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Senberber</title> <meta name="description" content="Search results for: F. T. Senberber"> <meta name="keywords" content="F. T. Senberber"> <meta name="viewport" content="width=device-width, initial-scale=1, minimum-scale=1, maximum-scale=1, user-scalable=no"> <meta charset="utf-8"> <link href="https://cdn.waset.org/favicon.ico" type="image/x-icon" rel="shortcut icon"> <link href="https://cdn.waset.org/static/plugins/bootstrap-4.2.1/css/bootstrap.min.css" rel="stylesheet"> <link href="https://cdn.waset.org/static/plugins/fontawesome/css/all.min.css" rel="stylesheet"> <link href="https://cdn.waset.org/static/css/site.css?v=150220211555" rel="stylesheet"> </head> <body> <header> <div class="container"> <nav class="navbar navbar-expand-lg navbar-light"> <a class="navbar-brand" href="https://waset.org"> <img src="https://cdn.waset.org/static/images/wasetc.png" alt="Open Science Research Excellence" title="Open Science Research Excellence" /> </a> <button class="d-block d-lg-none navbar-toggler ml-auto" type="button" data-toggle="collapse" data-target="#navbarMenu" aria-controls="navbarMenu" aria-expanded="false" aria-label="Toggle navigation"> <span class="navbar-toggler-icon"></span> </button> <div class="w-100"> <div class="d-none d-lg-flex flex-row-reverse"> <form method="get" action="https://waset.org/search" class="form-inline my-2 my-lg-0"> <input class="form-control mr-sm-2" type="search" placeholder="Search Conferences" value="F. 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T. Senberber"> <input type="submit" class="btn_search" value="Search"> </div> </div> </form> </div> </div> <div class="row mt-3"> <div class="col-sm-3"> <div class="card"> <div class="card-body"><strong>Commenced</strong> in January 2007</div> </div> </div> <div class="col-sm-3"> <div class="card"> <div class="card-body"><strong>Frequency:</strong> Monthly</div> </div> </div> <div class="col-sm-3"> <div class="card"> <div class="card-body"><strong>Edition:</strong> International</div> </div> </div> <div class="col-sm-3"> <div class="card"> <div class="card-body"><strong>Paper Count:</strong> 7</div> </div> </div> </div> <h1 class="mt-3 mb-3 text-center" style="font-size:1.6rem;">Search results for: F. T. Senberber</h1> <div class="card publication-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">7</span> The Effect of Solution Density on the Synthesis of Magnesium Borate from Boron-Gypsum</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/search?q=N.%20Tugrul">N. Tugrul</a>, <a href="https://publications.waset.org/search?q=E.%20Sariburun"> E. Sariburun</a>, <a href="https://publications.waset.org/search?q=F.%20T.%20Senberber"> F. T. Senberber</a>, <a href="https://publications.waset.org/search?q=A.%20S.%20Kipcak"> A. S. Kipcak</a>, <a href="https://publications.waset.org/search?q=E.%20Moroydor%20Derun"> E. Moroydor Derun</a>, <a href="https://publications.waset.org/search?q=S.%20Piskin"> S. Piskin</a> </p> <p class="card-text"><strong>Abstract:</strong></p> <p>Boron-gypsum is a waste which occurs in the boric acid production process. In this study, the boron content of this waste is evaluated for the use in synthesis of magnesium borates and such evaluation of this kind of waste is useful more than storage or disposal. Magnesium borates, which are a sub-class of boron minerals, are useful additive materials for the industries due to their remarkable thermal and mechanical properties. Magnesium borates were obtained hydrothermally at different temperatures. Novelty of this study is the search of the solution density effects to magnesium borate synthesis process for the increasing the possibility of borongypsum usage as a raw material. After the synthesis process, products are subjected to XRD and FT-IR to identify and characterize their crystal structure, respectively.</p> <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/search?q=Boron-gypsum" title="Boron-gypsum">Boron-gypsum</a>, <a href="https://publications.waset.org/search?q=hydrothermal%20synthesis" title=" hydrothermal synthesis"> hydrothermal synthesis</a>, <a href="https://publications.waset.org/search?q=magnesium%0D%0Aborate" title=" magnesium borate"> magnesium borate</a>, <a href="https://publications.waset.org/search?q=solution%20density." title=" solution density."> solution density.