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material detonation reaction</title> <meta name="description" content="Search results for: energetic material detonation reaction"> <meta name="keywords" content="energetic material detonation reaction"> <meta name="viewport" content="width=device-width, initial-scale=1, minimum-scale=1, maximum-scale=1, user-scalable=no"> <meta charset="utf-8"> <link href="https://cdn.waset.org/favicon.ico" type="image/x-icon" rel="shortcut icon"> <link href="https://cdn.waset.org/static/plugins/bootstrap-4.2.1/css/bootstrap.min.css" rel="stylesheet"> <link href="https://cdn.waset.org/static/plugins/fontawesome/css/all.min.css" rel="stylesheet"> <link href="https://cdn.waset.org/static/css/site.css?v=150220211555" rel="stylesheet"> </head> <body> <header> <div class="container"> <nav class="navbar navbar-expand-lg navbar-light"> <a class="navbar-brand" href="https://waset.org"> <img src="https://cdn.waset.org/static/images/wasetc.png" alt="Open Science Research Excellence" title="Open Science Research 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method="get" action="https://publications.waset.org/abstracts/search"> <div id="custom-search-input"> <div class="input-group"> <i class="fas fa-search"></i> <input type="text" class="search-query" name="q" placeholder="Author, Title, Abstract, Keywords" value="energetic material detonation reaction"> <input type="submit" class="btn_search" value="Search"> </div> </div> </form> </div> </div> <div class="row mt-3"> <div class="col-sm-3"> <div class="card"> <div class="card-body"><strong>Commenced</strong> in January 2007</div> </div> </div> <div class="col-sm-3"> <div class="card"> <div class="card-body"><strong>Frequency:</strong> Monthly</div> </div> </div> <div class="col-sm-3"> <div class="card"> <div class="card-body"><strong>Edition:</strong> International</div> </div> </div> <div class="col-sm-3"> <div class="card"> <div class="card-body"><strong>Paper Count:</strong> 8928</div> </div> </div> </div> <h1 class="mt-3 mb-3 text-center" style="font-size:1.6rem;">Search results for: energetic material detonation reaction</h1> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8718</span> Alcoxysilanes Production from Silica and Dimethylcarbonate Promoted by Alkali Bases: A DFT Investigation of the Reaction Mechanism</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Valeria%20%20Butera">Valeria Butera</a>, <a href="https://publications.waset.org/abstracts/search?q=Norihisa%20Fukaya"> Norihisa Fukaya</a>, <a href="https://publications.waset.org/abstracts/search?q=Jun-Chu%20Choi"> Jun-Chu Choi</a>, <a href="https://publications.waset.org/abstracts/search?q=Kazuhiko%20Sato"> Kazuhiko Sato</a>, <a href="https://publications.waset.org/abstracts/search?q=Yoong-Kee%20Choe"> Yoong-Kee Choe</a> </p> <p class="card-text"><strong>Abstract:</strong></p> Several silicon dioxide sources can react with dimethyl carbonate (DMC) in presence of alkali bases catalysts to ultimately produce tetramethoxysilane (TMOS). Experimental findings suggested that the reaction proceeds through several steps in which the first molecule of DMC is converted to dimethylsilyloxide (DMOS) and CO₂. Following the same mechanistic steps, a second molecule of DMC reacts with the DMOS to afford the final product TMOS. Using a cluster model approach, a quantum-mechanical investigation of the first part of the reaction leading to DMOS formation is reported with a twofold purpose: (1) verify the viability of the reaction mechanism proposed on the basis of experimental evidences .(2) compare the behaviors of three different alkali hydroxides MOH, where M=Li, K and Cs, to determine whether diverse ionic radius and charge density can be considered responsible for the observed differences in reactivity. Our findings confirm the observed experimental trend and furnish important information about the effective role of the alkali hydroxides giving an explanation of the different catalytic activity of the three metal cations. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=Alcoxysilanes%20production" title="Alcoxysilanes production">Alcoxysilanes production</a>, <a href="https://publications.waset.org/abstracts/search?q=cluster%20model%20approach" title=" cluster model approach"> cluster model approach</a>, <a href="https://publications.waset.org/abstracts/search?q=DFT" title=" DFT"> DFT</a>, <a href="https://publications.waset.org/abstracts/search?q=DMC%20conversion" title=" DMC conversion"> DMC conversion</a> </p> <a href="https://publications.waset.org/abstracts/70173/alcoxysilanes-production-from-silica-and-dimethylcarbonate-promoted-by-alkali-bases-a-dft-investigation-of-the-reaction-mechanism" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/70173.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">274</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8717</span> Investigating Methanol Interaction on Hexagonal Ceria-BTC Microrods</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Jamshid%20Hussain">Jamshid Hussain</a>, <a href="https://publications.waset.org/abstracts/search?q=Kuen%20Song%20Lin"> Kuen Song Lin</a> </p> <p class="card-text"><strong>Abstract:</strong></p> For prospective applications, chemists and materials scientists are particularly interested in creating 3D-micro/nanocomposite structures with shapes and unique characteristics. Ceria has recently been produced with a variety of morphologies, including one-dimensional structures (nanoparticles, nanorods, nanowires, and nanotubes). It is anticipated that this material can be used in different fields, such as catalysis, methanol decomposition, carbon monoxide oxidation, optical materials, and environmental protection. Distinct three-dimensional hydrated ceria-BTC (CeO₂-1,3,5-Benzenetricarboxylic-acid) microstructures were successfully synthesized via a hydrothermal route in an aqueous solution. FE-SEM and XRD patterns reveal that a ceria-BTC framework diameter and length are approximately 1.45–2.4 and 5.5–6.5 µm, respectively, at 130 oC and with pH 2 for 72 h. It was demonstrated that the reaction conditions affected the 3D ceria-BTC architecture. The hexagonal ceria-BTC microrod comprises organic linkers, which are transformed into hierarchical ceria microrod in the presences of air at 400 oC was confirmed by Fourier transform infrared spectroscopy. The Ce-O bonding of the hierarchical ceria microrod (HCMs) species has a bond distance and coordination number of 2.44 and 6.89, respectively, which attenuates the EXAFS spectra. Compared to the ceria powder, the HCMs produced more oxygen vacancies and Ce3+ as shown by the XPS and XANES/EXAFS analyses. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=hierarchical%20ceria%20microrod" title="hierarchical ceria microrod">hierarchical ceria microrod</a>, <a href="https://publications.waset.org/abstracts/search?q=three-dimensional%20ceria" title=" three-dimensional ceria"> three-dimensional ceria</a>, <a href="https://publications.waset.org/abstracts/search?q=methanol%20decomposition" title=" methanol decomposition"> methanol decomposition</a>, <a href="https://publications.waset.org/abstracts/search?q=reaction%20mechanism" title=" reaction mechanism"> reaction mechanism</a>, <a href="https://publications.waset.org/abstracts/search?q=XANES%2FEXAFS" title=" XANES/EXAFS"> XANES/EXAFS</a> </p> <a href="https://publications.waset.org/abstracts/194227/investigating-methanol-interaction-on-hexagonal-ceria-btc-microrods" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/194227.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">8</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8716</span> Coupling of Microfluidic Droplet Systems with ESI-MS Detection for Reaction Optimization</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Julia%20R.%20Beulig">Julia R. Beulig</a>, <a href="https://publications.waset.org/abstracts/search?q=Stefan%20Ohla"> Stefan Ohla</a>, <a href="https://publications.waset.org/abstracts/search?q=Detlev%20Belder"> Detlev Belder</a> </p> <p class="card-text"><strong>Abstract:</strong></p> In contrast to off-line analytical methods, lab-on-a-chip technology delivers direct information about the observed reaction. Therefore, microfluidic devices make an important scientific contribution, e.g. in the field of synthetic chemistry. Herein, the rapid generation of analytical data can be applied for the optimization of chemical reactions. These microfluidic devices enable a fast change of reaction conditions as well as a resource saving method of operation. In the presented work, we focus on the investigation of multiphase regimes, more specifically on a biphasic microfluidic droplet systems. Here, every single droplet is a reaction container with customized conditions. The biggest challenge is the rapid qualitative and quantitative readout of information as most detection techniques for droplet systems are non-specific, time-consuming or too slow. An exception is the electrospray mass spectrometry (ESI-MS). The combination of a reaction screening platform with a rapid and specific detection method is an important step in droplet-based microfluidics. In this work, we present a novel approach for synthesis optimization on the nanoliter scale with direct ESI-MS detection. The development of a droplet-based microfluidic device, which enables the modification of different parameters while simultaneously monitoring the effect on the reaction within a single run, is shown. By common soft- and photolithographic techniques a polydimethylsiloxane (PDMS) microfluidic chip with different functionalities is developed. As an interface for the MS detection, we use a steel capillary for ESI and improve the spray stability with a Teflon siphon tubing, which is inserted underneath the steel capillary. By optimizing the flow rates, it is possible to screen parameters of various reactions, this is exemplarity shown by a Domino Knoevenagel Hetero-Diels-Alder reaction. Different starting materials, catalyst concentrations and solvent compositions are investigated. Due to the high repetition rate of the droplet production, each set of reaction condition is examined hundreds of times. As a result, of the investigation, we receive possible reagents, the ideal water-methanol ratio of the solvent and the most effective catalyst concentration. The developed system can help to determine important information about the optimal parameters of a reaction within a short time. With this novel tool, we make an important step on the field of combining droplet-based microfluidics with organic reaction screening. