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Effect of Microstructure on the Corrosion Behavior of TiN Coatings | Scientific.Net
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Li; citation_author=S. Guruvenket; citation_author=S. Hassani; citation_author=E. Bousser; citation_author=M. Azzi; citation_author=J.A. Szpunar; citation_author=J.E. Klemberg-Sapieha; citation_volume=519; citation_issue=10; citation_publication_date=2011/3; citation_pages=3128-3134; citation_doi=10.1016/j.tsf.2010.12.020" /> <meta name="citation_reference" content="citation_title=Relationship between the mechanical properties and the microstructure of nanocomposite TiN/SiN1.3 coatings prepared by low temperature plasma enhanced chemical vapor deposition; citation_author=P Jedrzejowski; citation_author=J.E Klemberg-Sapieha; citation_author=L Martinu; citation_volume=426; citation_issue=1-2; citation_publication_date=2003/2; citation_pages=150-159; citation_doi=10.1016/s0040-6090(03)00028-2" /> <meta name="citation_reference" content="citation_title=Design of hard coating architecture for the optimization of erosion resistance; citation_author=S. Hassani; citation_author=J.E. Klemberg-Sapieha; citation_author=M. Bielawski; citation_author=W. Beres; citation_author=L. Martinu; citation_author=M. Balazinski; citation_volume=265; citation_issue=5-6; citation_publication_date=2008/8; citation_pages=879-887; citation_doi=10.1016/j.wear.2008.01.021" /> <meta name="citation_reference" content="P. Jedrzejowski, J.E. Klemberg-Sapieha, L. Martinu, Surf. Coat. Technol., 188-189, 2004, 371-375" /> <meta name="citation_reference" content="citation_title=Quaternary hard nanocomposite TiCxNy/SiCN coatings prepared by plasma enhanced chemical vapor deposition; citation_author=P. Jedrzejowski; citation_author=J.E. Klemberg-Sapieha; citation_author=L. 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Buchanan, "Fundamental of Electrochemical Corrosion", ASM International (2000)." /> <meta name="citation_reference" content="citation_title=Corrosion and mechanical properties of duplex-treated 301 stainless steel; citation_author=M. Azzi; citation_author=M. Benkahoul; citation_author=J.E. Klemberg-Sapieha; citation_author=L. Martinu; citation_volume=205; citation_issue=5; citation_publication_date=2010/11; citation_pages=1557-1563; citation_doi=10.1016/j.surfcoat.2010.08.155" /> <meta name="citation_reference" content="K.W. Chen, J.F. Lin, Thin Solid Films, (517), 2009, 4916-4920." /> <meta name="citation_reference" content="citation_title=Corrosion performance and mechanical stability of 316L/DLC coating system: Role of interlayers; citation_author=M. Azzi; citation_author=P. Amirault; citation_author=M. Paquette; citation_author=J.E. Klemberg-Sapieha; citation_author=L. Martinu; citation_volume=204; citation_issue=24; citation_publication_date=2010/9; citation_pages=3986-3994; citation_doi=10.1016/j.surfcoat.2010.05.004" /> <meta name="citation_reference" content="M. Azzi, M. Paquette, J.E. Klemberg-Sapieha, L. Martinu, Proceedings of the 52th Aannual Technical CSVC conference of the SVC, 2009, Santa-Clara, USA." /> <meta name="citation_reference" content="citation_title=Enhancement of corrosion resistance of a biomedical grade 316LVM stainless steel by potentiodynamic cyclic polarization; citation_author=Ziad Bou-Saleh; citation_author=Abdullah Shahryari; citation_author=Sasha Omanovic; citation_volume=515; citation_issue=11; citation_publication_date=2007/4; citation_pages=4727-4737; citation_doi=10.1016/j.tsf.2006.11.054" /> <meta name="citation_reference" content="I. Gurappa, Mater. Charact. (49), 2002, 73." /> <meta name="person" content="Marwan Azzi, Jolanta Eva Klemberg Sapieha" /> <meta name="description" content="In this paper, the corrosion properties of AISI 301 stainless steel (SS) coated with 1-micron thick titanium nitride (TiN) hard coatings is investigated. TiN was deposited by pulsed magnetron sputtering resulting in different microstructure ranging from agglomerated crystallites to homogeneous film. Microstructure of the coatings was characterized by scanning electron microscopy (SEM), x-ray diffraction (XRD), and energy dispersive spectroscopy (EDS). Resistance to general and localized corrosion was evaluated by potentiodynamic polarization in NaCl 1% solution. It has been shown that the existence of columnar structure in the TiN film reduces significantly the resistance to localized corrosion due to infiltration of liquid through paths at the grain boundaries. Furthermore, by comparing the polarization curves of TiN coatings deposited on SS and glass, it was shown that the electrochemical response of TiN-coated SS at low potentials is the result of electrochemical activity at the coating/electrolyte interface whereas at high potentials the increase in the current is the result of pits generated at the substrate/electrolyte interface at defects/pores within the coating." /> <meta name="keywords" content="Corrosion, Electrochemical Polarization, Sputtering, SS301, Titanium Nitride" /> <meta name="copyright" content="2012 Trans Tech Publications Ltd. 