Adsorption of a Cationic Dye Crystal Violet onto a Binary Mixture of Forest Waste Biopolymer: Advanced Statistical Physics Studies

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Myers, Surfaces, interfaces, and colloids, Wiley New York, (1999)." /> <meta name="person" content="Aga Sarra, Djama Chaker, Bouguettoucha Abdallah, Chebli Derradji, Amrane Abdeltif" /> <meta name="description" content="An eco-friendly and low cost modified mixture of both Wild Carob and Cupressus sempervirens with H3PO4 (Cupcar-H3PO4) was prepared to extract a cationic dye (Crystal Violet) from an aqueous solution in a batch reactor at the laboratory of chemical engineering, Department of Process Engineering, Faculty of Technology, Farhat Abbas Setif University-1. The pH effect, contact time, initial concentration of dye, ionic strength and temperature were investigated in this study. The Maximum adsorption capacity was found to be 117.26 mg/g at 25°C for a natural pH (ph =6.22). The active functional groups of Cupcar-H3PO4. These peak shifts indicated that especially the bonded –OH groups, C–O stretching of ether groups, and C=C group played a major role in CV adsorption onto Cupcar-H3PO4. The new bands of low intensity which appeared at 890 cm−1 and 813 cm-1 after CV adsorption and which could be attributed to a υ (CV-biosorbent) constituted the most striking result. Kinetics of biosorption of crystal violet (CV) was analyzed and the results showed that both pseudo order (PSO) and the pseud nth-order model (PNO) models gave most accurate fit than the pseudo-first-order model (PFO). Isotherm data were analyzed by four classical models, Langmuir and Freundlich with two parameters, Sips and Redlich-Peterson with three parameters. And for more information on the mechanism of CV uptake on the Cupcar-H3PO4 material, three advanced models are applied to isothermal data, Monolayer with one energy (M1), Monolayer with two energies (M2), and Double layer with one energy (M3). For the classical models and in the case of the two parameters models the Langmuir one gives a better fit for the data isotherm according to the R2. In the case of three parameters models, both Sips and Redlich-Peterson accurately described experimental data. Monolayer with two energy sites model (M2) was shown to be the most appropriate advanced statistical physics model for fitting CV biosorption onto the Cupcar-H3PO4 biosorbent, this model suggested that the CV pollutant was adsorbed at two different Cupcar-H3PO4 biosorbent sites, and that a variable number of CV molecules could be adsorbed at each site; from this, the CV dye was adsorbed with 2 different adsorption energies. The changes in the enthalpy, the standard free energy and the entropy were also evaluated and the reaction was found to be spontaneous, endothermic and physical in nature." /> <meta name="keywords" content="Adsorption, Crystal Violet, Isotherms, Kinetics, Physical Models, Wastewater" /> <meta name="copyright" content="2022 Trans Tech Publications Ltd. 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Dye Crystal Violet onto a Binary Mixture of Forest Waste Biopolymer: Advanced Statistical Physics Studies</h1> </div> <div class="paper-statistics"> <div class="loading"> <i class="inline-icon download-and-visitor-statistics-icon"></i> <span class="normal-text" id="paperDownloadsAndVisitorsCount"></span> </div> </div> <div class="clearfix"></div> <div class="page-paper-title"> <div class="preview-block"> <img alt="Article Preview" width="128" height="180" src="/AMR.1168.93/thumbnail.gif"> <div id="preview-button" data-url-preview-log="/Paper/PreviewImageLog?paperId=580769"> <i class="inline-icon preview-icon"></i> </div>  <div id="paper-preview-modal" class="modal fade"> <div class="modal-dialog" role="document"> <div class="popup-page-name underline-begin"> <div class="page-name-block-text">Article Preview</div> </div> <img alt="Article Preview" class="preview-image lazyload" data-src="/AMR.1168.93/preview.gif"> <a data-dismiss="modal" title="Close" class="inline-icon close-icon"></a> </div> </div>  </div> <div class="abstract-block-description"> <h3 class="page-paper-first-header">Abstract:</h3> <p class="normal-text"> An eco-friendly and low cost modified mixture of both Wild Carob and <i>Cupressus sempervirens</i> with H<sub>3</sub>PO<sub>4 </sub>(Cupcar-H<sub>3</sub>PO<sub>4</sub>) was