Effect of Heat Treatment on Mechanical Properties and Corrosion Response of HVOF Sprayed High Entropy Alloy Coatings

<!DOCTYPE html> <html lang="iv" dir="ltr"> <head> <meta name="format-detection" content="telephone=no"> <meta name="viewport" content="width=device-width, initial-scale=1.0" /> <meta charset="utf-8"> <meta http-equiv="X-UA-Compatible" content="IE=edge"> <link rel="canonical" href="https://www.scientific.net/KEM.982.3" /> <meta property="og:title" content="Effect of Heat Treatment on Mechanical Properties and Corrosion Response of HVOF Sprayed High Entropy Alloy Coatings | Scientific.Net" /> <meta property="og:type" content="website" /> <meta property="og:url" content="https://www.scientific.net/KEM.982.3" /> <meta property="og:image" content="/Content/app/scinet5/images/metadata_logo.png" /> <meta property="og:image:type" content="image/png" /> <meta property="og:image:width" content="261" /> <meta property="og:image:height" content="260" /> <meta property="og:image:alt" content="Scientific.Net Logo" /> <meta name="citation_language" content="en" /> <meta name="citation_publisher" content="Trans Tech Publications Ltd" /> <meta name="citation_title" content="Effect of Heat Treatment on Mechanical Properties and Corrosion Response of HVOF Sprayed High Entropy Alloy Coatings" /> <meta name="citation_publication_date" content="2024" /> <meta name="citation_online_date" content="2024/07/03" /> <meta name="citation_journal_title" content="Key Engineering Materials" /> <meta name="citation_issn" content="1662-9795" /> <meta name="citation_volume" content="982" /> <meta name="citation_firstpage" content="3" /> <meta name="citation_lastpage" content="8" /> <meta name="citation_pdf_url" content="https://www.scientific.net/KEM.982.3.pdf" /> <meta name="citation_abstract_html_url" content="https://www.scientific.net/KEM.982.3" /> <meta name="citation_keywords" content="Corrosion;High Entropy Alloys;HVOF Process;Microstructure" /> <meta name="citation_doi" content="10.4028/p-UVGG3f" /> <meta name="citation_author" content="N.V. 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Munitz; citation_author=S. Salhov; citation_author=S. Hayun; citation_author=N. Frage; citation_volume=683; citation_publication_date=2016/10; citation_pages=221-230; citation_doi=10.1016/j.jallcom.2016.05.034" /> <meta name="citation_reference" content="citation_title=Microstructural evolution and effect of heat treatment on the precipitation and mechanical behavior of Al0.7CoCrFeNi alloy; citation_author=Rahul John; citation_author=M. Nagini; citation_author=U. Govind; citation_author=S.R.K. Malladi; citation_author=B.S. Murty; citation_author=Daniel Fabijanic; citation_volume=904; citation_publication_date=2022/5; citation_pages=164105; citation_doi=10.1016/j.jallcom.2022.164105" /> <meta name="person" content="N.V. Abhijith, Deepak Kumar, Karun Rawat" /> <meta name="description" content="Surface and sub-surface related degradation of steels can be minimized using suitable surface coatings. High entropy alloys (HEA) are prominent and emerging materials among many coating materials. The current study investigates the effect of heat treatment of HEA coating on mechanical, metallurgical, and corrosion properties. The HEA coatings on SS304 steel were deposited using a High-Velocity Oxy-Fuel (HVOF) thermal spray process. The developed coatings were furnace heat treated at 700 °C, 900 °C, and 1100 °C, respectively, and their performance was benchmarked with the as-sprayed coatings. The metallurgical, mechanical, and microstructural analyses were performed using X-ray diffraction (XRD), Nanoindentation, Scratch test, and Field Emission Scanning Electron Microscope (FESEM) techniques. The corrosion response of the as sprayed and heat-treated coatings were recorded using a Potentiostat. The results indicated that as-sprayed coatings consisted of a single-phase BCC solid solution; however, the single-phase changed to a dual dual-phase system after heat treatment (BCC+FCC). The 900 °C heat-treated HEA coating exhibited superior mechanical and corrosion properties. But those characteristics started diminishing when the heat treatment temperature exceeded 900 °C. The introduction of the new FCC phase softened the coating, thereby leading to the evolution of microcracks in the coating. These micro-cracks acted as channels for electrolyte diffusion and further corroded the coatings. The current study surmised that HVOF-sprayed HEA coating should not be heat treated at above 900 °C." /> <meta name="keywords" content="Corrosion, High Entropy Alloys, HVOF Process, Microstructure" /> <meta name="copyright" content="2024 Trans Tech Publications Ltd. 