赛默飞新一代液质联用系统TSQ Altis同时分析检测17种全氟化合物

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<div class="detailsModule"> <div class="main_title"> <h1>赛默飞新一代液质联用系统TSQ Altis同时分析检测17种全氟化合物</h1> <div class="information"> <div class="infor_time"> <span>2022-04-07</span>  </div>  </div> </div> <div class="in_detailsModule"> <div class="in_detailsModule_tilte"> <span>文献描述</span> <a href="/eco/api/solution/12505/download" target="_blank" class="download_btn"> <em>免费下载此文献</em> </a> </div> <div class="in_detailsModule_con"> <ul class="list-eighteen"> <li><label>应用领域</label><span>土壤</span></li> <li><label>样品</label><span>17种全氟化合物</span></li> <li><label>项目</label><span>同时分析检测方法</span></li> </ul> </div> </div> <div class="in_detailsModule"> <div class="in_detailsModule_tilte"> <span>相关产品清单</span> </div> <div class="in_detailsModule_con"> <div class="list-nineteen"> <div class="in-list-nineteen"> <div class="img_box"> <div class="in_img_box"> <a href="/ibook1263/p/485271-p.html" target="_blank"> <img src="https://img.antpedia.com/instrument-library/attachments/product/1263/1681180581-7851.jpg!w256x192.jpg" alt="赛默飞TSQ Altis™ Plus 三重四极杆质谱仪"> </a> </div> </div> <div class="txt_box"> <div class="title_name"> <a href="/ibook1263/p/485271-p.html" target="_blank">赛默飞TSQ Altis™ Plus 三重四极杆质谱仪 </a> </div> <div class="parameter"> <div class="in_parameter"> <label>品牌</label><span>赛默飞</span> </div> <div class="in_parameter"> <label>产地</label><span>美国</span> </div> <div class="in_parameter"> <label>型号</label><span>TSQ Altis™ Plus </span> </div> </div> <div class="price"> <span>面议</span> </div> <a href="//www.antpedia.com/?action-inquiry-type-2-pid-485271" target="_blank" class="consultBtn">咨询</a> </div> </div> </div> </div> </div> <div class="in_detailsModule"> <div class="in_detailsModule_tilte"><span>摘要</span> </div> <div class="in_detailsModule_con detailsModule_txt"> <p>本文基于赛默飞新一代三重四极杆液质联用平台TSQ Altis建立了 17种全氟化合物的同时分析检测方法。优化后的色谱条件：接 C18 Trap柱，分析柱为Thermo Scientic Accucore RPMS (100 ×  2.1 mm, 2.6 μm)，甲醇-水（水相含10mM乙酸铵）为流动相，流速0.3 mL/min，柱温35℃。采用H-ESI源，扫描方式为选择反应检测（SRM）。结果表明：环境水样直接进样10uL，17种全氟化合物检出限均能较好满足环境法规限值的要求，各化合物线性关系良好，线性相关系数均＞0.99。在20 pg/mL浓度水平下连续进样6 针，RSD均小于5.1%。采用该方法对生活饮用水、地下水等环境水体样品进行分析，灵敏度和重现性结果良好。 1. 引言全氟化合物（PFCs）是一类具有特殊化学性质的人造化合物，其以表面活性、热稳定性、耐酸性以及疏水疏油性而广泛应用于生产与生活中，如纺织品涂层、染色剂、泡沫灭火器、皮革等行业。PFCs 具有键能很强的C-F键，其极大的稳定性导致该类化合物难以在环境介质中化学降解及生物降解，并且可在生物体内放大、富集。研究表明，全氟类化合物在生物体内的蓄积水平高于已知的有机氯农药和二恶英等持久性有机污染物的数百倍至数千倍。全氟类化合物还具有生殖毒性、诱变毒性、发育毒性、神经毒性、免疫毒性等多种毒性，是一类具有全身多脏器毒性的环境污染物。因此在2009年，全氟辛烷磺酰氟、全氟辛烷磺酸及其盐类、全氟辛酸及其盐类作为新型持久性有机污染物（POPs）被添加到《斯德哥尔摩公约》的附件B中。此后，中国、欧盟及世界各国都对相关 </p><p>产品中的PFCs提出了限制要求，并陆续发布了相应的检测标准。这些标准涉及的检测方法有LCMS、GCMS以及LCMSMS等。其中，EPA 537针对生活饮用水中的PFCs更是规定了方法检出限低至 0.53 ng/L - 6.5 ng/L（取样量250mL，经SPE净化浓缩，LCMSMS 检测，进样体积10μL）。本文建立了超高效液相色谱串联三重四极杆质谱TSQ Altis分析17种全氟化合物的直接进样方法，该法选择性高，分析速度快，灵敏度完全满足法规要求，同时具有良好的重现性和线性范围。实际环境基质样品分析结果满意，可用于环境水体中痕量PFCs的快速、准确定量分析。</p> </div> </div> <div class="in_detailsModule"> <div class="in_detailsModule_tilte"> <span>下载此应用文献</span> </div> <div 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赛默飞新一代液质联用系统TSQ Altis同时分析检测17种全氟化合物 — 应用