Effect of SiO2 Content on the Microstructure and Photocatalytic Activity of TiO2 Films on Ceramic Substrate | Journal of Advanced Research in Micro and Nano Engineering

<!DOCTYPE html> <html lang="en-US" xml:lang="en-US"> <head> <meta charset="utf-8"> <meta name="viewport" content="width=device-width, initial-scale=1.0"> <title> Effect of SiO2 Content on the Microstructure and Photocatalytic Activity of TiO2 Films on Ceramic Substrate | Journal of Advanced Research in Micro and Nano Engineering </title> <link rel="icon" href="https://semarakilmu.com.my/journals/public/journals/13/favicon_en_US.ico"> <meta name="generator" content="Open Journal Systems 3.3.0.8"> <meta name="gs_meta_revision" content="1.1"/> <meta name="citation_journal_title" content="Journal of Advanced Research in Micro and Nano Engineering"/> <meta name="citation_journal_abbrev" content="J. Adv. Res. Micro Nano Eng."/> <meta name="citation_author" content="Zulkifli Mohd Rosli"/> <meta name="citation_author_institution" content="Faculty of Industrial and Manufacturing Technology and Engineering, Universiti Teknikal Malaysia Melaka, 76100 Durian Tunggal Melaka, Malaysia"/> <meta name="citation_author" content="Jariah Mohamad Juoi"/> <meta name="citation_author_institution" content="Faculty of Industrial and Manufacturing Technology and Engineering, Universiti Teknikal Malaysia Melaka, 76100 Durian Tunggal Melaka, Malaysia"/> <meta name="citation_author" content="Nur Najwa Aqilah Kamrul Zaman"/> <meta name="citation_author_institution" content="Faculty of Industrial and Manufacturing Technology and Engineering, Universiti Teknikal Malaysia Melaka, 76100 Durian Tunggal Melaka, Malaysia"/> <meta name="citation_author" content="Norhafizah Zaharuddin"/> <meta name="citation_author_institution" content="Faculty of Industrial and Manufacturing Technology and Engineering, Universiti Teknikal Malaysia Melaka, 76100 Durian Tunggal Melaka, Malaysia"/> <meta name="citation_author" content="Muharniza Azinita Musa"/> <meta name="citation_author_institution" content="Faculty of Engineering and Technology, Multimedia University, 75450 Bukit Beruang, Melaka, Malaysia"/> <meta name="citation_author" content="Toshihiro Moriga"/> <meta name="citation_author_institution" content="Department of Applied Chemistry and Engineering, Faculty of Science and Engineering, Tokushima University, Tokushima, 770-8506 Japan"/> <meta name="citation_title" content="Effect of SiO2 Content on the Microstructure and Photocatalytic Activity of TiO2 Films on Ceramic Substrate"/> <meta name="citation_language" content="en"/> <meta name="citation_date" content="2024/10/31"/> <meta name="citation_volume" content="24"/> <meta name="citation_issue" content="1"/> <meta name="citation_firstpage" content="95"/> <meta name="citation_lastpage" content="104"/> <meta name="citation_doi" content="10.37934/armne.24.1.95104"/> <meta name="citation_abstract_html_url" content="https://semarakilmu.com.my/journals/index.php/micro_nano_engineering/article/view/11230"/> <meta name="citation_keywords" xml:lang="en" content="SiO2"/> <meta name="citation_keywords" xml:lang="en" content="TiO2"/> <meta name="citation_keywords" xml:lang="en" content="photocatalytic"/> <meta name="citation_keywords" xml:lang="en" content="ceramic tiles "/> <meta name="citation_pdf_url" content="https://semarakilmu.com.my/journals/index.php/micro_nano_engineering/article/download/11230/6907"/> <link rel="schema.DC" href="http://purl.org/dc/elements/1.1/" /> <meta name="DC.Creator.PersonalName" content="Zulkifli Mohd Rosli"/> <meta name="DC.Creator.PersonalName" content="Jariah Mohamad Juoi"/> <meta name="DC.Creator.PersonalName" content="Nur Najwa Aqilah Kamrul Zaman"/> <meta name="DC.Creator.PersonalName" content="Norhafizah