The Development Study of a Prototype of Sodium Carboxymethylcellulose and Poly(Vinyl Alcohol) Wound Dressings Using a Mixer Torque Rheometer

<!DOCTYPE html> <html lang="en" dir="ltr"> <head> <meta name="format-detection" content="telephone=no"> <meta name="viewport" content="width=device-width, initial-scale=1.0" /> <meta charset="utf-8"> <meta http-equiv="X-UA-Compatible" content="IE=edge"> <link rel="canonical" href="https://www.scientific.net/AMR.1171.25" /> <meta property="og:title" content="The Development Study of a Prototype of Sodium Carboxymethylcellulose and Poly(Vinyl Alcohol) Wound Dressings Using a Mixer Torque Rheometer | Scientific.Net" /> <meta property="og:type" content="website" /> <meta property="og:url" content="https://www.scientific.net/AMR.1171.25" /> <meta property="og:image" content="/Content/app/scinet5/images/metadata_logo.png" /> <meta property="og:image:type" content="image/png" /> <meta property="og:image:width" content="261" /> <meta property="og:image:height" content="260" /> <meta property="og:image:alt" content="Scientific.Net Logo" /> <meta name="citation_language" content="en" /> <meta name="citation_publisher" content="Trans Tech Publications Ltd" /> <meta name="citation_title" content="The Development Study of a Prototype of Sodium Carboxymethylcellulose and Poly(Vinyl Alcohol) Wound Dressings Using a Mixer Torque Rheometer" /> <meta name="citation_publication_date" content="2022" /> <meta name="citation_online_date" content="2022/05/03" /> <meta name="citation_journal_title" content="Advanced Materials Research" /> <meta name="citation_issn" content="1662-8985" /> <meta name="citation_volume" content="1171" /> <meta name="citation_firstpage" content="25" /> <meta name="citation_lastpage" content="47" /> <meta name="citation_pdf_url" content="https://www.scientific.net/AMR.1171.25.pdf" /> <meta name="citation_abstract_html_url" content="https://www.scientific.net/AMR.1171.25" /> <meta name="citation_keywords" content="Carboxymethilcellulose;Mix Torque Rheomether;Poly(Vinyl Alcohol);Wound Dressing" /> <meta name="citation_doi" content="10.4028/p-h118we" /> <meta name="citation_author" content="Alessandra Moreira de Oliveira" /> <meta name="citation_author" content="Ricardo da Silva Souza" /> <meta name="citation_author" content="Débora Omena Futuro" /> <meta name="citation_author" content="Valéria Gonçalves Costa" /> <meta name="citation_reference" content="citation_title=Modern wound dressings: Manufacturing and properties; citation_author=T. 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Entezami; citation_volume=33; citation_issue=1; citation_publication_date=2011/1; citation_pages=229-235; citation_doi=10.1016/j.indcrop.2010.10.016" /> <meta name="citation_reference" content="citation_title=Effect of starch type on the properties of starch containing films; citation_author=J.W. Lawton; citation_volume=29; citation_issue=3; citation_publication_date=1996/3; citation_pages=203-208; citation_doi=10.1016/0144-8617(96)00028-8" /> <meta name="citation_reference" content="C. Chang, L. Zhang. Cellulose-based hydrogels: Present status and application prospects. Carbohydr. Polym. 84(1) (2011) 40-56." /> <meta name="citation_reference" content="citation_title=Thermal, mechanical and water adsorption properties of corn starch–carboxymethylcellulose/methylcellulose biodegradable films; citation_author=E. Aytunga Arık Kibar; citation_author=Ferhunde Us; citation_volume=114; citation_issue=1; citation_publication_date=2013/1; citation_pages=123-131; citation_doi=10.1016/j.jfoodeng.2012.07.034" /> <meta name="person" content="Alessandra Moreira de Oliveira, Ricardo da Silva Souza, Débora Omena Futuro, Valéria Gonçalves Costa" /> <meta name="description" content="The search for new materials that serve as dressings and promote the proper means for wound healing, without yielding toxic waste to the wound bed and at low cost, is currently the subject of research. In this sense, the present study aimed to develop a prototype of a poly(vinyl alcohol) (PVA) polymeric film, sodium carboxymethylcellulose (NaCMC). PVA and NaCMC as miscible polymer blend films for wound dressings was developed using internal mixing chamber processing in a mix torque rheometer (MTR) without the use of binders or crosslinks in different mixing conditions that were investigated by thermal characteristics (differential scanning calorimetry (DSC)) and thermogravimetric analysis (TGA) and crystallinity (X-ray Diffraction Technique (XRD)). The films obtained by pouring from this starting material were characterized by DSC, TGA, Fourier transform infrared spectroscopy (FTIR), scanning electron microscope (SEM), optical microscopy and swelling assay. All stages of development of this prototype are discussed, from the quality control of the raw materials, through the development of the preparation technique of the blends in 14 different processing conditions. The processed PVA/NaCMC film showed physical crosslinking which may have promoted its ability to resist dissolution in water (unprocessed PVA/NaCMC films’ characteristic). The results demonstrated that the processing of the PVA and NaCMC polymers in the MTR constitutes a viable technique to obtain membranes for use as dressings." /> <meta name="keywords" content="Carboxymethilcellulose, Mix Torque Rheomether, Poly(Vinyl Alcohol), Wound Dressing" /> <meta name="copyright" content="2022 Trans Tech Publications Ltd. 