</a> </p> <a href="https://publications.waset.org/9999536/the-effect-of-solution-density-on-the-synthesis-of-magnesium-borate-from-boron-gypsum" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/9999536/apa" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">APA</a> <a href="https://publications.waset.org/9999536/bibtex" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">BibTeX</a> <a href="https://publications.waset.org/9999536/chicago" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">Chicago</a> <a href="https://publications.waset.org/9999536/endnote" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">EndNote</a> <a href="https://publications.waset.org/9999536/harvard" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">Harvard</a> <a href="https://publications.waset.org/9999536/json" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">JSON</a> <a href="https://publications.waset.org/9999536/mla" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">MLA</a> <a href="https://publications.waset.org/9999536/ris" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">RIS</a> <a href="https://publications.waset.org/9999536/xml" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">XML</a> <a href="https://publications.waset.org/9999536/iso690" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">ISO 690</a> <a href="https://publications.waset.org/9999536.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">2159</span> </span> </div> </div> <div class="card publication-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">6</span> Evaluation of the Magnesium Wastes with Boron Oxide in Magnesium Borate Synthesis</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/search?q=A.%20S.%20Kipcak">A. S. Kipcak</a>, <a href="https://publications.waset.org/search?q=F.%20T.%20Senberber"> F. T. Senberber</a>, <a href="https://publications.waset.org/search?q=E.%20Moroydor%20Derun"> E. Moroydor Derun</a>, <a href="https://publications.waset.org/search?q=S.%20Piskin"> S. Piskin</a> </p> <p class="card-text"><strong>Abstract:</strong></p> <p>Magnesium wastes and scraps, one of the metal wastes, are produced by many industrial activities, all over the world. Their growing size is becoming a future problem for the world. In this study, the use of magnesium wastes as a raw material in the production of the magnesium borate hydrates are aimed. The method used in the experiments is hydrothermal synthesis. The conditions are set to, waste magnesium to B2O3, 1:3 as a molar ratio. Four different reaction times are studied which are 30, 60, 120 and 240 minutes. For the identification analyses X-Ray Diffraction (XRD), Fourier Transform Infrared Spectroscopy (FT-IR) and Raman spectroscopy techniques are used. As a result at all the reaction times magnesium borate hydrates are synthesized and the most crystalline forms are obtained at a reaction time of 120 minutes. The overall yields of the production are found between the values of 65-80 %.</p> <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/search?q=Hydrothermal%20synthesis" title="Hydrothermal synthesis">Hydrothermal synthesis</a>, <a href="https://publications.waset.org/search?q=magnesium%20borates" title=" magnesium borates"> magnesium borates</a>, <a href="https://publications.waset.org/search?q=magnesium%20wastes" title=" magnesium wastes"> magnesium wastes</a>, <a href="https://publications.waset.org/search?q=boron%20oxide" title=" boron oxide"> boron oxide</a> </p> <a href="https://publications.waset.org/2151/evaluation-of-the-magnesium-wastes-with-boron-oxide-in-magnesium-borate-synthesis" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/2151/apa" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">APA</a> <a href="https://publications.waset.org/2151/bibtex" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">BibTeX</a> <a href="https://publications.waset.org/2151/chicago" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">Chicago</a> <a href="https://publications.waset.org/2151/endnote" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">EndNote</a> <a href="https://publications.waset.org/2151/harvard" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">Harvard</a> <a href="https://publications.waset.org/2151/json" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">JSON</a> <a href="https://publications.waset.org/2151/mla" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">MLA</a> <a href="https://publications.waset.org/2151/ris" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">RIS</a> <a href="https://publications.waset.org/2151/xml" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">XML</a> <a href="https://publications.waset.org/2151/iso690" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">ISO 690</a> <a href="https://publications.waset.org/2151.