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(PDF) Nanometric ultracapacitors fabricated using multilayer of conducting polymers on self-assembled octanethiol monolayers | Jose Iribarren - Academia.edu
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[{"id":48747181,"identifier":"Attachment_48747181","shouldShowBulkDownload":false}]; window.loswp.shouldDetectTimezone = true; window.loswp.shouldShowBulkDownload = true; window.loswp.showSignupCaptcha = false window.loswp.willEdgeCache = false; window.loswp.work = {"work":{"id":28406445,"created_at":"2016-09-11T04:52:41.195-07:00","from_world_paper_id":157381334,"updated_at":"2024-11-14T19:33:59.156-08:00","_data":{"grobid_abstract":"Symmetric ultracapacitors have been fabricated considering nanometric 3-layered films made of alternated layers of poly(3,4-ethylenedioxythiophene) (external and internal layers) and polypyrrole (intermediate layer) deposited on steel uncoated and coated with octanethiol self-assembled monolayer. The highest electrochemical and capacitance parameters (i.e. electroactivity, doping level, stored charge, specific capacitance, Coulomb efficiency, energy density and power density) correspond to the ultracapacitor derived from the assembly of 3-layered films deposited on pre-treated steel. Thus, the interface separating the octanethiol monolayer and the most internal layer of the 3-layered film produces a very favorable interaction, which promotes important electrochemical benefits similar to those found for the interfaces in conventional multilayered films. Moreover, the pre-treatment of the steel electrode enhances the roughness and porosity of the film deposited on it, transmitting this effect layer-by-layer. Structural and morphological characteristics, which have been characterized using scanning electron microscopy and atomic force microscopy, have been related with the electrochemical and capacitance properties of the ultracapacitors.","publication_date":"2013,,","publication_name":"Organic Electronics","grobid_abstract_attachment_id":"48747181"},"document_type":"paper","pre_hit_view_count_baseline":null,"quality":"high","language":"en","title":"Nanometric ultracapacitors fabricated using multilayer of conducting polymers on self-assembled octanethiol monolayers","broadcastable":false,"draft":null,"has_indexable_attachment":true,"indexable":true}}["work"]; window.loswp.workCoauthors = [53252628]; window.loswp.locale = "en"; window.loswp.countryCode = "SG"; window.loswp.cwvAbTestBucket = ""; window.loswp.designVariant = "ds_vanilla"; window.loswp.fullPageMobileSutdModalVariant = "full_page_mobile_sutd_modal"; window.loswp.useOptimizedScribd4genScript = false; window.loswp.appleClientId = 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href="https://www.academia.edu/15065824/Electrochemical_Characterization_of_Chemically_Synthesized_Polythiophene_Thin_Films_Performance_of_Asymmetric_Supercapacitor_Device_B_H">Electrochemical Characterization of Chemically Synthesized Polythiophene Thin Films: Performance of Asymmetric Supercapacitor Device B. H.</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="34205525" href="https://independent.academia.edu/ChandrakantLokhande">Chandrakant Lokhande</a><span>, </span><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="34094136" href="https://independent.academia.edu/SwatiPatil30">Swati Patil</a></div><p class="ds-related-work--abstract ds2-5-body-sm">Polythiophene (PT) thin films have been prepared by chemical bath deposition (CBD) method at room temperature (300 K) via oxidative polymerization of thiophene using ammonium peroxodisulfate (APS) as an oxidizing agent. Globular particulates of PT are deposited on the stainless steel and glass substrates. The morphology and chain structure of PT are studied using scanning electron microscopy (SEM) and Raman spectroscopy techniques, respectively. 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class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/82016291/A_new_generation_of_electrochemical_supercapacitors_based_on_layer_by_layer_polymer_films">A new generation of electrochemical supercapacitors based on layer-by-layer polymer films</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="20346725" href="https://ufscar.academia.edu/RogerGon%C3%A7alves">Roger Gonçalves</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Power Sources, 2016</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"A new generation of electrochemical supercapacitors based on layer-by-layer polymer films","attachmentId":87858034,"attachmentType":"pdf","work_url":"https://www.academia.edu/82016291/A_new_generation_of_electrochemical_supercapacitors_based_on_layer_by_layer_polymer_films","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/82016291/A_new_generation_of_electrochemical_supercapacitors_based_on_layer_by_layer_polymer_films"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="2" data-entity-id="82016293" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" 