Growth and Characterization of Bis-Thiourea Nickel Barium Chloride Single Crystals

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Bis-Thiourea Nickel Barium Chloride Single Crystals</title> <meta name="description" content="Growth and Characterization of Bis-Thiourea Nickel Barium Chloride Single Crystals"> <meta name="keywords" content="crystal growth, dielectric study, optical parameters, organo-metallic crystals, powder xrd, slow evaporation technique, TGA"> <meta name="viewport" content="width=device-width, initial-scale=1, minimum-scale=1, maximum-scale=1, user-scalable=no"> <meta charset="utf-8"> <link href="https://cdn.waset.org/favicon.ico" type="image/x-icon" rel="shortcut icon"> <link href="https://cdn.waset.org/static/plugins/bootstrap-4.2.1/css/bootstrap.min.css" rel="stylesheet"> <link href="https://cdn.waset.org/static/plugins/fontawesome/css/all.min.css" rel="stylesheet"> <link href="https://cdn.waset.org/static/css/site.css?v=150220211555" rel="stylesheet"> </head> <body> <header> <div class="container"> <nav class="navbar navbar-expand-lg navbar-light"> <a class="navbar-brand" 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</div> <div class="card publication-listing mt-3 mb-3"> <h5 class="card-header" style="font-size:.9rem">Growth and Characterization of Bis-Thiourea Nickel Barium Chloride Single Crystals</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Rakesh%20Hajiyani">Rakesh Hajiyani</a>, <a href="https://publications.waset.org/abstracts/search?q=Chetan%20Chauhan"> Chetan Chauhan</a>, <a href="https://publications.waset.org/abstracts/search?q=Harshkant%20Jethva"> Harshkant Jethva</a>, <a href="https://publications.waset.org/abstracts/search?q=Mihir%20Joshi"> Mihir Joshi</a> </p> <p class="card-text"><strong>Abstract:</strong></p> Metal bis-thiourea type organo-metallic crystals are popular as non-linear optical materials. Bis-thiourea nickel barium chloride was synthesized and crystals were grown by slow aqueous solvent evaporation technique. The transparent and colorless crystals having maximum dimensions of 13 mm x 8 mm x 2.2 mm were obtained. The EDAX was carried out to estimate the content of nickel and barium in the grown crystals. The powder XRD analysis suggested orthorhombic crystal structure with unit cell parameters as: a= 9.70 脜, b= 10.68 脜 and c= 17.95 脜. The FTIR spectroscopy study confirmed the presence of various functional groups. The UV-vis spectroscopy study indicated that the crystals were transparent in the visible region with 90% transmittance level further optical parameters were studied. From the TGA it was found that the crystals remained stable up to 170 0C and then decomposed through two decomposition stages. The dielectric study was carried out in the frequency range of applied field from 500 Hz to 1 MHz. The variations of dielectric constant, dielectric loss were studied with frequency. It was found that the dielectric constant and the dielectric loss decreased as the frequency of applied field increased. The results are discussed. <iframe src="https://publications.waset.org/abstracts/36334.pdf" style="width:100%; height:400px;" frameborder="0"></iframe> <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=crystal%20growth" title="crystal growth">crystal growth</a>, <a href="https://publications.waset.org/abstracts/search?q=dielectric%20study" title=" dielectric study"> dielectric study</a>, <a href="https://publications.waset.org/abstracts/search?q=optical%20parameters" title=" optical parameters"> optical parameters</a>, <a href="https://publications.waset.org/abstracts/search?q=organo-metallic%20crystals" title=" organo-metallic crystals"> organo-metallic crystals</a>, <a href="https://publications.waset.org/abstracts/search?q=powder%20xrd" title=" powder xrd"> powder xrd</a>, <a href="https://publications.waset.org/abstracts/search?q=slow%20evaporation%20technique" title=" slow evaporation technique"> slow evaporation technique</a>, <a href="https://publications.waset.org/abstracts/search?q=TGA" title=" TGA"> TGA</a> </p> <a href="https://publications.waset.org/abstracts/36334/growth-and-characterization-of-bis-thiourea-nickel-barium-chloride-single-crystals" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/36334.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">450</span> </span> </div> </div> </div> </main> <footer> <div id="infolinks" class="pt-3 pb-2"> <div class="container"> <div style="background-color:#f5f5f5;" class="p-3"> <div class="row"> <div class="col-md-2"> <ul class="list-unstyled"> About <li><a href="https://waset.org/page/support">About Us</a></li> <li><a href="https://waset.org/page/support#legal-information">Legal</a></li> <li><a target="_blank" rel="nofollow" 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Growth and Characterization of Bis-Thiourea Nickel Barium Chloride Single Crystals