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class="trig-item"><a href="javascript:;" target="_self" id="nav2">详细介绍</a></li><li class="trig-item"><a href="javascript:;" target="_self" id="nav6">技术资料</a></li> </ul> </div> <dl class="mtabx"> <dd class="mtite"><h2 class="f14 fw" id="m02">详细介绍</h2></dd> <dd class="mtitex"><span style="color: #b22222"><span style="font-size: 14px"><span style="font-size: 18px"><b>仪器简介：</b></span></span></span><br /> <p> <span style="color: #696969"><span style="font-size: 14px">不同于业内其他公司基于平面传感器结构的DSC产品（测试效率仅为20%~50%），法国塞塔拉姆（Setaram）公司的SENSYSEvolutionDSC系统得益于塞塔拉姆公司独有的基于卡尔维(CALVET)量热原理的“三维传感器”（“3D-sensor”）技术，能够更真实地反映样品的热性质（效率高达94%），并提供无以伦比的测试精度。而独特的三维传感器结构提供了更大的样品室容量（250uL），使得很多在其它仪器上无法实现的研究变为可能，如混合反应量热。样品室（坩埚）内加压，对传感器没有影响，使得基线稳定，并且节约气体。仪器高度模块化，可随时与热重(TG)及气体分析仪（FT-IR,MS）联用。<br /> </span></span><br /> <span style="color: #b22222"><span style="font-size: 14px"><span style="font-size: 18px"><strong>卡尔维原理：</strong></span></span></span><br /> <span style="color: #696969"><span style="font-size: 14px">法国化学家ECalvet教授zuixian设计制作了卡尔维式量热仪。以高灵敏度为特性，样品在实验过程中所产生的总热量有95%以上被检测出来，相对灵敏度（灵敏度/样品容量）非常高，可以测到非常微弱的热量变化（例如细菌活动产生的热变化），并且具有极高的信号稳定性。<br /> 整个量热仪所形成的隔热环境，可保持恒温稳定性达到±0.001~0.00001℃，可以作为开放体系进行内、外部的固-固、气-固、液-固、液-液等二相间的交换反应实验，这是普通热分析产品所无法达到的。如用微热测量表征混合物组分间相互作用、相容性、液体比热和催化剂的吸附/脱附等。</span></span></p> <br /> <br /> <span style="color: #b22222"><span style="font-size: 14px"><span style="font-size: 18px"><b>技术参数：</b></span></span></span><br /> <p> <span style="color: #696969"><span style="font-size: 14px">炉体： 温度范围：-120--830℃；温度重复性：+/-0.1%<br /> 可编程温度扫描速率：0.01-30℃/min<br /> DSC：最大样品容积：320μL；<br /> 分辨率：0.4μW，<br /> 检测限：5μw<br /> 样品池/坩埚最高承受压力：500bar，600℃<br /> 样品池/坩埚最高可监控压力：400bar，600℃</span></span></p> <p> <span style="color: #b22222"><span style="font-size: 18px"><strong>可加配TG升及成一台同步热分析仪：</strong></span></span></p> <p> <span style="color: #696969"><span style="font-size: 14px">TG最大样品量：35g<br /> TGA分辨率：0.03μg<br /> 气路：3路载气，1路反应/辅助气<br /> 气氛：氧化，还原（H2,CO)，腐蚀（H2S,NH3)，水蒸气<br /> 自动进样器：48样品<br /> 全新Calisto操作软件</span></span></p> <br /> <br /> <span style="color: #b22222"><span style="font-size: 14px"><span style="font-size: 18px"><b>主要特点：</b></span></span></span><br /> <p> <span style="color: #696969"><span style="font-size: 14px">*SENSYS DSC采用Setaram 独有的基于卡尔维量热原理的“三维传感器”（“3D-sensor”），更真实地反映样品的热性质（效率高达，并提供无以伦比的测试精度<br /> *-120/+830℃温度工作范围满足大多数研究需要<br /> *焦耳校准，排除样品形态、测试环境及操作对测试结果的影响<br /> *高性能Incloy合金坩埚可承受500bar的最大压力，工作温度600℃ ，非常适用于研究高压反应、危险化学品稳定性及过程安全的评估。<br /> *独特的三维传感器结构提供了更大的样品室容量，达250μL<br /> *样品室内加压，对传感器无冲击，基线稳定，且节约气体<br /> *坩埚内压力可监测并可控制，最高至400bar，600℃<br /> *可在还原气氛（H2,CO)及腐蚀气氛下工作<br /> *混合气路设计，可在50/50至1/99间任意比例混合两路反应气<br /> *可配备全自动进样系统，实现48个样品的自动连续测试<br /> *高度模块化，可随时与TG及气体分析仪（IR, GC, MS）联用<br /> *TG为上天平设计，不受加热炉影响，且测量更加准确<br /> *可与湿度控制器联用，研究可控湿度下的反应如吸附、水合及材料在特定湿度下稳定性等<br /> *全新Calisto操作软件，界面友好，功能强大，包含比热功能</span></span></p> </dd> <dd class="mtite mgbotm10"><h2 class="f14 fw" id="m06">技术资料</h2></dd> <dd class="mtabx"> <ul class="mtabds mtabdsb"> <li><i class="fl 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