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class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/113195648/Free_Standing_Flexible_Nanofeatured_Polymeric_Films_Prepared_by_Spin_Coating_and_Anodic_Polymerization_as_Electrodes_for_Supercapacitors">Free-Standing, Flexible Nanofeatured Polymeric Films Prepared by Spin-Coating and Anodic Polymerization as Electrodes for Supercapacitors</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="33535317" href="https://independent.academia.edu/Torras">Juan Torras</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Molecules, 2021</p><p class="ds-related-work--abstract ds2-5-body-sm">Flexible and self-standing multilayered films made of nanoperforated poly(lactic acid) (PLA) layers separated by anodically polymerized poly(3,4-ethylenedioxythiophene) (PEDOT) conducting layers have been prepared and used as electrodes for supercapacitors. 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Santiago-Aviles</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Physics: Conference Series, 2013</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Electrochemical characterization of poly-(3,4 propylene-dioxythiophene) pseudo-capacitor","attachmentId":98834631,"attachmentType":"pdf","work_url":"https://www.academia.edu/97126810/Electrochemical_characterization_of_poly_3_4_propylene_dioxythiophene_pseudo_capacitor","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/97126810/Electrochemical_characterization_of_poly_3_4_propylene_dioxythiophene_pseudo_capacitor"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="6" data-entity-id="116004792" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/116004792/Fabrication_and_Characterization_of_Flexible_Solid_Polymers_Electrolytes_for_Supercapacitor_Application">Fabrication and Characterization of Flexible Solid Polymers Electrolytes for Supercapacitor Application</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="127128141" href="https://uwasa.academia.edu/TheodoreAzemtsopManfo">Theodore Azemtsop Manfo</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Polymers, 2022</p><p class="ds-related-work--abstract ds2-5-body-sm">: In this work, solid flexible polymer blend electrolytes (PBE) composed of polyvinyl alcohol (PVA) and polyvinyl pyrrolidone (PVP) with different amounts of sodium thiocyanate (NaSCN) salt mixed in double-distilled water (solvent) are prepared via solution casting method. The obtained films are characterized using several techniques. The study of the surface morphology of the polymer blend salt complex films via the POM technique reveals the presence of amorphous regions due to the NaSCN effect. FTIR spectra studies confirm the complex formation between PVA, PVP, and NaSCN. The addition of 20 wt% NaSCN salt in the composition PVA: PVP (50:50 wt%) polymer blend matrix leads to an increase in the number of charge carriers and thus improves the ionic conductivity. The ionic conductivity of each polymer blend electrolyte was studied using the electrochemical impedance spectroscopy (EIS) method. The highest room temperature ionic conductivity of 8.1 × 10−5 S/cm S cm−1 is obtained for the composition of PVA: PVP (50:50 wt%) with 20 wt% NaSCN. LSV test shows the optimized ion-conducting polymer blend electrolyte is electrochemically stable up to 1.5 V. TNM analysis reveals that 99% of ions contribute for the conductivity against 1% of electrons only in the highly conductive polymer electrolyte PVA: PVP (50:50 wt%) + 20 wt% NaSCN. A supercapacitor device was fabricated using the optimized ion-conducting polymer blend film and graphene oxide (GO) coated electrodes. The GCD curve clearly reveals the behavior of an ideal capacitor with less Faradic process and low ESR value. The columbic efficiency of the GO-based system is found to be 100%, the GO-based electrode exhibits a specific capacitance of 12.15 F/g and the system delivers the charge for a long duration. The specific capacitance of the solid-state supercapacitor cell was found to be 13.28 F/g via the CV approach close to 14.25 F/g obtained with EIS data at low frequency</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Fabrication and Characterization of Flexible Solid Polymers Electrolytes for Supercapacitor Application","attachmentId":112254886,"attachmentType":"pdf","work_url":"https://www.academia.edu/116004792/Fabrication_and_Characterization_of_Flexible_Solid_Polymers_Electrolytes_for_Supercapacitor_Application","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/116004792/Fabrication_and_Characterization_of_Flexible_Solid_Polymers_Electrolytes_for_Supercapacitor_Application"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="7" data-entity-id="65079144" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/65079144/High_performance_of_symmetrical_supercapacitor_based_on_multilayer_films_of_graphene_oxide_polypyrrole_electrodes">High performance of symmetrical supercapacitor based on multilayer films of graphene