:1.75rem!important}}@media 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class="space-x-xs text-xs"><span>Hardback</span></li></ul></div><div data-v-2fcfbc20><span class="text-xs font-bold" data-v-2fcfbc20>License and Copyright</span><div class="m-rich-text text-xs" data-v-2fcfbc20>漏 2022 by the authors; CC BY-NC-ND license</div></div><div data-v-2fcfbc20><span class="text-xs font-bold" data-v-2fcfbc20>Keywords</span><div class="m-rich-text text-xs" data-v-2fcfbc20>PMN-32PT; characterization; segregation; Bridgman technique; ferroelectric materials; piezoelectric; ceramic; lead-free; PMN-32PT single crystal; acceptor doping; charged defects; dielectric relaxation; electrical conduction; NBT epitaxial film; ferroelectric properties; ultraviolet light; BSZT thin films; capacitance properties; RF magnetron sputtering; PMN-PT; single crystals; P鈥揈 hysteresis loop; electrocaloric effect; Maxwell relation; n/a</div></div><button class="flex cursor-pointer flex-row items-center gap-sm" type="button"><span class="text-xs font-bold"> Order & Delivery </span><svg 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viewBox="0 0 16 16"></svg></span></button></div></div><div class="flex flex-col gap-xs"><div class=""><h1 class="m-heading text-inherit m-h4 font-light mb-xs"><span class="m-rich-text">Synthesis and Characterization of Ferroelectrics</span></h1></div></div><div class="flex lg:hidden"><button type="button" class="group relative max-w-[12.5rem] lg:w-80 lg:max-w-full"><img src="https://mdpi-res.com/bookfiles/book/3336/Synthesis_and_Characterization_of_Ferroelectrics.jpg?v=1732672922" onerror="this.setAttribute('data-error', 1)" alt="Book cover" data-nuxt-img srcset="https://mdpi-res.com/bookfiles/book/3336/Synthesis_and_Characterization_of_Ferroelectrics.jpg?v=1732672922 1x, https://mdpi-res.com/bookfiles/book/3336/Synthesis_and_Characterization_of_Ferroelectrics.jpg?v=1732672922 2x" class="h-full w-full object-cover object-top shadow"><div class="absolute inset-0 bg-content-inverse opacity-0 transition-opacity lg:group-hover:opacity-10"></div><span class="m-text text-xs absolute right-xs top-xs rounded bg-content-subtler px-xs text-color-default transition-opacity"> Look inside </span></button></div><div class="flex flex-wrap items-center gap-x-sm gap-y-0.5 text-sm"><span>Edited by</span><button class="flex items-center gap-xs" type="button"><span class="m-avatar flex items-center justify-center overflow-hidden rounded-full bg-brand-bold font-medium text-color-on-brand h-5 w-5 min-w-5 text-[0.575rem] !bg-brand-boldest [&>span]:text-[0.625rem]" data-testid="m-avatar"><span translate="no">JD</span><span class="sr-only">Jan Dec</span></span><span class="text-color-brand-bold">Jan Dec</span></button></div><div class="flex items-center gap-xl text-xs font-bold"><div> January 2021</div><div>74 pages</div></div><div class="flex flex-col text-xs"><ul><li class="space-x-xs break-words"><span>ISBN</span><span>978-3-03943-655-2</span><span class="capitalize"> (Hardback) </span></li><li class="space-x-xs break-words"><span>ISBN</span><span>978-3-03943-656-9</span><span class="capitalize"> (PDF) </span></li></ul></div><div class="text-xs"><a href="https://doi.org/10.3390/books978-3-03943-656-9" rel="noopener noreferrer" class="hover:underline"> https://doi.org/10.3390/books978-3-03943-656-9</a></div><div class="flex w-full flex-wrap items-center gap-md lg:max-w-content"><button class="m-button m-button--lg m-button--primary m-button--full-width rounded max-w-[34%]" type="button" aria-label="Add to cart"><span class="inline-flex h-full w-full items-center gap-2 whitespace-nowrap justify-between"><span></span><svg xmlns="http://www.w3.org/2000/svg" xmlns:xlink="http://www.w3.org/1999/xlink" aria-hidden="true" role="img" data-testid="shopping_bag" weight="400" style="" width="24" height="24" viewBox="0 0 16 16"></svg></span></button><div class="m-button m-button--lg m-button--secondary m-button--link m-button--full-width rounded max-w-[34%]" type="button"><span class="inline-flex h-full w-full items-center gap-2 whitespace-nowrap justify-between"><a href="https://mdpi-res.com/bookfiles/book/3336/Synthesis_and_Characterization_of_Ferroelectrics.pdf?v=1732672922" target="_blank" class="flex h-full w-full items-center !justify-between rounded bg-inherit"> Free Download (PDF) <svg xmlns="http://www.w3.org/2000/svg" xmlns:xlink="http://www.w3.org/1999/xlink" aria-hidden="true" role="img" data-testid="open_in_new" style="" width="24" height="24" viewBox="0 0 16 16"></svg></a></span></div></div><p class="m-text text-sm text-small max-w-content font-bold"><span>This is a