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=droplet" title="droplet">droplet</a>, <a href="https://publications.waset.org/abstracts/search?q=mass%20spectrometry" title=" mass spectrometry"> mass spectrometry</a>, <a href="https://publications.waset.org/abstracts/search?q=microfluidics" title=" microfluidics"> microfluidics</a>, <a href="https://publications.waset.org/abstracts/search?q=organic%20reaction" title=" organic reaction"> organic reaction</a>, <a href="https://publications.waset.org/abstracts/search?q=screening" title=" screening"> screening</a> </p> <a href="https://publications.waset.org/abstracts/46791/coupling-of-microfluidic-droplet-systems-with-esi-ms-detection-for-reaction-optimization" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/46791.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">301</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8715</span> A Study on Kinetic of Nitrous Oxide Catalytic Decomposition over CuO/HZSM-5</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Y.%20J.%20Song">Y. J. Song</a>, <a href="https://publications.waset.org/abstracts/search?q=Q.%20S.%20Xu"> Q. S. Xu</a>, <a href="https://publications.waset.org/abstracts/search?q=X.%20C.%20Wang"> X. C. Wang</a>, <a href="https://publications.waset.org/abstracts/search?q=H.%20Wang"> H. Wang</a>, <a href="https://publications.waset.org/abstracts/search?q=C.%20Q.%20Li"> C. Q. Li</a> </p> <p class="card-text"><strong>Abstract:</strong></p> The catalyst of copper oxide loaded on HZSM-5 was developed for nitrous oxide (N₂O) direct decomposition. The kinetic of nitrous oxide decomposition was studied for CuO/HZSM-5 catalyst prepared by incipient wetness impregnation method. The external and internal diffusion of catalytic reaction were considered in the investigation. Experiment results indicated that the external diffusion was basically eliminated when the reaction gas mixture gas hourly space velocity (GHSV) was higher than 9000h⁻¹ and the influence of the internal diffusion was negligible when the particle size of the catalyst CuO/HZSM-5 was small than 40-60 mesh. The experiment results showed that the kinetic of catalytic decomposition of N₂O was a first-order reaction and the activation energy and the pre-factor of the kinetic equation were 115.15kJ/mol and of 1.6×109, respectively. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=catalytic%20decomposition" title="catalytic decomposition">catalytic decomposition</a>, <a href="https://publications.waset.org/abstracts/search?q=CuO%2FHZSM-5" title=" CuO/HZSM-5"> CuO/HZSM-5</a>, <a href="https://publications.waset.org/abstracts/search?q=kinetic" title=" kinetic"> kinetic</a>, <a href="https://publications.waset.org/abstracts/search?q=nitrous%20oxide" title=" nitrous oxide"> nitrous oxide</a> </p> <a href="https://publications.waset.org/abstracts/130896/a-study-on-kinetic-of-nitrous-oxide-catalytic-decomposition-over-cuohzsm-5" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/130896.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">185</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8714</span> Efficient Ni(II)-Containing Layered Triple Hydroxide-Based Catalysts: Synthesis, Characterisation and Their Role in the Heck Reaction</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Gabor%20Varga">Gabor Varga</a>, <a href="https://publications.waset.org/abstracts/search?q=Krisztina%20Karadi"> Krisztina Karadi</a>, <a href="https://publications.waset.org/abstracts/search?q=Zoltan%20Konya"> Zoltan Konya</a>, <a href="https://publications.waset.org/abstracts/search?q=Akos%20Kukovecz"> Akos Kukovecz</a>, <a href="https://publications.waset.org/abstracts/search?q=Pal%20Sipos"> Pal Sipos</a>, <a href="https://publications.waset.org/abstracts/search?q=Istvan%20Palinko"> Istvan Palinko</a> </p> <p class="card-text"><strong>Abstract:</strong></p> Nickel can efficiently replace palladium in the Heck, Suzuki and Negishi reactions. This study focuses on the synthesis and catalytic application of Ni(II)-containing layered double hydroxides (LDHs) and layered triple hydroxides (LTHs). Our goals were to incorporate Ni(II) ions among the layers of LDHs or LTHs, or binding it to their surface or building it into their layers in such a way that their catalytic activities are maintained or even increased. The LDHs and LTHs were prepared by the co-precipitation method using ethylene glycol as co-solvent. In several cases, post-synthetic modifications (e.g., thermal treatment) were performed. After optimizing the synthesis conditions, the composites displayed good crystallinity and were free of byproducts. The success of the syntheses and the post-synthetic modifications was confirmed by relevant characterization methods (XRD, SEM, SEM-EDX and combined IR techniques). Catalytic activities of the produced and well-characterized solids were investigated through the Heck reaction. The composites behaved as efficient, recyclable catalysts in the Heck reaction between 4-bromoanisole and styrene. Through varying the reaction parameters, we were able to obtain acceptable conversions under mild conditions. Our study highlights the possibility of the application of Ni(II)-containing composites as efficient catalysts in coupling reactions. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=layered%20double%20hydroxide" title="layered double hydroxide">layered double hydroxide</a>, <a href="https://publications.waset.org/abstracts/search?q=layered%20triple%20hydroxide" title=" layered triple hydroxide"> layered triple hydroxide</a>, <a href="https://publications.waset.org/abstracts/search?q=heterogeneous%20catalysis" title=" heterogeneous catalysis"> heterogeneous catalysis</a>, <a href="https://publications.waset.org/abstracts/search?q=heck%20reaction" title=" heck reaction"> heck reaction</a> </p> <a href="https://publications.waset.org/abstracts/95373/efficient-niii-containing-layered-triple-hydroxide-based-catalysts-synthesis-characterisation-and-their-role-in-the-heck-reaction" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/95373.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">174</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8713</span> Mesoporous RGO@(Co,Mn)3O4 Nanocomposite Prepared by Microwave Method and Its Electrochemical Performance</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Charmaine%20Lamiel">Charmaine Lamiel</a>, <a href="https://publications.waset.org/abstracts/search?q=Van%20Hoa%20Nguyen"> Van Hoa Nguyen</a>, <a href="https://publications.waset.org/abstracts/search?q=Jae-Jin%20Shim"> Jae-Jin Shim</a> </p> <p class="card-text"><strong>Abstract:</strong></p> Supercapacitors are energy storage devices capable of storing more energy than conventional capacitors and have higher power density than batteries. The advantages of this method include the non-use of reducing agents and acidic medium, and no further use of a post-heat treatment unlike the conventional processes, in which calcination is generally employed after obtaining the initial product. Furthermore, it also offers a shorter reaction time at low temperatures and low power requirements, which allows low fabrication and energy cost. In this study, microwave irradiation was used for the facile and rapid synthesis of mesoporous RGO@(Co,Mn)3O4 nanosheets as an electrode material. The as-prepared electrode exhibited a high capacitance of 953 F•g^−1 at 1 A•g^−1 in a 6 M KOH electrolyte solution. Moreover, the electrode exhibited a high energy density of 76.2 Wh•kg^−1 at a power density of 720 W•kg^−1, and a high power density of 7200 W•kg^−1 at an energy density of 38 Wh•kg^−1. The successful methodology was considered to be efficient and cost-effective, thereby providing an active electrode material with very promising electrochemical performance. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=cobalt-manganese%20oxide" title="cobalt-manganese oxide">cobalt-manganese oxide</a>, <a href="https://publications.waset.org/abstracts/search?q=electrochemical" title=" electrochemical"> electrochemical</a>, <a href="https://publications.waset.org/abstracts/search?q=graphene" title=" graphene"> graphene</a>, <a href="https://publications.waset.org/abstracts/search?q=microwave%20synthesis" title=" microwave synthesis"> microwave synthesis</a>, <a href="https://publications.waset.org/abstracts/search?q=supercapacitor" title=" supercapacitor"> supercapacitor</a> </p> <a href="https://publications.waset.org/abstracts/42664/mesoporous-rgo-at-comn3o4-nanocomposite-prepared-by-microwave-method-and-its-electrochemical-performance" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/42664.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">213</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8712</span> Radiative Reactions Analysis at the Range of Astrophysical Energies </h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=A.%20Amar">A. Amar</a> </p> <p class="card-text"><strong>Abstract:</strong></p> Analysis of the elastic scattering of protons on <sup>10</sup>B nuclei has been done in the framework of the optical model and single folding model at the beam energies up to 17 MeV. We could enhance the optical potential parameters using Esis88 Code, as well as SPI GENOA Code. Linear relationship between volume real potential (V<sub>0</sub>) and proton energy (E<sub>p</sub>) has been obtained. Also, surface imaginary potential W<sub>D</sub> is proportional to the proton energy (E<sub>p</sub>) in the range 0.400 and 17 MeV. The radiative reaction <sup>10</sup>B(p,γ)<sup>11</sup>C has been analyzed using potential model. A comparison between <sup>10</sup>B(p,γ)<sup>11</sup>C and <sup>6</sup>Li(p,γ)<sup>7</sup>Be has been made. Good agreement has been found between theoretical and experimental results in the whole range of energy. The radiative resonance reaction <sup>7</sup>Li(p,γ)<sup>8</sup>Be has been studied. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=elastic%20scattering%20of%20protons%20on%2010B%20nuclei" title="elastic scattering of protons on 10B nuclei">elastic scattering of protons on 10B nuclei</a>, <a href="https://publications.waset.org/abstracts/search?q=optical%20potential%20parameters" title=" optical potential parameters"> optical potential parameters</a>, <a href="https://publications.waset.org/abstracts/search?q=potential%20model" title=" potential model"> potential model</a>, <a href="https://publications.waset.org/abstracts/search?q=radiative%20reaction" title=" radiative reaction"> radiative reaction</a> </p> <a href="https://publications.waset.org/abstracts/88571/radiative-reactions-analysis-at-the-range-of-astrophysical-energies" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/88571.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">210</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8711</span> The Optimization of Copper Sulfate and Tincalconite Molar Ratios on the Hydrothermal Synthesis of Copper Borates</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=E.%20Moroydor%20Derun">E. Moroydor Derun</a>, <a href="https://publications.waset.org/abstracts/search?q=N.%20Tugrul"> N. Tugrul</a>, <a href="https://publications.waset.org/abstracts/search?q=F.%20T.%20Senberber"> F. T. Senberber</a>, <a href="https://publications.waset.org/abstracts/search?q=A.