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class="normal-large-text icon-container"> <div class="element-list"> <div class="element-list-text"> Effect of Different Chemical Admixtures on Fresh and Hardened Properties of M30 and M40 Grade Concrete <br /> <span class="paper-volume-number">p.105</span> </div> <div class="element-list-arrow"> <i class="inline-icon arrow-right-black no-focus-icon on-hover-arrow-left-red"></i> </div> </div> </a> </div> </div> <div class="right-content col-md-8 col-sm-7 col-xs-12 paper-title-main-page"> <div class="bread-crumbs hidden-xs"> <a class="bread-crumbs-first" href="/">Home</a><i class="inline-icon arrow-breadcrumbs"></i><a class="bread-crumbs-first" href="/AMR">Advanced Materials Research</a><i class="inline-icon arrow-breadcrumbs"></i><a class="bread-crumbs-first" href="/AMR.1171">Advanced Materials Research Vol. 1171</a><i class="inline-icon arrow-breadcrumbs"></i><span class="bread-crumbs-second">The Development Study of a Prototype of Sodium...</span></div> <div class="page-name-block underline-begin"> <h1 class="page-name-block-text">The Development Study of a Prototype of Sodium Carboxymethylcellulose and Poly(Vinyl Alcohol) Wound Dressings Using a Mixer Torque Rheometer</h1> </div> <div class="paper-statistics"> <div class="loading"> <i class="inline-icon download-and-visitor-statistics-icon"></i> <span class="normal-text" id="paperDownloadsAndVisitorsCount"></span> </div> </div> <div class="clearfix"></div> <div class="page-paper-title"> <div class="preview-block"> <img alt="Article Preview" width="128" height="180" src="/AMR.1171.25/thumbnail.gif"> <div id="preview-button" data-url-preview-log="/Paper/PreviewImageLog?paperId=577500"> <i class="inline-icon preview-icon"></i> </div>  <div id="paper-preview-modal" class="modal fade"> <div class="modal-dialog" role="document"> <div class="popup-page-name underline-begin"> <div class="page-name-block-text">Article Preview</div> </div> <img alt="Article Preview" class="preview-image lazyload" data-src="/AMR.1171.25/preview.gif"> <a data-dismiss="modal" title="Close" class="inline-icon close-icon"></a> </div> </div>  </div> <div class="abstract-block-description"> <h3 class="page-paper-first-header">Abstract:</h3> <p class="normal-text"> The search for new materials that serve as dressings and promote the proper means for wound healing, without yielding toxic waste to the wound bed and at low cost, is currently the subject of research. In this sense, the present study aimed to develop a prototype of a poly(vinyl alcohol) (PVA) polymeric film, sodium carboxymethylcellulose (NaCMC). PVA and NaCMC as miscible polymer blend films for wound dressings was developed using internal mixing chamber processing in a mix torque rheometer (MTR) without the use of binders or crosslinks in different mixing conditions that were investigated by thermal characteristics (differential scanning calorimetry (DSC)) and thermogravimetric analysis (TGA) and crystallinity (X-ray Diffraction Technique (XRD)). The films obtained by pouring from this starting material were characterized by DSC, TGA, Fourier transform infrared spectroscopy (FTIR), scanning electron microscope (SEM), optical microscopy and swelling assay. All stages of development of this prototype are discussed, from the quality control of the raw materials, through the development of the preparation technique of the blends in 14 different processing conditions. The processed PVA/NaCMC film showed physical crosslinking which may have promoted its ability to resist dissolution in water (unprocessed PVA/NaCMC films’ characteristic). The results demonstrated that the processing of the PVA and NaCMC polymers in the MTR constitutes a viable technique to obtain membranes for use as dressings. </p> </div> <div class="paper-access-buttons col-xs-12"> <div class="row"> <div class="sa-button-wrap"> <a id="sa-button" class="wayfinder-login d-flex sa-button" href="javascript:;"> <div class="sa-button-logo-wrap"> <i class="inline-icon sa-white"></i> </div> <div class="d-flex justify-content-center align-items-center sa-button-text text-truncate"> <div class="sa-button-text-primary text-truncate">Access through your institution</div> </div> </a> </div> <div class="title-button-pdf"> <button id="readPaperButton" data-url-read-paper-log="/Paper/ReadThePaperLog?paperId=577500" class="button button-160"> <span class="inline-element">Read The Paper</span> </button> </div> </div> <div class="row"> </div> </div> <div class="clearfix"></div> <div class="connected-title-container"> <div class="connected-title-text 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data-url="/Paper/_Message?paperId=577500&personId=1651792&urlSent=https%3A%2F%2Fwww.scientific.net%2FAMR.1171.25" title="Send message to Corresponding Author"> </a> <a href="/author-papers/alessandra-oliveira">Alessandra Moreira de Oliveira</a>*, <a href="/author-papers/ricardo-souza">Ricardo da Silva Souza</a>, <a href="/author-papers/débora-futuro">Débora Omena Futuro</a>, <a href="/author-papers/valéria-costa">Valéria Gonçalves Costa</a> </div> </div> </div> </div> <div class="papers-block-info col-lg-12"> <div class="row"> <div class="info-row-name normal-text-gray col-md-2 col-sm-3 col-xs-4"> <div class="row"> <p>Keywords:</p> </div> </div> <div class="info-row-content semibold-middle-text col-md-10 col-sm-9 col-xs-8"> <div class="row"> <a href="/paper-keyword/carboxymethilcellulose">Carboxymethilcellulose</a>, <a href="/paper-keyword/mix-torque-rheomether">Mix Torque Rheomether</a>, <a href="/paper-keyword/poly-vinyl-alcohol-2">Poly(Vinyl Alcohol)</a>, <a 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