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{"work":{"id":81671508,"created_at":"2022-06-16T23:38:47.551-07:00","from_world_paper_id":208581437,"updated_at":"2024-11-08T06:21:02.158-08:00","_data":{"publisher":"Elsevier BV","publication_date":"2019,,","publication_name":"Trends in Food Science \u0026 Technology"},"document_type":"paper","pre_hit_view_count_baseline":null,"quality":"high","language":"en","title":"A review on nuclear Overhauser enhancement (NOE) and rotating-frame Overhauser effect (ROE) NMR techniques in food science: basic principles and applications","broadcastable":true,"draft":null,"has_indexable_attachment":true,"indexable":true}}["work"]; window.loswp.workCoauthors = [20149928]; window.loswp.locale = "en"; window.loswp.countryCode = "SG"; window.loswp.cwvAbTestBucket = ""; window.loswp.designVariant = "ds_vanilla"; window.loswp.fullPageMobileSutdModalVariant = "full_page_mobile_sutd_modal"; window.loswp.useOptimizedScribd4genScript = false; window.loswp.appleClientId = 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data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Diverse food-based applications of nuclear magnetic resonance (NMR) technology","attachmentId":92924511,"attachmentType":"pdf","work_url":"https://www.academia.edu/89055026/Diverse_food_based_applications_of_nuclear_magnetic_resonance_NMR_technology","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/89055026/Diverse_food_based_applications_of_nuclear_magnetic_resonance_NMR_technology"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="1" data-entity-id="49460188" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/49460188/31P_NMR_spectroscopy_in_food_analysis">31P NMR spectroscopy in food analysis</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="24286180" href="https://crete.academia.edu/PDais">Photis Dais</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Prog Nucl Magn Reson Spectros, 2009</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"31P NMR spectroscopy in food analysis","attachmentId":67806637,"attachmentType":"pdf","work_url":"https://www.academia.edu/49460188/31P_NMR_spectroscopy_in_food_analysis","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/49460188/31P_NMR_spectroscopy_in_food_analysis"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="2" data-entity-id="30717215" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/30717215/A_discussion_about_the_potentials_and_pitfalls_of_quantitative_nuclear_magnetic_resonance_qNMR_spectroscopy_in_food_science_and_beyond">A discussion about the potentials and pitfalls of quantitative nuclear magnetic resonance (qNMR) spectroscopy in food science and beyond</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="7502613" href="https://cvua-karlsruhe.academia.edu/Lachenmeier">Dirk Lachenmeier</a></div><p class="ds-related-work--abstract ds2-5-body-sm">During the XIII International Conference on the Applications of Magnetic Resonance in Food Science, which was held in Karlsruhe, Germany, from 7th to 10th of June 2016, a discussion session entitled " Quantitative nuclear magnetic resonance (qNMR) " was organized. The conference participants had the opportunity to submit written questions as well as to ask ad-hoc questions during the session, which were to be answered by a panel of qNMR experts from several application fields. This article provides an edited and referenced transcript of the session. The major topics were centred on instrumental requirements for qNMR, and the participants were in agreement that modern digital NMR spectrometers guarantee a long-term stability of measurements and calibrations, sometimes over several years. However, the panel also agreed that method validation is an absolute necessity in qNMR as in every other field of quantitative analytical chemistry. Validation strategies may depend on the purpose of the method and vary between multi-component analyses of foods and beverages, compared to single target assays e.g. in verification of reference standards. Approaches to establish limits of detection and to ensure the required method accuracy were suggested. The discussion was closed with a general agreement of the experts that qNMR in food science will gain a wider application range in the future. The necessity to abolish regulatory hindrances – including the approval of using qNMR in reference methods – was stressed.</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"A discussion about the potentials and pitfalls of quantitative nuclear magnetic resonance (qNMR) spectroscopy in food science and beyond","attachmentId":51165689,"attachmentType":"pdf","work_url":"https://www.academia.edu/30717215/A_discussion_about_the_potentials_and_pitfalls_of_quantitative_nuclear_magnetic_resonance_qNMR_spectroscopy_in_food_science_and_beyond","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/30717215/A_discussion_about_the_potentials_and_pitfalls_of_quantitative_nuclear_magnetic_resonance_qNMR_spectroscopy_in_food_science_and_beyond"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="3" data-entity-id="10054077" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/10054077/Chemometric_methods_in_NMR_spectroscopic_analysis_of_food_products">Chemometric methods in NMR spectroscopic analysis of food products</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="7502613" href="https://cvua-karlsruhe.academia.edu/Lachenmeier">Dirk Lachenmeier</a></div><p class="ds-related-work--abstract ds2-5-body-sm">The main achievements of high-resolution NMR spectroscopy in combination with different chemometric methods in the analysis of food products in the last 40 years are reviewed. The essence of chemometric methods used for the analysis and interpretation of NMR spectra is briefly described. Sample preparation for NMR-spectroscopic analysis is characterized. Methods for the mathematical treatment of NMR spectra (smoothing, Fourier transformation, bucketing, normalization, and selection of spectral ranges) are considered. Currently available methods for the suppression of the signals of macrocomponents, including those for the simultaneous suppression of several signals, are described. 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