%20S.%20Kipcak"> A. S. Kipcak</a>, <a href="https://publications.waset.org/abstracts/search?q=S.%20Piskin"> S. Piskin</a> </p> <p class="card-text"><strong>Abstract:</strong></p> In this research, copper borates are synthesized by the reaction of copper sulfate pentahydrate (CuSO4.5H2O) and tincalconite (Na2O4B7.10H2O). The experimental parameters are selected as 80°C reaction temperature and 60 of reaction time. The effect of mole ratio of CuSO4.5H2O to Na2O4B7.5H2O is studied. For the identification analyses X-Ray Diffraction (XRD) and Fourier Transform Infrared Spectroscopy (FT-IR) techniques are used. At the end of the experiments, synthesized copper borate is matched with the powder diffraction file of “00-001-0472” [Cu(BO2)2] and characteristic vibrations between B and O atoms are seen. The proper crystals are obtained at the mole ratio of 3:1. This study showed that simplified synthesis process is suitable for the production of copper borate minerals. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=hydrothermal%20synthesis" title="hydrothermal synthesis">hydrothermal synthesis</a>, <a href="https://publications.waset.org/abstracts/search?q=copper%20borates" title=" copper borates"> copper borates</a>, <a href="https://publications.waset.org/abstracts/search?q=copper%20sulfate" title=" copper sulfate"> copper sulfate</a>, <a href="https://publications.waset.org/abstracts/search?q=tincalconite" title=" tincalconite"> tincalconite</a> </p> <a href="https://publications.waset.org/abstracts/16418/the-optimization-of-copper-sulfate-and-tincalconite-molar-ratios-on-the-hydrothermal-synthesis-of-copper-borates" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/16418.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">381</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8710</span> ADCOR © Muscle Damage Rapid Detection Test Based on Skeletal Troponin I Immunochromatography Reaction</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Muhammad%20Solikhudin%20Nafi">Muhammad Solikhudin Nafi</a>, <a href="https://publications.waset.org/abstracts/search?q=Wahyu%20Afif%20Mufida"> Wahyu Afif Mufida</a>, <a href="https://publications.waset.org/abstracts/search?q=Mita%20Erna%20Wati"> Mita Erna Wati</a>, <a href="https://publications.waset.org/abstracts/search?q=Fitri%20Setyani%20Rokim"> Fitri Setyani Rokim</a>, <a href="https://publications.waset.org/abstracts/search?q=M.%20Al-Rizqi%20Dharma%20Fauzi"> M. Al-Rizqi Dharma Fauzi</a> </p> <p class="card-text"><strong>Abstract:</strong></p> High dose activity without any pre-exercise will impact Delayed Onset Muscle Soreness (DOMS). DOMS known as delayed pain post-exercise and induce skeletal injury which will decrease athletes’ performances. From now on, post-exercise muscle damage can be detected by measuring skeletal troponin I (sTnI) concentration in serum using ELISA but this method needs more time and cost. To prevent decreased athletes performances, screening need to be done rapidly. We want to introduce our new prototype to detect DOMS acutely. Rapid detection tests are based on immunological reaction between skeletal troponin I antibodies and sTnI in human serum or whole blood. Chemical methods that are used in the manufacture of diagnostic test is lateral flow immunoassay. The material used is rat monoclonal antibody sTnI, colloidal gold, anti-mouse IgG, nitrocellulose membrane, conjugate pad, sample pad, wick and backing card. The procedure are made conjugate (colloidal gold and mAb sTnI) and insert into the conjugate pad, gives spray sTnI mAb and anti-mouse IgG into nitrocellulose membrane, and assemble RDT. RDT had been evaluated by measuring the sensitivity of positive human serum (n = 30) and negative human serum (n = 30). Overall sensitivity value was 93% and specificity value was 90%. ADCOR as the first rapid detection test qualitatively showed antigen-antibody reaction and showed good overall performances for screening of muscle damage. Furthermore, these finding still need more improvements to get best results. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=DOMS" title="DOMS">DOMS</a>, <a href="https://publications.waset.org/abstracts/search?q=sTnI" title=" sTnI"> sTnI</a>, <a href="https://publications.waset.org/abstracts/search?q=rapid%20detection%20test" title=" rapid detection test"> rapid detection test</a>, <a href="https://publications.waset.org/abstracts/search?q=ELISA" title=" ELISA "> ELISA </a> </p> <a href="https://publications.waset.org/abstracts/34547/adcor-muscle-damage-rapid-detection-test-based-on-skeletal-troponin-i-immunochromatography-reaction" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/34547.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">513</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8709</span> Can We Meet the New Challenges of NonIsocyanates Polyurethanes (NIPU) towards NIPU Foams?</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Adrien%20Cornille">Adrien Cornille</a>, <a href="https://publications.waset.org/abstracts/search?q=Marine%20Blain"> Marine Blain</a>, <a href="https://publications.waset.org/abstracts/search?q=Bernard%20Boutevin"> Bernard Boutevin</a>, <a href="https://publications.waset.org/abstracts/search?q=Sylvain%20Caillol"> Sylvain Caillol</a> </p> <p class="card-text"><strong>Abstract:</strong></p> Generally, linear polyurethanes (PUs) are obtained by the reaction between an oligomeric diol, a short diol as chain extender and a diisocyanate. However the use of diisocyanate should be avoided since they are generally very harmful for human health. Therefore the synthesis of NIPUs (non isocyanate PUs) from step growth polymerization of dicyclocarbonates and diamines should be favoured. This method is particularly interesting since no hazardous isocyanates are used. Thus, this reaction, extensively studied by Endo et al. is currently gaining a lot of attention as a substitution route for the synthesis of NIPUs, both from industrial and academic community. However, the reactivity of reaction between amine and cyclic carbonate is a major scientific issue, since cyclic carbonates are poorly reactive. Thus, our team developed several synthetic ways for the synthesis of various di-cyclic carbonates based on C5-, C6- and dithio- cyclic carbonates, from different biobased raw materials (glycerin isosorbide, vegetable oils…). These monomers were used to synthesize NIPUs with various mechanical and thermal properties for various applications. We studied the reactivity of reaction with various catalysts and find optimized conditions for room temperature reaction. We also studied the radical copolymerization of cyclic carbonate monomers in styrene-acrylate copolymers for coating applications. We also succeeded in the elaboration of biobased NIPU flexible foams. To the best of our knowledge, there is no report in literature on the preparation of non-isocyanate polyurethane foams. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=foam" title="foam">foam</a>, <a href="https://publications.waset.org/abstracts/search?q=nonisocyanate%20polyurethane" title=" nonisocyanate polyurethane"> nonisocyanate polyurethane</a>, <a href="https://publications.waset.org/abstracts/search?q=cyclic%20carbonate" title=" cyclic carbonate"> cyclic carbonate</a>, <a href="https://publications.waset.org/abstracts/search?q=blowing%20agent" title=" blowing agent"> blowing agent</a>, <a href="https://publications.waset.org/abstracts/search?q=scanning%20electron%20microscopy" title=" scanning electron microscopy"> scanning electron microscopy</a> </p> <a href="https://publications.waset.org/abstracts/40035/can-we-meet-the-new-challenges-of-nonisocyanates-polyurethanes-nipu-towards-nipu-foams" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/40035.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">232</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8708</span> Comparative Study for Biodiesel Production Using a Batch and a Semi-Continuous Flow Reactor</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=S.%20S.%20L.%20Andrade">S. S. L. Andrade</a>, <a href="https://publications.waset.org/abstracts/search?q=E.%20A.%20Souza"> E. A. Souza</a>, <a href="https://publications.waset.org/abstracts/search?q=L.%20C.%20L.%20Santos"> L. C. L. Santos</a>, <a href="https://publications.waset.org/abstracts/search?q=C.%20Moraes"> C. Moraes</a>, <a href="https://publications.waset.org/abstracts/search?q=A.%20K.%20C.%20L.%20Lobato"> A. K. C. L. Lobato</a> </p> <p class="card-text"><strong>Abstract:</strong></p> Biodiesel may be produced through transesterification reaction (or alcoholysis), that is the transformation of a long chain fatty acid in an alkyl ester. This reaction can occur in the presence of acid catalysts, alkali, or enzyme. Currently, for industrial processes, biodiesel is produced by alkaline route. The alkali most commonly used in these processes is hydroxides and methoxides of sodium and potassium. In this work, biodiesel production was conducted in two different systems. The first consisted of a batch reactor operating with a traditional washing system and the second consisted of a semi-continuous flow reactor operating with a membrane separation system. Potassium hydroxides was used as catalyst at a concentration of 1% by weight, the molar ratio oil/alcohol was 1/9 and temperature of 55 °C. Tests were performed using soybeans and palm oil and the ester conversion results were compared for both systems. It can be seen that the results for both oils are similar when using the batch reator or the semi-continuous flow reactor. The use of the semi-continuous flow reactor allows the removal of the formed products. Thus, in the case of a reversible reaction, with the removal of reaction products, the concentration of the reagents becomes higher and the equilibrium reaction is shifted towards the formation of more products. The higher conversion to ester with soybean and palm oil using the batch reactor was approximately 98%. In contrast, it was observed a conversion of 99% when using the same operating condition on a semi-continuous flow reactor. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=biodiesel" title="biodiesel">biodiesel</a>, <a href="https://publications.waset.org/abstracts/search?q=batch%20reactor" title=" batch reactor"> batch reactor</a>, <a href="https://publications.waset.org/abstracts/search?q=semi-continuous%20flow%20reactor" title=" semi-continuous flow reactor"> semi-continuous flow reactor</a>, <a href="https://publications.waset.org/abstracts/search?q=transesterification" title=" transesterification"> transesterification</a> </p> <a href="https://publications.waset.org/abstracts/39572/comparative-study-for-biodiesel-production-using-a-batch-and-a-semi-continuous-flow-reactor" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/39572.