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on the Corrosion Behavior of TiN Coatings</h1> </div> <div class="paper-statistics"> <div class="loading"> <i class="inline-icon download-and-visitor-statistics-icon"></i> <span class="normal-text" id="paperDownloadsAndVisitorsCount"></span> </div> </div> <div class="clearfix"></div> <div class="page-paper-title"> <div class="preview-block"> <img alt="Article Preview" width="128" height="180" src="/AMR.415-417.1911/thumbnail.gif"> <div id="preview-button" data-url-preview-log="/Paper/PreviewImageLog?paperId=159709"> <i class="inline-icon preview-icon"></i> </div> <!--Modal window for article preview--> <div id="paper-preview-modal" class="modal fade"> <div class="modal-dialog" role="document"> <div class="popup-page-name underline-begin"> <div class="page-name-block-text">Article Preview</div> </div> <img alt="Article Preview" class="preview-image lazyload" data-src="/AMR.415-417.1911/preview.gif"> <a data-dismiss="modal" title="Close" class="inline-icon close-icon"></a> </div> </div> <!--End modal--> </div> <div class="abstract-block-description"> <h3 class="page-paper-first-header">Abstract:</h3> <p class="normal-text"> In this paper, the corrosion properties of AISI 301 stainless steel (SS) coated with 1-micron thick titanium nitride (TiN) hard coatings is investigated. TiN was deposited by pulsed magnetron sputtering resulting in different microstructure ranging from agglomerated crystallites to homogeneous film. Microstructure of the coatings was characterized by scanning electron microscopy (SEM), x-ray diffraction (XRD), and energy dispersive spectroscopy (EDS). Resistance to general and localized corrosion was evaluated by potentiodynamic polarization in NaCl 1% solution. It has been shown that the existence of columnar structure in the TiN film reduces significantly the resistance to localized corrosion due to infiltration of liquid through paths at the grain boundaries. Furthermore, by comparing the polarization curves of TiN coatings deposited on SS and glass, it was shown that the electrochemical response of TiN-coated SS at low potentials is the result of electrochemical activity at the coating/electrolyte interface whereas at high potentials the increase in the current is the result of pits generated at the substrate/electrolyte interface at defects/pores within the coating. </p> </div> <div class="paper-access-buttons col-xs-12"> <div class="row"> <div class="sa-button-wrap"> <a id="sa-button" class="wayfinder-login d-flex sa-button" href="javascript:;"> <div class="sa-button-logo-wrap"> <i class="inline-icon sa-white"></i> </div> <div class="d-flex justify-content-center align-items-center sa-button-text text-truncate"> <div class="sa-button-text-primary text-truncate">Access through your institution</div> </div> </a> </div> <div class="title-button-pdf"> <button id="readPaperButton" 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class="info-row-name normal-text-gray col-md-2 col-sm-3 col-xs-4"> <div class="row"> <p>Authors:</p> </div> </div> <div class="info-row-content semibold-middle-text col-md-10 col-sm-9 col-xs-8"> <div class="row"> <a href="/author-papers/marwan-azzi-1">Marwan Azzi</a>, <a href="/author-papers/jolanta-eva-klemberg-sapieha">Jolanta Eva Klemberg Sapieha</a> </div> </div> </div> </div> <div class="papers-block-info col-lg-12"> <div class="row"> <div class="info-row-name normal-text-gray col-md-2 col-sm-3 col-xs-4"> <div class="row"> <p>Keywords:</p> </div> </div> <div class="info-row-content semibold-middle-text col-md-10 col-sm-9 col-xs-8"> <div class="row"> <a href="/paper-keyword/corrosion">Corrosion</a>, <a href="/paper-keyword/electrochemical-polarization">Electrochemical Polarization</a>, <a href="/paper-keyword/sputtering">Sputtering</a>, <a href="/paper-keyword/ss301">SS301</a>, <a href="/paper-keyword/titanium-nitride">Titanium Nitride</a> </div> </div> </div> </div> <div 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