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">2337</span> </span> </div> </div> <div class="card publication-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">5</span> The Optimization of Copper Sulfate and Tincalconite Molar Ratios on the Hydrothermal Synthesis of Copper Borates</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/search?q=E.%20Moroydor%20Derun">E. Moroydor Derun</a>, <a href="https://publications.waset.org/search?q=N.%20Tugrul"> N. Tugrul</a>, <a href="https://publications.waset.org/search?q=F.%20T.%20Senberber"> F. T. Senberber</a>, <a href="https://publications.waset.org/search?q=A.%20S.%20Kipcak"> A. S. Kipcak</a>, <a href="https://publications.waset.org/search?q=S.%20Piskin"> S. Piskin</a> </p> <p class="card-text"><strong>Abstract:</strong></p> <p>In this research, copper borates are synthesized by the reaction of copper sulfate pentahydrate (CuSO4.5H2O) and tincalconite (Na2O4B7.10H2O). The experimental parameters are selected as 80oC reaction temperature and 60 of reaction time. The effect of mole ratio of CuSO4.5H2O to Na2O4B7.5H2O is studied. For the identification analyses X-Ray Diffraction (XRD) and Fourier Transform Infrared Spectroscopy (FT-IR) techniques are used. At the end of the experiments, synthesized copper borate is matched with the powder diffraction file of “00-001-0472” [Cu(BO2)2] and characteristic vibrations between B and O atoms are seen. The proper crystals are obtained at the mole ratio of 3:1. This study showed that simplified synthesis process is suitable for the production of copper borate minerals.</p> <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/search?q=Hydrothermal%20synthesis" title="Hydrothermal synthesis">Hydrothermal synthesis</a>, <a href="https://publications.waset.org/search?q=copper%20borates" title=" copper borates"> copper borates</a>, <a href="https://publications.waset.org/search?q=copper%0D%0Asulfate" title=" copper sulfate"> copper sulfate</a>, <a href="https://publications.waset.org/search?q=tincalconite." title=" tincalconite."> tincalconite.</a> </p> <a href="https://publications.waset.org/9999594/the-optimization-of-copper-sulfate-and-tincalconite-molar-ratios-on-the-hydrothermal-synthesis-of-copper-borates" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/9999594/apa" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">APA</a> <a href="https://publications.waset.org/9999594/bibtex" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">BibTeX</a> <a href="https://publications.waset.org/9999594/chicago" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">Chicago</a> <a href="https://publications.waset.org/9999594/endnote" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">EndNote</a> <a href="https://publications.waset.org/9999594/harvard" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">Harvard</a> <a href="https://publications.waset.org/9999594/json" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">JSON</a> <a href="https://publications.waset.org/9999594/mla" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">MLA</a> <a href="https://publications.waset.org/9999594/ris" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">RIS</a> <a href="https://publications.waset.org/9999594/xml" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">XML</a> <a href="https://publications.waset.org/9999594/iso690" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">ISO 690</a> <a href="https://publications.waset.org/9999594.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">3509</span> </span> </div> </div> <div class="card publication-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">4</span> Microwave Dehydration Behavior of Admontite Mineral at 360W</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/search?q=E.%20Moroydor%20Derun">E. Moroydor Derun</a>, <a href="https://publications.waset.org/search?q=F.%20T.%20Senberber"> F. T. Senberber</a>, <a href="https://publications.waset.org/search?q=A.%20S.%20Kipcak"> A. S. Kipcak</a>, <a href="https://publications.waset.org/search?q=N.