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">384</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8707</span> Graphene-reinforced Metal-organic Framework Derived Cobalt Sulfide/Carbon Nanocomposites as Efficient Multifunctional Electrocatalysts</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Yongde%20Xia">Yongde Xia</a>, <a href="https://publications.waset.org/abstracts/search?q=Laicong%20Deng"> Laicong Deng</a>, <a href="https://publications.waset.org/abstracts/search?q=Zhuxian%20Yang"> Zhuxian Yang</a> </p> <p class="card-text"><strong>Abstract:</strong></p> Developing cost-effective electrocatalysts for oxygen reduction reaction (ORR), oxygen evolution reaction (OER) and hydrogen evolution reaction (HER) is vital in energy conversion and storage applications. Herein, we report a simple method for the synthesis of graphene-reinforced cobalt sulfide/carbon nanocomposites and the evaluation of their electrocatalytic performance for typical electrocatalytic reactions. Nanocomposites of cobalt sulfide embedded in N, S co-doped porous carbon and graphene (CoS@C/Graphene) were generated via simultaneous sulfurization and carbonization of one-pot synthesized graphite oxide-ZIF-67 precursors. The obtained CoS@C/Graphene nanocomposite was characterized by X-ray diffraction, Raman spectroscopy, Thermogravimetric analysis-Mass spectroscopy, Scanning electronic microscopy, Transmission electronic microscopy, X-ray photoelectron spectroscopy and gas sorption. It was found that cobalt sulfide nanoparticles were homogenously dispersed in the in-situ formed N, S co-doped porous carbon/Graphene matrix. The CoS@C/10Graphene composite not only shows excellent electrocatalytic activity toward ORR with high onset potential of 0.89 V, four-electron pathway and superior durability of maintaining 98% current after continuously running for around 5 hours, but also exhibits good performance for OER and HER, due to the improved electrical conductivity, increased catalytic active sites and connectivity between the electrocatalytic active cobalt sulfide and the carbon matrix. This work offers a new approach for the development of novel multifunctional nanocomposites for the next generation of energy conversion and storage applications. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=MOF%20derivative" title="MOF derivative">MOF derivative</a>, <a href="https://publications.waset.org/abstracts/search?q=graphene" title=" graphene"> graphene</a>, <a href="https://publications.waset.org/abstracts/search?q=electrocatalyst" title=" electrocatalyst"> electrocatalyst</a>, <a href="https://publications.waset.org/abstracts/search?q=oxygen%20reduction%20reaction" title=" oxygen reduction reaction"> oxygen reduction reaction</a>, <a href="https://publications.waset.org/abstracts/search?q=oxygen%20evolution%20reaction" title=" oxygen evolution reaction"> oxygen evolution reaction</a>, <a href="https://publications.waset.org/abstracts/search?q=hydrogen%20evolution%20reaction" title=" hydrogen evolution reaction"> hydrogen evolution reaction</a> </p> <a href="https://publications.waset.org/abstracts/182174/graphene-reinforced-metal-organic-framework-derived-cobalt-sulfidecarbon-nanocomposites-as-efficient-multifunctional-electrocatalysts" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/182174.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">50</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8706</span> Angiogenic Potential of Collagen Based Biomaterials Implanted on Chick Embryo Chorioallantoic Membrane as Alternative Microenvironment for in Vitro and in Vivo Angiogenesis Assays</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Anca%20Maria%20Cimpean">Anca Maria Cimpean</a>, <a href="https://publications.waset.org/abstracts/search?q=Serban%20Comsa"> Serban Comsa</a> </p> <p class="card-text"><strong>Abstract:</strong></p> Chick embryo chorioallantoic membrane (CAM) is a well vascularised in vivo experimental model used as a platform for testing the behavior of different implants inserted on it from tumor fragments to therapeutic agents or various biomaterials. Five types of collagen-based biomaterials with 2D and 3D structure (MotifMesh, Optimaix2D, Optimaix3D, Dual Layer Collagen and Xenoderm) were implanted on CAM and continuously evaluated by stereomicroscope for up to 5 days post-implant with an emphasis of their ability to requisite and develop new blood vessels (BVs) followed by microscopic analysis. MotifMEsh did not induce any angiogenic response lacking to be invaded by BVs from the CAM, but it induced intense inflammatory response necrosis and fibroblastic reaction around the implant. Optimaix2D has good adherence. CAM with minimal or no inflammatory reaction, a good integration of the CAM between the collagen mesh’s fibers, consistent adhesion of the cells to the collagen fibers,and a good ability to form pseudo-vascular channels filled with cells. Optimaix3D induced the highest angiogenic effects on CAM. The material shows good integration on CAM. The collagen fibers of the material show the ability to organize themselves into linear and tubular structures. It is possible to see blood elements, especially at the periphery of the implant. Dual-layer collagen behaves similar to Optimaix 3D, while Xenoderm induced a moderate angiogenic effect on CAM. Based on these data, we may conclude that collagen-based materials have variable ability to requisite and develop new blood vessels. A proper selection of collagen-based biomaterial scaffolds may crucially influence the acquisition and development of blood vessels during angiogenesis assays. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=chick%20embryo%20chorioallantoic%20membrane" title="chick embryo chorioallantoic membrane">chick embryo chorioallantoic membrane</a>, <a href="https://publications.waset.org/abstracts/search?q=collagen%20scaffolds" title=" collagen scaffolds"> collagen scaffolds</a>, <a href="https://publications.waset.org/abstracts/search?q=blood%20vessels" title=" blood vessels"> blood vessels</a>, <a href="https://publications.waset.org/abstracts/search?q=vascular%20microenvironment" title=" vascular microenvironment"> vascular microenvironment</a> </p> <a href="https://publications.waset.org/abstracts/143642/angiogenic-potential-of-collagen-based-biomaterials-implanted-on-chick-embryo-chorioallantoic-membrane-as-alternative-microenvironment-for-in-vitro-and-in-vivo-angiogenesis-assays" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/143642.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">193</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8705</span> Development of Standard Evaluation Technique for Car Carpet Floor</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=In-Sung%20Lee">In-Sung Lee</a>, <a href="https://publications.waset.org/abstracts/search?q=Un-Hwan%20Park"> Un-Hwan Park</a>, <a href="https://publications.waset.org/abstracts/search?q=Jun-Hyeok%20Heo"> Jun-Hyeok Heo</a>, <a href="https://publications.waset.org/abstracts/search?q=Tae-Hyeon%20Oh"> Tae-Hyeon Oh</a>, <a href="https://publications.waset.org/abstracts/search?q=Dae-Gyu%20Park"> Dae-Gyu Park</a> </p> <p class="card-text"><strong>Abstract:</strong></p> Statistical Energy Analysis is to be the most effective CAE Method for air-born noise analysis in the Automotive area. This study deals with a method to predict the noise level inside of the car under the steady-state condition using the SEA model of car for air-born noise analysis. We can identify weakened part due to the acoustic material properties using it. Therefore, it is useful for the material structural design. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=air-born%20noise" title="air-born noise">air-born noise</a>, <a href="https://publications.waset.org/abstracts/search?q=material%20structural%20design" title=" material structural design"> material structural design</a>, <a href="https://publications.waset.org/abstracts/search?q=acoustic%20material%20properties" title=" acoustic material properties"> acoustic material properties</a>, <a href="https://publications.waset.org/abstracts/search?q=absorbing" title=" absorbing"> absorbing</a> </p> <a href="https://publications.waset.org/abstracts/51024/development-of-standard-evaluation-technique-for-car-carpet-floor" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/51024.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">423</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8704</span> Toughness of a Silt-Based Construction Material Reinforced with Fibers</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Y.%20Shamas">Y. Shamas</a>, <a href="https://publications.waset.org/abstracts/search?q=S.%20Imanzadeh"> S. Imanzadeh</a>, <a href="https://publications.waset.org/abstracts/search?q=A.%20Jarno"> A. Jarno</a>, <a href="https://publications.waset.org/abstracts/search?q=S.%20Taibi"> S. Taibi</a> </p> <p class="card-text"><strong>Abstract:</strong></p> Silt-based construction material is acknowledged since forever and lately received the researchers’ attention more than before as being an ecological and economical alternative for typical cement-based concrete. Silt-based material is known for its worldwide availability, cheapness, and various applications. Some rules should be defined to obtain a standardized method for the use of raw earth as a modern construction material; but first, its mechanical properties should be precisely studied to better understand its behavior in order to find new aspects in making it a better competitor for the cement concrete that is high energy-demanding in terms of gray energy. Some researches were performed on the raw earth material to enhance its characteristics as strength and ductility for their importance and their wide use for various materials. Yet, many other mechanical properties can be used to study the mechanical behavior of raw earth materials such as Young’smodulus and toughness. Studies concerning the toughness of material were rarely conducted previously except for metals despite its significant role associated to the energy absorbed by the material under loading before fracturing. The purpose of this paper is to restate different toughness definitions used in the literature and propose a new definition. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=silt-based%20material" title="silt-based material">silt-based material</a>, <a href="https://publications.waset.org/abstracts/search?q=raw%20earth%20concrete" title=" raw earth concrete"> raw earth concrete</a>, <a href="https://publications.waset.org/abstracts/search?q=stress-strain%20curve" title=" stress-strain curve"> stress-strain curve</a>, <a href="https://publications.waset.org/abstracts/search?q=energy" title=" energy"> energy</a>, <a href="https://publications.waset.org/abstracts/search?q=toughness" title=" toughness"> toughness</a> </p> <a href="https://publications.waset.org/abstracts/142789/toughness-of-a-silt-based-construction-material-reinforced-with-fibers" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/142789.