Reprint of the Special Issue </span><a href="https://www.mdpi.com/journal/crystals/special_issues/characterization_ferroelectrics" class="text-color-link-bold" target="_blank"><span class="m-rich-text">Synthesis and Characterization of Ferroelectrics</span></a><span> that was published in </span><span></span></p></div><div class="flex flex-wrap items-center gap-xs"><div class="m-tag flex items-center gap-2 rounded py-0.5 h-6 bg-content-subtler text-color-default px-2 rounded-full text-xs"><span class="flex items-center whitespace-nowrap text-xs leading-normal">Chemistry & Materials Science</span></div><div class="m-tag flex items-center gap-2 rounded py-0.5 h-6 bg-content-subtler text-color-default px-2 rounded-full text-xs"><span class="flex items-center whitespace-nowrap text-xs leading-normal">Engineering</span></div><div class="m-tag flex items-center gap-2 rounded py-0.5 h-6 bg-content-subtler text-color-default px-2 rounded-full text-xs"><span class="flex items-center whitespace-nowrap text-xs leading-normal">Environmental & Earth Sciences</span></div></div><div><div><span class="font-bold"></span><span class="m-text text-body font-bold">Summary</span><div class="max-w-content space-y-sm"><div class="m-rich-text text-body">The Special Issue on “Synthesis and Characterization of Ferroelectrics” reports on several physical properties of ferroelectric materials and their technological aspects. Different substitution mechanisms provide ideas toward future improvement of lead-free (Ba,Ca)(Zr,Ti)O3 piezoelectric ceramics, including the electrocaloric effect, fluorescence, and energy storage. It is established that axial and radial element segregation differently influences electrical properties of 0.68Pb(Mg1/3Nb2/3)0.32PbTiO3 (PMN-32PT for short) single crystals. While the electrical properties along the axial direction strongly depend on the PbTiO3 content, the electrical properties along the axial direction are mainly determined by the ratio of Nb and Mg. On the other hand, Fe-substitution of PMN-32PT crystals lead to an enhancement of the coercive field due to wall pinning induced by charged defect dipoles. It is also found, that capacitors based on Pt/Na0.5Bi0.5TiO3/La0.5Sr0.5CoO3 thin films display good fatigue resistance and retention. Another lead-free thin film capacitor fabricated from Ba0.3Sr0.7Zr0.18Ti0.82 features a low leakage current density and high breakdown strength. Such capacitors are essential for energy storage. Furthermore, an enhanced electrocaloric effect on 0.73Pb(Mg1/3Nb2/3)0.27PbTiO3 single crystals is demonstrated. This effect is promising for novel solid-state cooling systems.</div></div></div></div><div class="lg:hidden"><div class="flex flex-col gap-md"><div class="flex flex-col gap-sm"><div><span class="text-xs font-bold">Format</span><ul><li class="space-x-xs text-xs"><span>Hardback</span></li></ul></div><div data-v-2fcfbc20><span class="text-xs font-bold" data-v-2fcfbc20>License and Copyright</span><div class="m-rich-text text-xs" data-v-2fcfbc20>漏 2022 by the authors; CC BY-NC-ND license</div></div><div data-v-2fcfbc20><span class="text-xs font-bold" data-v-2fcfbc20>Keywords</span><div class="m-rich-text text-xs" data-v-2fcfbc20>PMN-32PT; characterization; segregation; Bridgman technique; ferroelectric materials; piezoelectric; ceramic; lead-free; PMN-32PT single crystal; acceptor doping; charged defects; dielectric relaxation; electrical conduction; NBT epitaxial film; ferroelectric properties; ultraviolet light; BSZT thin films; capacitance properties; RF magnetron sputtering; PMN-PT; single crystals; P鈥揈 hysteresis loop; electrocaloric effect; Maxwell relation; n/a</div></div><button class="flex cursor-pointer flex-row items-center gap-sm" type="button"><span class="text-xs font-bold"> Order & Delivery </span><svg xmlns="http://www.w3.org/2000/svg" xmlns:xlink="http://www.w3.org/1999/xlink" aria-hidden="true" role="img" data-testid="report" style="" width="16" height="16" viewBox="0 0 16 16"></svg></button></div></div></div></div></div></main></div><div class="w-full bg-surface-subtle pt-2xl"><div class="m-container mx-auto block pb-section-mobile lg:pb-section-desktop" style="--container-ideal-width:95vw;"><h2 class="m-heading text-inherit m-h4 font-light mb-xl"> Related Books </h2><div class="swiper"><div class="swiper-wrapper"><div class="swiper-slide max-w-[80%] rounded bg-white p-lg lg:max-w-[25%] lg:max-w-[23%]"><div data-score="89.017" class="relative h-[200px] overflow-hidden lg:max-h-[300px]"><span class="m-text text-sm font-medium">December 2022</span><a 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