%20Tugrul"> N. Tugrul</a>, <a href="https://publications.waset.org/search?q=S.%20Piskin"> S. Piskin</a> </p> <p class="card-text"><strong>Abstract:</strong></p> <p>Dehydration behavior gives a hint about thermal properties of materials. It is important for the usage areas and transportation of minerals. Magnesium borates can be used as additive materials in areas such as in the production of superconducting materials, in the composition of detergents, due to the content of boron in the friction-reducing additives in oils and insulating coating compositions due to their good mechanic and thermal properties. In this study, thermal dehydration behavior of admontite (MgO(B2O3)3.7(H2O)), which is a kind of magnesium borate mineral, is experimented by microwave energy at 360W. Structure of admontite is suitable for the investigation of dehydration behavior by microwave because of its seven moles of crystal water. It is seen that admontite lost its 28.7% of weight at the end of the 120 minutes heating in microwave furnace. </p> <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/search?q=Admontite" title="Admontite">Admontite</a>, <a href="https://publications.waset.org/search?q=dehydration" title=" dehydration"> dehydration</a>, <a href="https://publications.waset.org/search?q=magnesium%20borate" title=" magnesium borate"> magnesium borate</a>, <a href="https://publications.waset.org/search?q=microwave." title=" microwave."> microwave.</a> </p> <a href="https://publications.waset.org/16262/microwave-dehydration-behavior-of-admontite-mineral-at-360w" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/16262/apa" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">APA</a> <a href="https://publications.waset.org/16262/bibtex" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">BibTeX</a> <a href="https://publications.waset.org/16262/chicago" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">Chicago</a> <a href="https://publications.waset.org/16262/endnote" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">EndNote</a> <a href="https://publications.waset.org/16262/harvard" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">Harvard</a> <a href="https://publications.waset.org/16262/json" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">JSON</a> <a href="https://publications.waset.org/16262/mla" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">MLA</a> <a href="https://publications.waset.org/16262/ris" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">RIS</a> <a href="https://publications.waset.org/16262/xml" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">XML</a> <a href="https://publications.waset.org/16262/iso690" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">ISO 690</a> <a href="https://publications.waset.org/16262.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">2123</span> </span> </div> </div> <div class="card publication-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">3</span> Synthesis of Magnesium Borates from the Slurries of Magnesium Wastes by Microwave Energy</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/search?q=N.%20Tugrul">N. Tugrul</a>, <a href="https://publications.waset.org/search?q=F.%20T.%20Senberber"> F. T. Senberber</a>, <a href="https://publications.waset.org/search?q=A.%20S.%20Kipcak%20E.%20Moroydor%20Derun"> A. S. Kipcak E. Moroydor Derun</a>, <a href="https://publications.waset.org/search?q=S.%20Piskin"> S. Piskin</a> </p> <p class="card-text"><strong>Abstract:</strong></p> <p>In this research, it is aimed not only microwave synthesis of magnesium borates but also evaluation of magnesium wastes. Synthesis process can be described with the reaction of Mg wastes and boric acid using microwave energy. X-Ray Diffraction (XRD) and Fourier Transform Infrared Spectroscopy (FT-IR) were applied to synthesized minerals. According to XRD results, magnesium borate hydrate mixtures were obtained as mcallisterite (pdf# = 01-070-1902, Mg<sub>2</sub>(B<sub>6</sub>O<sub>7</sub>(OH)<sub>6</sub>)<sub>2</sub>.9(H<sub>2</sub>O)) at higher crystallinity properties was achieved at the mole ratio raw material 1:1. Also, other kinds of magnesium borate hydrates were obtained at lower crystallinity such as admontite (pdf # = 01-076-0540, MgO(B<sub>2</sub>O<sub>3</sub>)<sub>3</sub>.7(H<sub>2</sub>O)), inderite (pdf # = 01-072-2308, 2MgO.3B<sub>2</sub>O<sub>3</sub>.15(H<sub>2</sub>O)) and magnesium borate hydrates (pdf # = 01-076-0539, MgO(B<sub>2</sub>O<sub>3</sub>)<sub>3</sub>.6(H<sub>2</sub>O)). FT-IR spectrums indicated that minor changes were seen at the band values of characteristic stretching in each experiment. At the end of experiments it is seen that using microwave energy may contribute positive effects to design of synthesis process such as reducing reaction time and products at higher crystallinity.