prepared to extract a cationic dye (Crystal Violet) from an aqueous solution in a batch reactor at the laboratory of chemical engineering, Department of Process Engineering, Faculty of Technology, Farhat Abbas Setif University-1. The pH effect, contact time, initial concentration of dye, ionic strength and temperature were investigated in this study. The Maximum adsorption capacity was found to be 117.26 mg/g at 25°C for a natural pH (ph =6.22). The active functional groups of Cupcar-H<sub>3</sub>PO<sub>4</sub>. These peak shifts indicated that especially the bonded –OH groups, C–O stretching of ether groups, and C=C group played a major role in CV adsorption onto Cupcar-H<sub>3</sub>PO<sub>4</sub>. The new bands of low intensity which appeared at 890 cm<sup>−1</sup> and 813 cm<sup>-1</sup> after CV adsorption and which could be attributed to a υ (CV-biosorbent) constituted the most striking result. Kinetics of biosorption of crystal violet (CV) was analyzed and the results showed that both pseudo order (PSO) and the pseud nth-order model (PNO) models gave most accurate fit than the pseudo-first-order model (PFO). Isotherm data were analyzed by four classical models, Langmuir and Freundlich with two parameters, Sips and Redlich-Peterson with three parameters. And for more information on the mechanism of CV uptake on the Cupcar-H<sub>3</sub>PO<sub>4</sub> material, three advanced models are applied to isothermal data, Monolayer with one energy (M1), Monolayer with two energies (M2), and Double layer with one energy (M3). For the classical models and in the case of the two parameters models the Langmuir one gives a better fit for the data isotherm according to the R<sup>2</sup>. In the case of three parameters models, both Sips and Redlich-Peterson accurately described experimental data. Monolayer with two energy sites model (M2) was shown to be the most appropriate advanced statistical physics model for fitting CV biosorption onto the Cupcar-H<sub>3</sub>PO<sub>4 </sub>biosorbent, this model suggested that the CV pollutant was adsorbed at two different Cupcar-H<sub>3</sub>PO<sub>4 </sub>biosorbent sites, and that a variable number of CV molecules could be adsorbed at each site; from this, the CV dye was adsorbed with 2 different adsorption energies. The changes in the enthalpy, the standard free energy and the entropy were also evaluated and the reaction was found to be spontaneous, endothermic and physical in nature. </p> </div> <div class="paper-access-buttons col-xs-12"> <div class="row"> <div class="sa-button-wrap"> <a id="sa-button" class="wayfinder-login d-flex sa-button" href="javascript:;"> <div class="sa-button-logo-wrap"> <i class="inline-icon sa-white"></i> </div> <div class="d-flex justify-content-center align-items-center sa-button-text text-truncate"> <div class="sa-button-text-primary text-truncate">Access through your institution</div> </div> </a> </div> <div class="title-button-pdf"> <button id="readPaperButton" data-url-read-paper-log="/Paper/ReadThePaperLog?paperId=580769" class="button button-160"> <span class="inline-element">Read The Paper</span> </button> </div> </div> <div class="row"> </div> </div> <div class="clearfix"></div> <div class="connected-title-container"> <div class="connected-title-text 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href="/author-papers/chaker-djama">Djama Chaker</a>, <a class="inline-icon mail-icon-red author-send-message" href="#" data-url="/Paper/_Message?paperId=580769&personId=1572181&urlSent=https%3A%2F%2Fwww.scientific.net%2FAMR.1168.93" title="Send message to Corresponding Author"> </a> <a href="/author-papers/abdallah-bouguettoucha">Bouguettoucha Abdallah</a>*, <a href="/author-papers/chebli-derradji">Chebli Derradji</a>, <a href="/author-papers/abdeltif-amrane">Amrane Abdeltif</a> </div> </div> </div> </div> <div class="papers-block-info col-lg-12"> <div class="row"> <div class="info-row-name normal-text-gray col-md-2 col-sm-3 col-xs-4"> <div class="row"> <p>Keywords:</p> </div> </div> <div class="info-row-content semibold-middle-text col-md-10 col-sm-9 col-xs-8"> <div class="row"> <a href="/paper-keyword/adsorption">Adsorption</a>, <a href="/paper-keyword/crystal-violet-1">Crystal Violet</a>, <a href="/paper-keyword/isotherms">Isotherms</a>, <a 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