Zaharuddin"/> <meta name="DC.Creator.PersonalName" content="Muharniza Azinita Musa"/> <meta name="DC.Creator.PersonalName" content="Toshihiro Moriga"/> <meta name="DC.Date.created" scheme="ISO8601" content="2024-10-31"/> <meta name="DC.Date.dateSubmitted" scheme="ISO8601" content="2024-07-13"/> <meta name="DC.Date.issued" scheme="ISO8601" content="2024-10-31"/> <meta name="DC.Date.modified" scheme="ISO8601" content="2024-11-20"/> <meta name="DC.Description" xml:lang="en" content="TiO2 films has been widely used and deposited on various substrates due to its potential application as a photocatalyst. However, on unglazed or glazed ceramic tiles, TiO2 films on both substrates commonly resulted in a cracked morphology of the film. The cracks present usually lead to delamination and peel off of film from substrate and reduce its photocatalytic efficiency. Therefore, a binder needs to be added into the composition of TiO2 sol in an effort to eliminate cracking when deposited on ceramic substrates. In this work, silica (SiO2) powders were added into TiO2 sol preparation as an additive to act as a binder, in order to improve the microstructure of TiO2 films on unglazed ceramic tiles by sol-gel dip-coating. TiO2 sol with different amount of SiO2 (1, 3, 5 mol%) were utilized during film deposition. The crystalline phases were characterized by XRD, while film morphologies were analysed by SEM. The photocatalytic activity was evaluated by degradation of methylene blue under UV irradiation according to ISO 10678. The reduction of cracks formation was observed at a high amount of SiO2 (5 mol%) added and resulted in lower thickness of the films. The reduced cracks and delamination of film ensures film to bind closely to the substrate hence reducing film thickness. The highest degradation observed is at 3 mol% SiO2 where the microstructure consists of small cracks which promoted to more exposure of UV irradiation that enhanced the film’s photocatalytic activity."/> <meta name="DC.Format" scheme="IMT" content="application/pdf"/> <meta name="DC.Format" scheme="IMT" content=""/> <meta name="DC.Identifier" content="11230"/> <meta name="DC.Identifier.pageNumber" content="95-104"/> <meta name="DC.Identifier.DOI" content="10.37934/armne.24.1.95104"/> <meta name="DC.Identifier.URI" content="https://semarakilmu.com.my/journals/index.php/micro_nano_engineering/article/view/11230"/> <meta name="DC.Language" scheme="ISO639-1" content="en"/> <meta name="DC.Rights" content="Copyright (c) 2024 Journal of Advanced Research in Micro and Nano Engineering"/> <meta name="DC.Rights" content=""/> <meta name="DC.Source" content="Journal of Advanced Research in Micro and Nano Engineering"/> <meta name="DC.Source.Issue" content="1"/> <meta name="DC.Source.Volume" 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class="separator">/</span> </li> <li> <a href="https://semarakilmu.com.my/journals/index.php/micro_nano_engineering/issue/archive"> Archives </a> <span class="separator">/</span> </li> <li> <a href="https://semarakilmu.com.my/journals/index.php/micro_nano_engineering/issue/view/641"> Vol. 24 No. 1: October (2024) </a> <span class="separator">/</span> </li> <li class="current" aria-current="page"> <span aria-current="page"> Articles </span> </li> </ol> </nav> <article class="obj_article_details"> <h1 class="page_title"> Effect of SiO2 Content on the Microstructure and Photocatalytic Activity of TiO2 Films on Ceramic Substrate </h1> <div class="row"> <div class="main_entry"> <section class="item authors"> <h2 class="pkp_screen_reader">Authors</h2> <ul class="authors"> <li> <span class="name"> Zulkifli Mohd Rosli </span> <span class="affiliation"> Faculty of Industrial and Manufacturing Technology