</p> <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/search?q=Magnesium%20wastes" title="Magnesium wastes">Magnesium wastes</a>, <a href="https://publications.waset.org/search?q=boric%20acid" title=" boric acid"> boric acid</a>, <a href="https://publications.waset.org/search?q=magnesium%20borate" title=" magnesium borate"> magnesium borate</a>, <a href="https://publications.waset.org/search?q=microwave%20energy." title=" microwave energy. "> microwave energy. </a> </p> <a href="https://publications.waset.org/9998769/synthesis-of-magnesium-borates-from-the-slurries-of-magnesium-wastes-by-microwave-energy" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/9998769/apa" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">APA</a> <a href="https://publications.waset.org/9998769/bibtex" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">BibTeX</a> <a href="https://publications.waset.org/9998769/chicago" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">Chicago</a> <a href="https://publications.waset.org/9998769/endnote" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">EndNote</a> <a href="https://publications.waset.org/9998769/harvard" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">Harvard</a> <a href="https://publications.waset.org/9998769/json" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">JSON</a> <a href="https://publications.waset.org/9998769/mla" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">MLA</a> <a href="https://publications.waset.org/9998769/ris" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">RIS</a> <a href="https://publications.waset.org/9998769/xml" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">XML</a> <a href="https://publications.waset.org/9998769/iso690" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">ISO 690</a> <a href="https://publications.waset.org/9998769.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">2147</span> </span> </div> </div> <div class="card publication-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">2</span> Zinc Borate Synthesis Using Hydrozincite and Boric Acid with Ultrasonic Method</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/search?q=D.%20S.%20Vardar">D. S. Vardar</a>, <a href="https://publications.waset.org/search?q=A.%20S.%20Kipcak"> A. S. Kipcak</a>, <a href="https://publications.waset.org/search?q=F.%20T.%20Senberber"> F. T. Senberber</a>, <a href="https://publications.waset.org/search?q=E.%20M.%20Derun"> E. M. Derun</a>, <a href="https://publications.waset.org/search?q=N.%20Tugrul"> N. Tugrul</a>, <a href="https://publications.waset.org/search?q=S.%20Piskin"> S. Piskin</a> </p> <p class="card-text"><strong>Abstract:</strong></p> Zinc borate is an important inorganic hydrate borate material, which can be used as a flame retardant agent and corrosion resistance material. This compound can loss its structural water content at higher than 290掳C. Due to thermal stability; Zinc Borate can be used as flame retardant at high temperature process of plastic and gum. In this study, the ultrasonic reaction of zinc borates were studied using hydrozincite (Zn5(CO3)2路(OH)6) and boric acid (H3BO3) raw materials. Before the synthesis raw materials were characterized by X-Ray Diffraction (XRD) and Fourier Transform Infrared Spectroscopy (FT-IR). Ultrasonic method is a new application on the zinc borate synthesis. The synthesis parameters were set to 90掳C reaction temperature and 55 minutes of reaction time, with 1:1, 1:2, 1:3, 1:4 and 1:5 molar ratio of starting materials (Zn5(CO3)2路(OH)6 : H3BO3). After the zinc borate synthesis, the products were analyzed by XRD and FT-IR. As a result, optimum molar ratio of 1:5 is determined for the synthesis of zinc borates with ultrasonic method. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/search?q=Borate" title="Borate">Borate</a>, <a href="https://publications.waset.org/search?q=ultrasonic%20method" title=" ultrasonic method"> ultrasonic method</a>, <a href="https://publications.waset.org/search?q=zinc%20borate" title=" zinc borate"> zinc borate</a>, <a href="https://publications.waset.org/search?q=zinc%20borate%0D%0Asynthesis." title=" zinc borate synthesis."