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">221</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8703</span> Cross Section Measurement for Formation of Metastable State of ¹¹¹ᵐCd through ¹¹¹Cd (γ, γ`) ¹¹¹ᵐCd Reaction Induced by Bremsstrahlung Generated through 6 MeV Electrons</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Vishal%20D.%20Bharud">Vishal D. Bharud</a>, <a href="https://publications.waset.org/abstracts/search?q=B.%20J.%20Patil"> B. J. Patil</a>, <a href="https://publications.waset.org/abstracts/search?q=S.%20S.%20Dahiwale"> S. S. Dahiwale</a>, <a href="https://publications.waset.org/abstracts/search?q=V.%20N.%20Bhoraskar"> V. N. Bhoraskar</a>, <a href="https://publications.waset.org/abstracts/search?q=S.%20D.%20Dhole"> S. D. Dhole</a> </p> <p class="card-text"><strong>Abstract:</strong></p> Photon induced average reaction cross section of ¹¹¹Cd (γ, γ`) ¹¹¹ᵐCd reaction was experimentally determined for the bremsstrahlung energy spectrum of 6 MeV by utilizing the activation and offline γ-ray spectrometric techniques. The 6 MeV electron accelerator Racetrack Microtron of Savitribai Phule Pune University, Pune was used for the experimental work. The bremsstrahlung spectrum generated by bombarding 6 MeV electrons on lead target was theoretically estimated by FLUKA code. Bremsstrahlung radiation can have energies exceeding the threshold of the particle emission, which is normally above 6 MeV. Photons of energies below the particle emission threshold undergo absorption into discrete energy levels, with possibility of exciting nuclei to excited state including metastable state. The ¹¹¹Cd (γ, γ`) ¹¹¹ᵐCd reaction cross sections were calculated at different energies of bombarding Photon by using the TALYS 1.8 computer code with a default parameter. The focus of the present work was to study the (γ,γ’) reaction for exciting ¹¹¹Cd nuclei to metastable states which have threshold energy below 3 MeV. The flux weighted average cross section was obtained from the theoretical values of TALYS 1.8 and TENDL 2017 and is found to be in good agreement with the present experimental cross section. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=bremsstrahlung" title="bremsstrahlung">bremsstrahlung</a>, <a href="https://publications.waset.org/abstracts/search?q=cross%20section" title=" cross section"> cross section</a>, <a href="https://publications.waset.org/abstracts/search?q=FLUKA" title=" FLUKA"> FLUKA</a>, <a href="https://publications.waset.org/abstracts/search?q=TALYS-1.8" title=" TALYS-1.8"> TALYS-1.8</a> </p> <a href="https://publications.waset.org/abstracts/97710/cross-section-measurement-for-formation-of-metastable-state-of-111cd-through-111cd-gh-gh-111cd-reaction-induced-by-bremsstrahlung-generated-through-6-mev-electrons" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/97710.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">172</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8702</span> Reusability of Coimmobilized Enzymes</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Aleksandra%20%C5%81ochowicz">Aleksandra Łochowicz</a>, <a href="https://publications.waset.org/abstracts/search?q=Daria%20%C5%9Awi%C4%99tochowska"> Daria Świętochowska</a>, <a href="https://publications.waset.org/abstracts/search?q=Loredano%20Pollegioni"> Loredano Pollegioni</a>, <a href="https://publications.waset.org/abstracts/search?q=Nazim%20Ocal"> Nazim Ocal</a>, <a href="https://publications.waset.org/abstracts/search?q=Franck%20Charmantray"> Franck Charmantray</a>, <a href="https://publications.waset.org/abstracts/search?q=Laurence%20Hecquet"> Laurence Hecquet</a>, <a href="https://publications.waset.org/abstracts/search?q=Katarzyna%20Szyma%C5%84ska"> Katarzyna Szymańska</a> </p> <p class="card-text"><strong>Abstract:</strong></p> Multienzymatic cascade reactions are nowadays widely used in pharmaceutical, chemical and cosmetics industries to produce high valuable compounds. They can be carried out in two ways, step by step and one-pot. If two or more enzymes are in the same reaction vessel is necessary to work out the compromise to run the reaction in optimal conditions for each enzyme. So far most of the reports of multienzymatic cascades concern on usage of free enzymes. Unfortunately using free enzymes as catalysts of reactions accomplish high cost. What is more, free enzymes are soluble in solvents which makes reuse impossible. To overcome this obstacle enzymes can be immobilized what provides heterogeneity of biocatalyst that enables reuse and easy separation of the enzyme from solvents and reaction products. Usually, immobilization increase also the thermal and operational stability of enzyme. The advantages of using immobilized multienzymes are enhanced enzyme stability, improved cascade enzymatic activity via substrate channeling, and ease of recovery for reuse. The one-pot immobilized multienzymatic cascade can be carried out in mixed or coimmobilized type. When biocatalysts are coimmobilized on the same carrier the are in close contact to each other which increase the reaction rate and catalytic efficiency, and eliminate the lag time. However, in this type providing the optimal conditions both in the process of immobilization and cascade reaction for each enzyme is complicated. Herein, we examined immobilization of 3 enzymes: D-amino acid oxidase from Rhodotorula gracilis, commercially available catalase and transketolase from Geobacillus stearothermophilus. As a support we used silica monoliths with hierarchical structure of pores. Then we checked their stability and reusability in one-pot cascade of L-erythrulose and hydroxypuryvate acid synthesis. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=biocatalysts" title="biocatalysts">biocatalysts</a>, <a href="https://publications.waset.org/abstracts/search?q=enzyme%20immobilization" title=" enzyme immobilization"> enzyme immobilization</a>, <a href="https://publications.waset.org/abstracts/search?q=multienzymatic%20reaction" title=" multienzymatic reaction"> multienzymatic reaction</a>, <a href="https://publications.waset.org/abstracts/search?q=silica%20carriers" title=" silica carriers"> silica carriers</a> </p> <a href="https://publications.waset.org/abstracts/152282/reusability-of-coimmobilized-enzymes" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/152282.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">150</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8701</span> Dissolution Leaching Kinetics of Ulexite in Disodium Hydrogen Phosphate Solutions</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Bet%C3%BCl%20%C3%96zgen%C3%A7">Betül Özgenç</a>, <a href="https://publications.waset.org/abstracts/search?q=Soner%20Ku%C5%9Flu"> Soner Kuşlu</a>, <a href="https://publications.waset.org/abstracts/search?q=Sabri%20%C3%87olak"> Sabri Çolak</a>, <a href="https://publications.waset.org/abstracts/search?q=Turan%20%C3%87alban"> Turan Çalban</a> </p> <p class="card-text"><strong>Abstract:</strong></p> The aim of this study was investigate the leaching kinetics of ulexite in disodium hydrogen phosphate solutions in a mechanical agitation system. Reaction temperature, concentration of disodium hydrogen phosphate solutions, stirring speed, solid/liquid ratio and ulexite particle size were selected as parameters. The experimental results were successfully correlated by linear regression using Statistica program. Dissolution curves were evaluated shrinking core models for solid-fluid systems. It was observed that increase in the reaction temperature and decrease in the solid/liquid ratio causes an increase the dissolution rate of ulexite. The activation energy was found to be 63.4 kJ/mol. The leaching of ulexite was controlled by chemical reaction. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=ulexite" title="ulexite">ulexite</a>, <a href="https://publications.waset.org/abstracts/search?q=disodium%20hydrogen%20phosphate" title=" disodium hydrogen phosphate"> disodium hydrogen phosphate</a>, <a href="https://publications.waset.org/abstracts/search?q=leaching%20kinetics" title=" leaching kinetics"> leaching kinetics</a> </p> <a href="https://publications.waset.org/abstracts/27457/dissolution-leaching-kinetics-of-ulexite-in-disodium-hydrogen-phosphate-solutions" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/27457.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">410</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8700</span> Asymmetric Synthesis of Catalponol Using Chiral Iridium Catalyst </h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Takeyuki%20Suzuki">Takeyuki Suzuki</a>, <a href="https://publications.waset.org/abstracts/search?q=Ismiyarto"> Ismiyarto</a>, <a href="https://publications.waset.org/abstracts/search?q=Da-Yang%20Zhou"> Da-Yang Zhou</a>, <a href="https://publications.waset.org/abstracts/search?q=Kaori%20Asano"> Kaori Asano</a>, <a href="https://publications.waset.org/abstracts/search?q=Hiroaki%20Sasai"> Hiroaki Sasai</a> </p> <p class="card-text"><strong>Abstract:</strong></p> The development of catalytic asymmetric reaction is important for the synthesis of natural products. To construct the multiple stereogenic centers, the desymmetrization of meso compounds is powerful strategy for the synthesis of chiral molecules. Oxidative desymmetrization of meso diols using chiral iridium catalyst provides a chiral hydroxyl ketone. The reaction is practical and an environmentally benign method which does not require the use of stoichiometric amount of heavy metals. This time we report here catalytic asymmetric synthesis of catalponol based on tandem coupling of meso-diols and an aldehyde. The tandem reaction includes oxidative desymmetrization of meso-diols, aldol condensation with an aldehyde. The reaction of meso-diol, benzaldehyde in the presence of a catalytic amount of chiral Ir complex and CsOH in tetrahydrofuran afforded the desired benzylidene ketone in 82% yield with 96% ee (enantiomeric excess). Next, we applied this benzylidene ketone derivative to the synthesis of catalponol. The corresponding benzylidene ketone was obtained in 87% yield with 99% ee. Finally, catalponol was synthesized by the regio- and stereo-selective reduction of dienone moiety in good yield. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=catalponol" title="catalponol">catalponol</a>, <a href="https://publications.waset.org/abstracts/search?q=desymmetrization" title=" desymmetrization"> desymmetrization</a>, <a href="https://publications.waset.org/abstracts/search?q=iridium" title=" iridium"> iridium</a>, <a href="https://publications.waset.org/abstracts/search?q=oxidation" title=" oxidation"> oxidation</a> </p> <a href="https://publications.waset.org/abstracts/95973/asymmetric-synthesis-of-catalponol-using-chiral-iridium-catalyst" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/95973.