oxide/polypyrrole electrodes</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="152202727" href="https://independent.academia.edu/MarisolSalas12">Marisol Salas</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Applied Surface Science, 2014</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"High performance of symmetrical supercapacitor based on multilayer films of graphene oxide/polypyrrole electrodes","attachmentId":76822935,"attachmentType":"pdf","work_url":"https://www.academia.edu/65079144/High_performance_of_symmetrical_supercapacitor_based_on_multilayer_films_of_graphene_oxide_polypyrrole_electrodes","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/65079144/High_performance_of_symmetrical_supercapacitor_based_on_multilayer_films_of_graphene_oxide_polypyrrole_electrodes"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="8" data-entity-id="14217863" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/14217863/Effect_of_Triton_X_100_on_the_double_layer_capacitance_and_conductivity_of_poly_3_4_ethylenedioxythiophene_poly_styrenesulfonate_PEDOT_PSS_films">Effect of Triton X-100 on the double layer capacitance and conductivity of poly(3,4-ethylenedioxythiophene):poly(styrenesulfonate) (PEDOT:PSS) films</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="33202476" href="https://usf.academia.edu/ArashTakshi">Arash Takshi</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Synthetic Metals, 2014</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Effect of Triton X-100 on the double layer capacitance and conductivity of poly(3,4-ethylenedioxythiophene):poly(styrenesulfonate) (PEDOT:PSS) films","attachmentId":44453513,"attachmentType":"pdf","work_url":"https://www.academia.edu/14217863/Effect_of_Triton_X_100_on_the_double_layer_capacitance_and_conductivity_of_poly_3_4_ethylenedioxythiophene_poly_styrenesulfonate_PEDOT_PSS_films","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/14217863/Effect_of_Triton_X_100_on_the_double_layer_capacitance_and_conductivity_of_poly_3_4_ethylenedioxythiophene_poly_styrenesulfonate_PEDOT_PSS_films"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="9" data-entity-id="34436853" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/34436853/Hybrid_supercapacitor_materials_from_poly_3_4_ethylenedioxythiophene_conformally_coated_aligned_carbon_nanotubes">Hybrid supercapacitor materials from poly(3,4-ethylenedioxythiophene) conformally coated aligned carbon nanotubes</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="27541667" href="https://psu-us.academia.edu/MehdiGhaffari">Mehdi Ghaffari</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Electrochimica Acta, 2013</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Hybrid supercapacitor materials from poly(3,4-ethylenedioxythiophene) conformally coated aligned carbon nanotubes","attachmentId":54312062,"attachmentType":"pdf","work_url":"https://www.academia.edu/34436853/Hybrid_supercapacitor_materials_from_poly_3_4_ethylenedioxythiophene_conformally_coated_aligned_carbon_nanotubes","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" 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You can download the paper by clicking the button above.</p></div></div></div></div><div class="ds-sidebar--container js-work-sidebar"><div class="ds-related-content--container"><h2 class="ds-related-content--heading">Related papers</h2><div class="ds-related-work--container js-related-work-sidebar-card" data-collection-position="0" data-entity-id="7099736" data-sort-order="default"><a class="ds-related-work--title js-related-work-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/7099736/Conducting_polymers_as_electrode_materials_in_supercapacitors">Conducting polymers as electrode materials in supercapacitors</a><div class="ds-related-work--metadata"><a class="js-related-work-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="12201067" href="https://unibo.academia.edu/FrancescaSoavi">Francesca Soavi</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Solid State Ionics, 2002</p><div class="ds-related-work--ctas"><button 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data-collection-position="14" data-entity-id="50697571" data-sort-order="default"><a class="ds-related-work--title js-related-work-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/50697571/Poly_3_4_ethylenedioxythiophene_Doped_with_Carbon_Materials_for_High_Performance_Supercapacitor_A_Comparison_Study">Poly(3,4-ethylenedioxythiophene) Doped with Carbon Materials for High-Performance Supercapacitor: A Comparison Study</a><div class="ds-related-work--metadata"><a class="js-related-work-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="56109094" href="https://independent.academia.edu/YusranSulaiman">Yusran Sulaiman</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Nanomaterials, 2017</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Poly(3,4-ethylenedioxythiophene) Doped with 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