and Engineering, Universiti Teknikal Malaysia Melaka, 76100 Durian Tunggal Melaka, Malaysia </span> </li> <li> <span class="name"> Jariah Mohamad Juoi </span> <span class="affiliation"> Faculty of Industrial and Manufacturing Technology and Engineering, Universiti Teknikal Malaysia Melaka, 76100 Durian Tunggal Melaka, Malaysia </span> </li> <li> <span class="name"> Nur Najwa Aqilah Kamrul Zaman </span> <span class="affiliation"> Faculty of Industrial and Manufacturing Technology and Engineering, Universiti Teknikal Malaysia Melaka, 76100 Durian Tunggal Melaka, Malaysia </span> </li> <li> <span class="name"> Norhafizah Zaharuddin </span> <span class="affiliation"> Faculty of Industrial and Manufacturing Technology and Engineering, Universiti Teknikal Malaysia Melaka, 76100 Durian Tunggal Melaka, Malaysia </span> </li> <li> <span class="name"> Muharniza Azinita Musa </span> <span class="affiliation"> Faculty of Engineering and Technology, Multimedia University, 75450 Bukit Beruang, Melaka, Malaysia </span> </li> <li> <span class="name"> Toshihiro Moriga </span> <span class="affiliation"> Department of Applied Chemistry and Engineering, Faculty of Science and Engineering, Tokushima University, Tokushima, 770-8506 Japan </span> </li> </ul> </section> <section class="item doi"> <h2 class="label"> DOI: </h2> <span class="value"> <a href="https://doi.org/10.37934/armne.24.1.95104"> https://doi.org/10.37934/armne.24.1.95104 </a> </span> </section> <section class="item keywords"> <h2 class="label"> Keywords: </h2> <span class="value"> SiO2, TiO2, photocatalytic, ceramic tiles </span> </section> <section class="item abstract"> <h2 class="label">Abstract</h2> <p>TiO2 films has been widely used and deposited on various substrates due to its potential application as a photocatalyst. However, on unglazed or glazed ceramic tiles, TiO2 films on both substrates commonly resulted in a cracked morphology of the film. The cracks present usually lead to delamination and peel off of film from substrate and reduce its photocatalytic efficiency. Therefore, a binder needs to be added into the composition of TiO2 sol in an effort to eliminate cracking when deposited on ceramic substrates. In this work, silica (SiO2) powders were added into TiO2 sol preparation as an additive to act as a binder, in order to improve the microstructure of TiO2 films on unglazed ceramic tiles by sol-gel dip-coating. TiO2 sol with different amount of SiO2 (1, 3, 5 mol%) were utilized during film deposition. The crystalline phases were characterized by XRD, while film morphologies were analysed by SEM. The photocatalytic activity was evaluated by degradation of methylene blue under UV irradiation according to ISO 10678. The reduction of cracks formation was observed at a high amount of SiO2 (5 mol%) added and resulted in lower thickness of the films. The reduced cracks and delamination of film ensures film to bind closely to the substrate hence reducing film thickness. The highest degradation observed is at 3 mol% SiO2 where the microstructure consists of small cracks which promoted to more exposure of UV irradiation that enhanced the film’s photocatalytic activity.</p> </section> <section class="item author_bios"> <h2 class="label"> Author Biographies </h2> <section class="sub_item"> <h3 class="label"> Zulkifli Mohd Rosli, <span class="affiliation">Faculty of Industrial and Manufacturing Technology and Engineering, Universiti Teknikal Malaysia Melaka, 76100 Durian Tunggal Melaka, Malaysia</span> </h3> <div class="value"> <p>zmr@utem.edu.my</p> </div> </section> <section class="sub_item"> <h3 class="label"> Jariah Mohamad Juoi, <span class="affiliation">Faculty of Industrial and Manufacturing Technology and Engineering, Universiti