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">170</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8699</span> HCIO4-SiO2 Nanoparticles as an Efficient Catalyst for Three-Component Synthesis of Triazolo[1,2-A]Indazole-Triones</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Hossein%20Anaraki-Ardakani">Hossein Anaraki-Ardakani</a>, <a href="https://publications.waset.org/abstracts/search?q=Tayebe%20Heidari-Rakati"> Tayebe Heidari-Rakati </a> </p> <p class="card-text"><strong>Abstract:</strong></p> An environmentally benign protocol for the one-pot, three-component synthesis of Triazolo[1,2-a]indazole-1,3,8-trione derivatives by condensation of dimedone, urazole and aromatic aldehydes catalyzed by HClO4/SiO2 NPS as an ecofriendly catalyst with high catalytic activity and reusability at 100 ºC under solvent-free conditions is reported. The reaction proceeds to completion within 20-30 min in 77-86 % yield. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=one-pot%20reaction" title="one-pot reaction">one-pot reaction</a>, <a href="https://publications.waset.org/abstracts/search?q=dimedone" title=" dimedone"> dimedone</a>, <a href="https://publications.waset.org/abstracts/search?q=triazoloindazole" title=" triazoloindazole"> triazoloindazole</a>, <a href="https://publications.waset.org/abstracts/search?q=urazole" title=" urazole"> urazole</a> </p> <a href="https://publications.waset.org/abstracts/18404/hcio4-sio2-nanoparticles-as-an-efficient-catalyst-for-three-component-synthesis-of-triazolo12-aindazole-triones" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/18404.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">372</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8698</span> Formation of the Water Assisted Supramolecular Assembly in the Transition Structure of Organocatalytic Asymmetric Aldol Reaction: A DFT Study</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Kuheli%20Chakrabarty">Kuheli Chakrabarty</a>, <a href="https://publications.waset.org/abstracts/search?q=Animesh%20Ghosh"> Animesh Ghosh</a>, <a href="https://publications.waset.org/abstracts/search?q=Atanu%20Roy"> Atanu Roy</a>, <a href="https://publications.waset.org/abstracts/search?q=Gourab%20Kanti%20Das"> Gourab Kanti Das</a> </p> <p class="card-text"><strong>Abstract:</strong></p> Aldol reaction is an important class of carbon-carbon bond forming reactions. One of the popular ways to impose asymmetry in aldol reaction is the introduction of chiral auxiliary that binds the approaching reactants and create dissymmetry in the reaction environment, which finally evolves to enantiomeric excess in the aldol products. The last decade witnesses the usage of natural amino acids as chiral auxiliary to control the stereoselectivity in various carbon-carbon bond forming processes. In this context, L-proline was found to be an effective organocatalyst in asymmetric aldol additions. In last few decades the use of water as solvent or co-solvent in asymmetric organocatalytic reaction is increased sharply. Simple amino acids like L-proline does not catalyze asymmetric aldol reaction in aqueous medium not only that, In organic solvent medium high catalytic loading (~30 mol%) is required to achieve moderate to high asymmetric induction. In this context, huge efforts have been made to modify L-proline and 4-hydroxy-L-proline to prepare organocatalyst for aqueous medium asymmetric aldol reaction. Here, we report the result of our DFT calculations on asymmetric aldol reaction of benzaldehyde, p-NO2 benzaldehyde and t-butyraldehyde with a number of ketones using L-proline hydrazide as organocatalyst in wet solvent free condition. Gaussian 09 program package and Gauss View program were used for the present work. Geometry optimizations were performed using B3LYP hybrid functional and 6-31G(d,p) basis set. Transition structures were confirmed by hessian calculation and IRC calculation. As the reactions were carried out in solvent free condition, No solvent effect were studied theoretically. Present study has revealed for the first time, the direct involvement of two water molecules in the aldol transition structures. In the TS, the enamine and the aldehyde is connected through hydrogen bonding by the assistance of two intervening water molecules forming a supramolecular network. Formation of this type of supramolecular assembly is possible due to the presence of protonated -NH2 group in the L-proline hydrazide moiety, which is responsible for the favorable entropy contribution to the aldol reaction. It is also revealed from the present study that, water assisted TS is energetically more favorable than the TS without involving any water molecule. It can be concluded from this study that, insertion of polar group capable of hydrogen bond formation in the L-proline skeleton can lead to a favorable aldol reaction with significantly high enantiomeric excess in wet solvent free condition by reducing the activation barrier of this reaction. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=aldol%20reaction" title="aldol reaction">aldol reaction</a>, <a href="https://publications.waset.org/abstracts/search?q=DFT" title=" DFT"> DFT</a>, <a href="https://publications.waset.org/abstracts/search?q=organocatalysis" title=" organocatalysis"> organocatalysis</a>, <a href="https://publications.waset.org/abstracts/search?q=transition%20structure" title=" transition structure "> transition structure </a> </p> <a href="https://publications.waset.org/abstracts/25023/formation-of-the-water-assisted-supramolecular-assembly-in-the-transition-structure-of-organocatalytic-asymmetric-aldol-reaction-a-dft-study" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/25023.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">434</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8697</span> Laccase Catalysed Conjugation of Tea Polyphenols for Enhanced Antioxidant Properties</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Parikshit%20Gogo">Parikshit Gogo</a>, <a href="https://publications.waset.org/abstracts/search?q=N.%20N.%20Dutta"> N. N. Dutta</a> </p> <p class="card-text"><strong>Abstract:</strong></p> The oxidative enzymes specially laccase (benzenediol: oxygen oxidoreductase, E.C.1.10.3.2) from bacteria, fungi and plants have been playing an important role in green technologies due to their specific advantageous properties. Laccase from different sources and in different forms was used as a biocatalyst in many oxidation and conjugation reactions starting from phenol to hydrocarbons. Tea polyphenols and its derivatives attract the scientific community because of their potential use as antioxidants in food, pharmaceutical and cosmetic industries. Conjugate of polyphenols emerged as a novel materials which shows better stability and antioxidant properties in applied fields. The conjugation reaction of catechin with poly (allylamine) has been studied using free, immobilized and cross-linked enzyme crystals (CLEC) of laccase from Trametes versicolor with particular emphasis on the effect of pertinent variables and kinetic aspects of the reaction. The stability and antioxidant property of the conjugated product was improved as compared to the unconjugated tea polyphenols. The reaction was studied in 11 different solvents in order to deduce the solvent effect through an attempt to correlate the initial reaction rate with solvent properties such as hydrophobicity (logP), water solubility (logSw), electron pair acceptance (ETN) and donation abilities (DNN), polarisibility and dielectric constant which exhibit reasonable correlations. The study revealed, in general that polar solvents favour the initial reaction rate. The kinetics of the conjugation reaction conformed to the so-called Ping-Pong-Bi-Bi mechanism with catechin inhibition. The stability as well as activity of the CLEC was better than the free enzymes and immobilized laccase for practical application. In case of immobilized laccase system marginal diffusional limitation could be inferred from the experimental data. The kinetic parameters estimated by non-linear regression analysis were found to be KmPAA(mM) = 0.75, 1.8967 and Kmcat (mM) = 11.769, 15.1816 for free and immobilized laccase respectively. An attempt has been made to assess the activity of the laccase for the conjugation reaction in relation to other reactions such as dimerisation of ferulic acids and develop a protocol to enhance polyphenol antioxidant activity. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=laccase" title="laccase">laccase</a>, <a href="https://publications.waset.org/abstracts/search?q=catechin" title=" catechin"> catechin</a>, <a href="https://publications.waset.org/abstracts/search?q=conjugation%20reaction" title=" conjugation reaction"> conjugation reaction</a>, <a href="https://publications.waset.org/abstracts/search?q=antioxidant%20properties" title=" antioxidant properties"> antioxidant properties</a> </p> <a href="https://publications.waset.org/abstracts/28634/laccase-catalysed-conjugation-of-tea-polyphenols-for-enhanced-antioxidant-properties" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/28634.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">270</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8696</span> Design and Development of Optical Sensor Based Ground Reaction Force Measurement Platform for GAIT and Geriatric Studies</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=K.%20Chethana">K. Chethana</a>, <a href="https://publications.waset.org/abstracts/search?q=A.%20S.%20Guru%20Prasad"> A. S. Guru Prasad</a>, <a href="https://publications.waset.org/abstracts/search?q=S.%20N.%20Omkar"> S. N. Omkar</a>, <a href="https://publications.waset.org/abstracts/search?q=B.%20Vadiraj"> B. Vadiraj</a>, <a href="https://publications.waset.org/abstracts/search?q=S.%20Asokan"> S. Asokan</a> </p> <p class="card-text"><strong>Abstract:</strong></p> This paper describes an ab-initio design, development and calibration results of an Optical Sensor Ground Reaction Force Measurement Platform (OSGRFP) for gait and geriatric studies. The developed system employs an array of FBG sensors to measure the respective ground reaction forces from all three axes (X, Y and Z), which are perpendicular to each other. The novelty of this work is two folded. One is in its uniqueness to resolve the tri axial resultant forces during the stance in to the respective pure axis loads and the other is the applicability of inherently advantageous FBG sensors which are most suitable for biomechanical instrumentation. To validate the response of the FBG sensors installed in OSGRFP and to measure the cross sensitivity of the force applied in other directions, load sensors with indicators are used. Further in this work, relevant mathematical formulations are presented for extracting respective ground reaction forces from wavelength shifts/strain of FBG sensors on the OSGRFP. The result of this device has implications in understanding the foot function, identifying issues in gait cycle and measuring discrepancies between left and right foot. The device also provides a method to quantify and compare relative postural stability of different subjects under test, which has implications in post surgical rehabilitation, geriatrics and optimizing training protocols for sports personnel. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=balance%20and%20stability" title="balance and stability">balance and stability</a>, <a href="https://publications.waset.org/abstracts/search?q=gait%20analysis" title=" gait analysis"> gait analysis</a>, <a href="https://publications.waset.org/abstracts/search?q=FBG%20applications" title=" FBG applications"> FBG applications</a>, <a href="https://publications.waset.org/abstracts/search?q=optical%20sensor%20ground%20reaction%20force%20platform" title=" optical sensor ground reaction force platform"> optical sensor ground reaction force platform</a> </p> <a href="https://publications.waset.org/abstracts/41550/design-and-development-of-optical-sensor-based-ground-reaction-force-measurement-platform-for-gait-and-geriatric-studies" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/41550.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">403</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8695</span> Identification Algorithm of Critical Interface, Modelling Perils on Critical Infrastructure Subjects</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Ji%C5%99%C3%AD.%20J.%20Urb%C3%A1nek">Jiří. J. Urbánek</a>, <a href="https://publications.waset.org/abstracts/search?q=Hana%20Malachov%C3%A1"> Hana Malachová</a>, <a href="https://publications.waset.org/abstracts/search?q=Josef%20Krahulec"> Josef Krahulec</a>, <a href="https://publications.waset.org/abstracts/search?q=Jitka%20Johanidisov%C3%A1"> Jitka Johanidisová</a> </p> <p class="card-text"><strong>Abstract:</strong></p> The paper deals with crisis situations investigation and modelling within the organizations of critical infrastructure. Every crisis situation has an origin in the emergency event occurrence in the organizations of energetic critical infrastructure especially. Here, the emergency events can be both the expected events, then crisis scenarios can be pre-prepared by pertinent organizational crisis management authorities towards their coping or the unexpected event (Black Swan effect) – without pre-prepared scenario, but it needs operational coping of crisis situations as well. The forms, characteristics, behaviour and utilization of crisis scenarios have various qualities, depending on real critical infrastructure organization prevention and training processes. An aim is always better organizational security and continuity obtainment. This paper objective is to find and investigate critical/ crisis zones and functions in critical situations models of critical infrastructure organization. The DYVELOP (Dynamic Vector Logistics of Processes) method is able to identify problematic critical zones and functions, displaying critical interfaces among actors of crisis situations on the DYVELOP maps named Blazons. Firstly, for realization of this ability is necessary to derive and create identification algorithm of critical interfaces. The locations of critical interfaces are the flags of crisis situation in real organization of critical infrastructure. Conclusive, the model of critical interface will be displayed at real organization of Czech energetic crisis infrastructure subject in Black Out peril environment. The Blazons need live power Point presentation for better comprehension of this paper mission. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=algorithm" title="algorithm">algorithm</a>, <a href="https://publications.waset.org/abstracts/search?q=crisis" title=" crisis"> crisis</a>, <a href="https://publications.waset.org/abstracts/search?q=DYVELOP" title=" DYVELOP"> DYVELOP</a>, <a href="https://publications.waset.org/abstracts/search?q=infrastructure" title=" infrastructure"> infrastructure</a> </p> <a href="https://publications.waset.org/abstracts/38771/identification-algorithm-of-critical-interface-modelling-perils-on-critical-infrastructure-subjects" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/38771.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">408</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8694</span> The Effect of Taekwondo on Plantar Pressure Distribution and Arch Index</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Maryam%20Kakavand">Maryam Kakavand</a>, <a href="https://publications.waset.org/abstracts/search?q=Samira%20Entezari"> Samira Entezari</a>, <a href="https://publications.waset.org/abstracts/search?q=Sara%20Khoshjamalfekri"> Sara Khoshjamalfekri</a>, <a href="https://publications.waset.org/abstracts/search?q=Raghad%20%20Mimar"> Raghad Mimar</a> </p> <p class="card-text"><strong>Abstract:</strong></p> The objective of this study is 1) to compare elite female and beginner taekwondo players in terms of plantar pressure distribution, vertical ground reaction force, contact area, mean pressure, and right and left longitudinal arches, and 2) to compare preferred and non-preferred limbs among elite players. To the best of authors’ knowledge, as of yet, there is no information available about the plantar pressure distribution and arch index among taekwondo players. Material and Methods: An analytical-comparative research method is applied. Therefore seven elite athletes and eight novice athletes were selected. The emed-C50 platform was used to assess plantar pressure distribution, vertical ground reaction force, contact area, mean pressure of different areas, and planter longitudinal arch in a second step protocol. Independent t-test and dependent t-test were used at a level of 0.05 to compare the elites and beginners' right and left feet, and preferred and non-preferred limbs among elite athletes, respectively. Results: In comparing the right and left limbs of elite and beginner groups, findings indicate that there is only a significant difference in the mean pressure of the first metatarsal of the right foot. Findings also showed a significant difference in the contact area of the toes 3, 4, 5 regions between elites’ preferred and non-preferred limbs. However, no significant difference was found between the two groups’ right and left limbs and elites’ preferred and non-preferred limbs in terms of pressure distribution, vertical ground reaction force, and arch index. Conclusion: It seems that taekwondo exercises have affected pressure distribution patterns among advanced players causing some differences in their planter pressure distribution pattern when compared to that of beginners. Therefore, taekwondo exercises may be a factor contributing to asymmetry performance in preferred and non-preferred limbs. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=planter%20pressure" title="planter pressure">planter pressure</a>, <a href="https://publications.waset.org/abstracts/search?q=arch%20index" title=" arch index"> arch index</a>, <a href="https://publications.waset.org/abstracts/search?q=taekwondo" title=" taekwondo"> taekwondo</a>, <a href="https://publications.waset.org/abstracts/search?q=elite" title=" elite"> elite</a> </p> <a href="https://publications.waset.org/abstracts/114635/the-effect-of-taekwondo-on-plantar-pressure-distribution-and-arch-index" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/114635.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">154</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8693</span> Graphene Supported Nano Cerium Oxides Hybrid as an Electrocatalyst for Oxygen Reduction Reactions</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Siba%20Soren">Siba Soren</a>, <a href="https://publications.waset.org/abstracts/search?q=Purnendu%20Parhi"> Purnendu Parhi</a> </p> <p class="card-text"><strong>Abstract:</strong></p> Today, the world is facing a severe challenge due to depletion of traditional fossil fuels. Scientists across the globe are working for a solution that involves a dramatic shift to practical and environmentally sustainable energy sources. High-capacity energy systems, such as metal-air batteries, fuel cells, are highly desirable to meet the urgent requirement of sustainable energies. Among the fuel cells, Direct methanol fuel cells (DMFCs) are recognized as an ideal power source for mobile applications and have received considerable attention in recent past. In this advanced electrochemical energy conversion technologies, Oxygen Reduction Reaction (ORR) is of utmost importance. However, the poor kinetics of cathodic ORR in DMFCs significantly hampers their possibilities of commercialization. The oxygen is reduced in alkaline medium either through a 4-electron (equation i) or a 2-electron (equation ii) reduction pathway at the cathode ((i) O₂ + 2H₂O + 4e⁻ → 4OH⁻, (ii) O₂ + H₂O + 2e⁻ → OH⁻ + HO₂⁻ ). Due to sluggish ORR kinetics the ability to control the reduction of molecular oxygen electrocatalytically is still limited. The electrocatalytic ORR starts with adsorption of O₂ on the electrode surface followed by O–O bond activation/cleavage and oxide removal. The reaction further involves transfer of 4 electrons and 4 protons. The sluggish kinetics of ORR, on the one hand, demands high loading of precious metal-containing catalysts (e.g., Pt), which unfavorably increases the cost of these electrochemical energy conversion devices. Therefore, synthesis of active electrocatalyst with an increase in ORR performance is need of the hour. In the recent literature, there are many reports on transition metal oxide (TMO) based ORR catalysts for their high activity TMOs are also having drawbacks like low electrical conductivity, which seriously affects the electron transfer process during ORR. It was found that 2D graphene layer is having high electrical conductivity, large surface area, and excellent chemical stability, appeared to be an ultimate choice as support material to enhance the catalytic performance of bare metal oxide. g-C₃N₄ is also another candidate that has been used by the researcher for improving the ORR performance of metal oxides. This material provides more active reaction sites than other N containing carbon materials. Rare earth oxide like CeO₂ is also a good candidate for studying the ORR activity as the metal oxide not only possess unique electronic properties but also possess catalytically active sites. Here we will discuss the ORR performance (in alkaline medium) of N-rGO/C₃N₄ supported nano Cerium Oxides hybrid synthesized by microwave assisted Solvothermal method. These materials exhibit superior electrochemical stability and methanol tolerance capability to that of commercial Pt/C. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=oxygen%20reduction%20reaction" title="oxygen reduction reaction">oxygen reduction reaction</a>, <a href="https://publications.waset.org/abstracts/search?q=electrocatalyst" title=" electrocatalyst"> electrocatalyst</a>, <a href="https://publications.waset.org/abstracts/search?q=cerium%20oxide" title=" cerium oxide"> cerium oxide</a>, <a href="https://publications.waset.org/abstracts/search?q=graphene" title=" graphene"> graphene</a> </p> <a href="https://publications.waset.org/abstracts/81299/graphene-supported-nano-cerium-oxides-hybrid-as-an-electrocatalyst-for-oxygen-reduction-reactions" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/81299.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">194</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8692</span> Effect of Addition and Reduction of Sharia Index Constituents</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Rosyidah">Rosyidah</a>, <a href="https://publications.waset.org/abstracts/search?q=Permata%20Wulandari"> Permata Wulandari</a> </p> <p class="card-text"><strong>Abstract:</strong></p> We investigate the price effect of addition and deletions from the Indonesia Sharia Stock Index (ISSI) and Jakarta Islamic Index (JII). Using event study methodology, we measure abnormal returns for firms over the period June 2019 - to December 2021. Through the sample of 107 additions and 95 deletions, we find evidence to support the theory of Muslim country investment behavior. We find that additions to the Islamic index led to a significant positive stock market reaction and deletions to the Islamic index led to a negative stock market reaction on Jakarta Islamic Index (JII) and there is no significant reaction of addition and deletion on Indonesia Sharia Stock Index (ISSI). <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=abnormal%20return" title="abnormal return">abnormal return</a>, <a href="https://publications.waset.org/abstracts/search?q=abnormal%20volume" title=" abnormal volume"> abnormal volume</a>, <a href="https://publications.waset.org/abstracts/search?q=event%20study" title=" event study"> event study</a>, <a href="https://publications.waset.org/abstracts/search?q=index%20changes" title=" index changes"> index changes</a>, <a href="https://publications.waset.org/abstracts/search?q=sharia%20index" title=" sharia index"> sharia index</a> </p> <a href="https://publications.waset.org/abstracts/149421/effect-of-addition-and-reduction-of-sharia-index-constituents" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/149421.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">130</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8691</span> Removal of Lead from Aqueous Solutions by Biosorption on Pomegranate Skin: Kinetics, Equilibrium and Thermodynamics</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Y.%20Laidani">Y. Laidani</a>, <a href="https://publications.waset.org/abstracts/search?q=G.%20Henini"> G. Henini</a>, <a href="https://publications.waset.org/abstracts/search?q=S.%20Hanini"> S. Hanini</a>, <a href="https://publications.waset.org/abstracts/search?q=A.%20Labbaci"> A. Labbaci</a>, <a href="https://publications.waset.org/abstracts/search?q=F.%20Souahi"> F. Souahi</a> </p> <p class="card-text"><strong>Abstract:</strong></p> In this study, pomegranate skin, a material suitable for the conditions in Algeria, was chosen as adsorbent material for removal of lead in an aqueous solution. Biosorption studies were carried out under various parameters such as mass adsorbent particle, pH, contact time, the initial concentration of metal, and temperature. The experimental results show that the percentage of biosorption increases with an increase in the biosorbent mass (0.25 g, 0.035 mg/g; 1.25 g, 0.096 mg/g). The maximum biosorption occurred at pH value of 8 for the lead. The equilibrium uptake was increased with an increase in the initial concentration of metal in solution (Co = 4 mg/L, q<sub>t</sub> = 1.2 mg/g). Biosorption kinetic data were properly fitted with the pseudo-second-order kinetic model. The best fit was obtained by the Langmuir model with high correlation coefficients (R<sup>2</sup> > 0.995) and a maximum monolayer adsorption capacity of 0.85 mg/g for lead. The adsorption of the lead was exothermic in nature (ΔH° = -17.833 kJ/mol for Pb (II). The reaction was accompanied by a decrease in entropy (ΔS° = -0.056 kJ/K. mol). The Gibbs energy (ΔG°) increased from -1.458 to -0.305 kJ/mol, respectively for Pb (II) when the temperature was increased from 293 to 313 K. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=biosorption" title="biosorption">biosorption</a>, <a href="https://publications.waset.org/abstracts/search?q=Pb%20%28%2BII%29" title=" Pb (+II)"> Pb (+II)</a>, <a href="https://publications.waset.org/abstracts/search?q=pomegranate%20skin" title=" pomegranate skin"> pomegranate skin</a>, <a href="https://publications.waset.org/abstracts/search?q=wastewater" title=" wastewater"> wastewater</a> </p> <a href="https://publications.waset.org/abstracts/49784/removal-of-lead-from-aqueous-solutions-by-biosorption-on-pomegranate-skin-kinetics-equilibrium-and-thermodynamics" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/49784.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">270</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8690</span> Study on the Changes in Material Strength According to Changes in Forming Methods in Hot-Stamping Process</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Yong-Jun%20Jeon">Yong-Jun Jeon</a>, <a href="https://publications.waset.org/abstracts/search?q=Hyung-Pil%20Park"> Hyung-Pil Park</a>, <a href="https://publications.waset.org/abstracts/search?q=Min-Jae%20Song"> Min-Jae Song</a>, <a href="https://publications.waset.org/abstracts/search?q=Baeg-Soon%20Cha"> Baeg-Soon Cha</a> </p> <p class="card-text"><strong>Abstract:</strong></p> Following the recent trend of having increased demand in producing lighter-weight car bodies for improvement of automobile safety and gas mileage, there is a forming method that makes use of hot-stamping technique, which satisfies all conditions mentioned above. Hot-stamping is a forming technique with advantages of excellent formability, good dimensional precision and others since it is a process in which steel plates are heated up to temperatures of at least approximately 900°C after which forming is conducted in die at room temperature followed by rapid cooling. In addition, it has characteristics of allowing for improvement in material strength through achievement of quenching effect by having simultaneous forming and rapid cooling of material of high temperatures. However, there is insufficient information on the changes in material strength according to changes in material temperature with regards to material heating method and forming process in hot-stamping. Accordingly, this study aims to design and press die for T-type product of the scale models of the center pillar and to understand the changes in material strength in relation to changes in forming methods of hot-stamping process. Thus in order to understand the changes in material strength due to quenching effect among the hot-stamping process, material strength and material forming precision were to be studied while varying the forming and forming method when forming. For test methods, material strength was observed by using boron steel that has boron additives, which was heated up to 950°C, after which it was transferred to a die and was cooled down to material temperature of 400°C followed by air cooling process. During the forming and cooling process here, experiment was conducted with forming parameters of 2 holding rates and 3 flange heating rates wherein changing appearance in material strength according to changes forming method were observed by verifying forming strength and forming precision for each of the conditions. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=hot-stamping" title="hot-stamping">hot-stamping</a>, <a href="https://publications.waset.org/abstracts/search?q=formability" title=" formability"> formability</a>, <a href="https://publications.waset.org/abstracts/search?q=quenching" title=" quenching"> quenching</a>, <a href="https://publications.waset.org/abstracts/search?q=forming" title=" forming"> forming</a>, <a href="https://publications.waset.org/abstracts/search?q=press%20die" title=" press die"> press die</a>, <a href="https://publications.waset.org/abstracts/search?q=forming%20methods" title=" forming methods"> forming methods</a> </p> <a href="https://publications.waset.org/abstracts/7061/study-on-the-changes-in-material-strength-according-to-changes-in-forming-methods-in-hot-stamping-process" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/7061.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> Downloads <span class="badge badge-light">462</span> </span> </div> </div> <div class="card paper-listing mb-3 mt-3"> <h5 class="card-header" style="font-size:.9rem"><span class="badge badge-info">8689</span> Material Saving Strategies, Technologies and Effects on Return on Sales</h5> <div class="card-body"> <p class="card-text"><strong>Authors:</strong> <a href="https://publications.waset.org/abstracts/search?q=Jasna%20Prester">Jasna Prester</a>, <a href="https://publications.waset.org/abstracts/search?q=Najla%20Podrug"> Najla Podrug</a>, <a href="https://publications.waset.org/abstracts/search?q=Davor%20Filipovi%C4%87"> Davor Filipović</a> </p> <p class="card-text"><strong>Abstract:</strong></p> Manufacturing companies invest a significant amount of sales into material resources for production. In our sample, 58% of sales is used for manufacturing inputs, while only 24% of sales is used for salaries. This means that if a company is looking to reduce costs, the greater potential is in reduction of material costs than downsizing. This research shows that manufacturing companies in Croatia did realize material savings in last three years. It is also shown by which technologies they achieved materials cost savings. Through literature research, we found research gap as to which technologies reduce material consumption. As methodology of research four regression analyses are used to prove our findings. <p class="card-text"><strong>Keywords:</strong> <a href="https://publications.waset.org/abstracts/search?q=Croatia" title="Croatia">Croatia</a>, <a href="https://publications.waset.org/abstracts/search?q=materials%20savings%20strategies" title=" materials savings strategies"> materials savings strategies</a>, <a href="https://publications.waset.org/abstracts/search?q=technologies" title=" technologies"> technologies</a>, <a href="https://publications.waset.org/abstracts/search?q=return%20on%20sales" title=" return on sales"> return on sales</a> </p> <a href="https://publications.waset.org/abstracts/39863/material-saving-strategies-technologies-and-effects-on-return-on-sales" class="btn btn-primary btn-sm">Procedia</a> <a href="https://publications.waset.org/abstracts/39863.pdf" target="_blank" class="btn btn-primary btn-sm">PDF</a> <span class="bg-info text-light px-1 py-1 float-right rounded"> 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