> zinc borate synthesis.</a> </p> <a href="https://publications.waset.org/10002670/zinc-borate-synthesis-using-hydrozincite-and-boric-acid-with-ultrasonic-method" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/10002670/apa" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">APA</a> <a href="https://publications.waset.org/10002670/bibtex" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">BibTeX</a> <a href="https://publications.waset.org/10002670/chicago" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">Chicago</a> <a href="https://publications.waset.org/10002670/endnote" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">EndNote</a> <a href="https://publications.waset.org/10002670/harvard" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">Harvard</a> <a href="https://publications.waset.org/10002670/json" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">JSON</a> <a href="https://publications.waset.org/10002670/mla" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">MLA</a> <a href="https://publications.waset.org/10002670/ris" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">RIS</a> <a href="https://publications.waset.org/10002670/xml" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">XML</a> <a href="https://publications.waset.org/10002670/iso690" target="_blank" rel="nofollow" class="btn btn-primary btn-sm">ISO 690</a> <a href="https://publications.waset.org/10002670.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">2064</span> </span> </div> </div> <div class="card publication-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">1</span> The Determination of the Potassium Nitrate, Sodium Hydroxide and Boric Acid Molar Ratio in the Synthesis of Potassium Borates via Hydrothermal Method</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/search?q=M.%20Yildirim">M. Yildirim</a>, <a href="https://publications.waset.org/search?q=A.%20S.%20Kipcak"> A. S. Kipcak</a>, <a href="https://publications.waset.org/search?q=F.%20T.%20Senberber"> F. T. Senberber</a>, <a href="https://publications.waset.org/search?q=M.%20O.%20Asensio"> M. O. Asensio</a>, <a href="https://publications.waset.org/search?q=E.%20M.%20Derun"> E. M. Derun</a>, <a href="https://publications.waset.org/search?q=S.%20Piskin"> S. Piskin</a> </p> <p class="card-text"><strong>Abstract:</strong></p> Potassium borates, which are widely used in welding and metal refining industry, as a lubricating oil additive, cement additive, fiberglass additive and insulation compound, are one of the important groups of borate minerals. In this study the production of a potassium borate mineral via hydrothermal method is aimed. The potassium source of potassium nitrate (KNO3) was used along with a sodium source of sodium hydroxide (NaOH) and boron source of boric acid (H3BO3). The constant parameters of reaction temperature and reaction time were determined as 80掳C and 1 h, respectively. The molar ratios of 1:1:3 (as KNO3:NaOH:H3BO3), 1:1:4, 1:1:5, 1:1:6 and 1:1:7 were used. Following the synthesis the identifications of the produced products were conducted by X-Ray Diffraction (XRD), Fourier Transform Infrared Spectroscopy (FT-IR) and Raman Spectroscopy. The results of the experiments and analysis showed in the ratio of 1:1:6, the Santite mineral with powder diffraction file number (pdf no.) of 01-072-1688, which is known as potassium pentaborate (KB5O8路4H2O) was synthesized as best. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/search?q=Hydrothermal%20synthesis" title="Hydrothermal synthesis">Hydrothermal synthesis</a>, <a href="https://publications.waset.org/search?q=potassium%20borate" title=" potassium borate"> potassium borate</a>, <a href="https://publications.waset.org/search?q=potassium%20nitrate" title=" potassium nitrate"> potassium nitrate</a>, <a href="https://publications.waset.org/search?q=santite." title=" santite."> santite.</a> </p> <a href="https://publications.waset.org/10001632/the-determination-of-the-potassium-nitrate-sodium-hydroxide-and-boric-acid-molar-ratio-in-the-synthesis-of-potassium-borates-via-hydrothermal-method" class="btn btn-primary btn-sm">Procedia</a> <a 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