Teknikal Malaysia Melaka, 76100 Durian Tunggal Melaka, Malaysia</span> </h3> <div class="value"> <p>jariah@utem.edu.my</p> </div> </section> <section class="sub_item"> <h3 class="label"> Nur Najwa Aqilah Kamrul Zaman, <span class="affiliation">Faculty of Industrial and Manufacturing Technology and Engineering, Universiti Teknikal Malaysia Melaka, 76100 Durian Tunggal Melaka, Malaysia</span> </h3> <div class="value"> <p>wawaaqilah@gmail.com</p> </div> </section> <section class="sub_item"> <h3 class="label"> Norhafizah Zaharuddin, <span class="affiliation">Faculty of Industrial and Manufacturing Technology and Engineering, Universiti Teknikal Malaysia Melaka, 76100 Durian Tunggal Melaka, Malaysia</span> </h3> <div class="value"> <p>hafizah909@gmail.com</p> </div> </section> <section class="sub_item"> <h3 class="label"> Muharniza Azinita Musa, <span class="affiliation">Faculty of Engineering and Technology, Multimedia University, 75450 Bukit Beruang, Melaka, Malaysia</span> </h3> <div class="value"> <p>azinita.musa@mmu.edu.my</p> </div> </section> <section class="sub_item"> <h3 class="label"> Toshihiro Moriga, <span class="affiliation">Department of Applied Chemistry and Engineering, Faculty of Science and Engineering, Tokushima University, Tokushima, 770-8506 Japan</span> </h3> <div class="value"> <p>moriga@tokushima-u.ac.jp</p> </div> </section> </section> </div> <div class="entry_details"> <div class="item cover_image"> <div class="sub_item"> <img src="https://semarakilmu.com.my/journals/public/journals/13/submission_11230_11230_coverImage_en_US.jpg" alt="" > </div> </div> <div class="item galleys"> <h2 class="pkp_screen_reader"> Downloads </h2> <ul class="value galleys_links"> <li> <a class="obj_galley_link pdf" href="https://semarakilmu.com.my/journals/index.php/micro_nano_engineering/article/view/11230/6907"> PDF </a> </li> <li> <a class="obj_galley_link file" href="https://semarakilmu.com.my/journals/index.php/micro_nano_engineering/article/view/11230/7546"> GOOGLE SCHOLAR </a> </li> </ul> </div> <div class="item published"> <section class="sub_item"> <h2 class="label"> Published </h2> <div class="value"> <span>2024-10-31</span> </div> </section> </div> <div class="item citation"> <section class="sub_item citation_display"> <h2 class="label"> How to Cite </h2> <div class="value"> <div id="citationOutput" role="region" aria-live="polite"> <div class="csl-bib-body"> <div class="csl-entry">Mohd Rosli, Z., Mohamad Juoi, J., Kamrul Zaman, N. 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Effect of SiO2 Content on the Microstructure and Photocatalytic Activity of TiO2 Films on Ceramic Substrate. <i>Journal of Advanced Research in Micro and Nano Engineering</i>, <i>24</i>(1), 95–104. https://doi.org/10.37934/armne.24.1.95104</div> </div> </div> <div class="citation_formats"> <button class="cmp_button citation_formats_button" aria-controls="cslCitationFormats" aria-expanded="false" data-csl-dropdown="true"> More Citation Formats </button> <div id="cslCitationFormats" class="citation_formats_list" aria-hidden="true"> <ul class="citation_formats_styles"> <li> <a aria-controls="citationOutput" href="https://semarakilmu.com.my/journals/index.php/micro_nano_engineering/citationstylelanguage/get/acm-sig-proceedings?submissionId=11230&publicationId=11230" data-load-citation data-json-href="https://semarakilmu.com.my/journals/index.php/micro_nano_engineering/citationstylelanguage/get/acm-sig-proceedings?submissionId=11230&publicationId=11230&return=json" > ACM </a> </li> <li> <a 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Effect of SiO2 Content on the Microstructure and Photocatalytic Activity of TiO2 Films on Ceramic Substrate | Journal of Advanced Research in Micro and Nano Engineering