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data-landing_url="https://www.academia.edu/71703801/A_high_pressure_macromolecular_crystallography_capability_developed_at_CHESS" data-login_uri="https://www.academia.edu/registrations/google_one_tap" data-moment_callback="onGoogleOneTapEvent" id="g_id_onload"></div><div class="ds-top-related-works--grid-container"><div class="ds-related-content--container ds-top-related-works--container"><h2 class="ds-related-content--heading">Related papers</h2><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="0" data-entity-id="19260035" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/19260035/Energy_recovery_linac_ERL_coherent_hard_x_ray_sources">Energy recovery linac (ERL) coherent hard x-ray sources</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="39405758" href="https://independent.academia.edu/KenFinkelstein">Ken Finkelstein</a></div><p class="ds-related-work--metadata ds2-5-body-xs">New Journal of Physics, 2010</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Energy recovery linac (ERL) coherent hard x-ray sources","attachmentId":40521231,"attachmentType":"pdf","work_url":"https://www.academia.edu/19260035/Energy_recovery_linac_ERL_coherent_hard_x_ray_sources","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/19260035/Energy_recovery_linac_ERL_coherent_hard_x_ray_sources"><span class="ds2-5-text-link__content">View PDF</span><span 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However, OA relies on energetically favorable nanocrystal facets to grow nanostructured materials. Consequently, nanostructures synthesized through OA are generally limited to a specific crystal facet in their final morphology. We report our discovery that high-pressure compression can induce consolidation of spherical CdSe nanocrystal arrays, leading to unexpected one-dimensional semiconductor nanowires that do not exhibit the typical crystal facet. In particular, in situ high-pressure synchrotron x-ray scattering, optical spectroscopy, and high-resolution transmission electron microscopy characterizations indicate that by manipulating the coupling between nanocrystals through external pressure, a reversible change in nanocrystal assemblies and properties can be achieved at modest pressure. When pressure is increased above a threshold, these nanoc...</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Pressure compression of CdSe nanoparticles into luminescent nanowires","attachmentId":71573654,"attachmentType":"pdf","work_url":"https://www.academia.edu/55944554/Pressure_compression_of_CdSe_nanoparticles_into_luminescent_nanowires","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/55944554/Pressure_compression_of_CdSe_nanoparticles_into_luminescent_nanowires"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="2" data-entity-id="58804503" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/58804503/Microcrystallography_high_pressure_cryocooling_and_BioSAXS_at_MacCHESS">Microcrystallography, high-pressure cryocooling and BioSAXS at MacCHESS</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="33002650" href="https://cornell.academia.edu/DolethaSzebenyi">Doletha Szebenyi</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Synchrotron Radiation, 2011</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Microcrystallography, high-pressure 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href="https://www.academia.edu/53569964/Phase_stability_of_TiH2_under_high_pressure_and_temperatures">Phase stability of TiH2 under high pressure and temperatures</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="49525735" href="https://independent.academia.edu/SelvaVennilaRaju">Selva Vennila Raju</a></div><p class="ds-related-work--metadata ds2-5-body-xs">International Journal of Hydrogen Energy, 2008</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Phase stability of TiH2 under high pressure and temperatures","attachmentId":70352594,"attachmentType":"pdf","work_url":"https://www.academia.edu/53569964/Phase_stability_of_TiH2_under_high_pressure_and_temperatures","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/53569964/Phase_stability_of_TiH2_under_high_pressure_and_temperatures"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="4" data-entity-id="55879100" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/55879100/In_situ_microfluidic_dialysis_for_biological_small_angle_X_ray_scattering">In situ microfluidic dialysis for biological small-angle X-ray scattering</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="39280269" href="https://independent.academia.edu/BenteVestergaard">Bente Vestergaard</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Applied Crystallography, 2014</p><p class="ds-related-work--abstract ds2-5-body-sm">Owing to the demand for low sample consumption and automated sample changing capabilities at synchrotron small-angle X-ray (solution) scattering (SAXS) beamlines, X-ray microfluidics is receiving continuously increasing attention. Here, a remote-controlled microfluidic device is presented for simultaneous SAXS and ultraviolet absorption measurements during protein dialysis, integrated directly on a SAXS beamline. Microfluidic dialysis can be used for monitoring structural changes in response to buffer exchange or, as demonstrated, protein concentration. By collecting X-ray data during the concentration procedure, the risk of inducing protein aggregation due to excessive concentration and storage is eliminated, resulting in reduced sample consumption and improved data quality. The proof of concept demonstrates the effect of halted or continuous flow in the microfluidic device. No sample aggregation was induced by the concentration process at the levels achieved in these experiments. ...</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"In situ microfluidic dialysis for biological small-angle X-ray scattering","attachmentId":71539595,"attachmentType":"pdf","work_url":"https://www.academia.edu/55879100/In_situ_microfluidic_dialysis_for_biological_small_angle_X_ray_scattering","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/55879100/In_situ_microfluidic_dialysis_for_biological_small_angle_X_ray_scattering"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="5" data-entity-id="47833120" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/47833120/Confocal_microscopy_on_the_beamline_novel_three_dimensional_imaging_and_sample_positioning">Confocal microscopy on the beamline: novel three-dimensional imaging and sample positioning</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="32906228" href="https://independent.academia.edu/WarrenZipfel">Warren Zipfel</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Journal of Applied Crystallography, 2012</p><p class="ds-related-work--abstract ds2-5-body-sm">Confocal microscopy, a technique that has been extensively applied in cellular biological studies, may also be applied to the visualization and three-dimensional imaging of protein crystals at high resolution on synchrotron beamlines. Protein crystal samples are examined using a commercially available confocal microscope adapted for cryogenic use. A preliminary test using a custom confocal design adapted for beamline use is also presented. The confocal optics configuration is compatible with nonlinear imaging techniques such as two-photon excited fluorescence imaging and second harmonic generation. The possibilities of this method are explored using two modes: fluorescence and reflection confocal. In fluorescence mode, small amounts of dye are introduced into the crystal through soaking or growth conditions. Under such conditions, protein crystals are easily resolved from salts and amorphous precipitates, which do not generally take up dye. Reflection mode, which does not require dy...</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Confocal microscopy on the beamline: novel three-dimensional imaging and sample positioning","attachmentId":66752629,"attachmentType":"pdf","work_url":"https://www.academia.edu/47833120/Confocal_microscopy_on_the_beamline_novel_three_dimensional_imaging_and_sample_positioning","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/47833120/Confocal_microscopy_on_the_beamline_novel_three_dimensional_imaging_and_sample_positioning"><span class="ds2-5-text-link__content">View PDF</span><span 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at high pressures","attachmentId":46317394,"attachmentType":"pdf","work_url":"https://www.academia.edu/25966422/Structural_behavior_of_Sr2Bi2O5_at_high_pressures","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/25966422/Structural_behavior_of_Sr2Bi2O5_at_high_pressures"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="7" data-entity-id="69395583" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/69395583/Reconstructing_a_solid_solid_phase_transformation_pathway_in_CdSe_nanosheets_with_associated_soft_ligands">Reconstructing a solid-solid phase transformation pathway in CdSe nanosheets with associated soft ligands</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="72945078" href="https://independent.academia.edu/DetlefSmilgies">Detlef Smilgies</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Proceedings of the National Academy of Sciences, 2010</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Reconstructing a solid-solid phase transformation pathway in CdSe nanosheets with associated soft 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