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on Mechanical Properties and Corrosion Response of HVOF Sprayed High Entropy Alloy Coatings</h1> </div> <div class="paper-statistics"> <div class="loading"> <i class="inline-icon download-and-visitor-statistics-icon"></i> <span class="normal-text" id="paperDownloadsAndVisitorsCount"></span> </div> </div> <div class="clearfix"></div> <div class="page-paper-title"> <div class="preview-block"> <img alt="Article Preview" width="128" height="180" src="/KEM.982.3/thumbnail.gif"> <div id="preview-button" data-url-preview-log="/Paper/PreviewImageLog?paperId=611231"> <i class="inline-icon preview-icon"></i> </div>  <div id="paper-preview-modal" class="modal fade"> <div class="modal-dialog" role="document"> <div class="popup-page-name underline-begin"> <div class="page-name-block-text">Article Preview</div> </div> <img alt="Article Preview" class="preview-image lazyload" data-src="/KEM.982.3/preview.gif"> <a data-dismiss="modal" title="Close" class="inline-icon close-icon"></a> </div> </div>  </div> <div class="abstract-block-description"> <h3 class="page-paper-first-header">Abstract:</h3> <p class="normal-text"> Surface and sub-surface related degradation of steels can be minimized using suitable surface coatings. High entropy alloys (HEA) are prominent and emerging materials among many coating materials. The current study investigates the effect of heat treatment of HEA coating on mechanical, metallurgical, and corrosion properties. The HEA coatings on SS304 steel were deposited using a High-Velocity Oxy-Fuel (HVOF) thermal spray process. The developed coatings were furnace heat treated at 700 掳C, 900 掳C, and 1100 掳C, respectively, and their performance was benchmarked with the as-sprayed coatings. The metallurgical, mechanical, and microstructural analyses were performed using X-ray diffraction (XRD), Nanoindentation, Scratch test, and Field Emission Scanning Electron Microscope (FESEM) techniques. The corrosion response of the as sprayed and heat-treated coatings were recorded using a Potentiostat. The results indicated that as-sprayed coatings consisted of a single-phase BCC solid solution; however, the single-phase changed to a dual dual-phase system after heat treatment (BCC+FCC). The 900 掳C heat-treated HEA coating exhibited superior mechanical and corrosion properties. But those characteristics started diminishing when the heat treatment temperature exceeded 900 掳C. The introduction of the new FCC phase softened the coating, thereby leading to the evolution of microcracks in the coating. These micro-cracks acted as channels for electrolyte diffusion and further corroded the coatings. The current study surmised that HVOF-sprayed HEA coating should not be heat treated at above 900 掳C. </p> </div> <div class="paper-access-buttons col-xs-12"> <div class="row"> <div class="sa-button-wrap"> <a id="sa-button" class="wayfinder-login d-flex sa-button" href="javascript:;"> <div class="sa-button-logo-wrap"> <i class="inline-icon sa-white"></i> </div> <div class="d-flex justify-content-center align-items-center sa-button-text text-truncate"> <div class="sa-button-text-primary text-truncate">Access through your institution</div> </div> </a> </div> <div class="title-button-pdf"> <button id="readPaperButton" data-url-read-paper-log="/Paper/ReadThePaperLog?paperId=611231" class="button button-160"> <span class="inline-element">Read The Paper</span> </button> </div> </div> <div class="row"> </div> </div> <div class="clearfix"></div> <div class="connected-title-container"> <div class="connected-title-text semibold-middle-text">You might also be interested in these eBooks</div> <div 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