Effects of Hydrothermal Treatment on Properties of Titanium Nitride Coating for Dental Implants

<!DOCTYPE html> <html lang="en" dir="ltr"> <head> <meta name="format-detection" content="telephone=no"> <meta name="viewport" content="width=device-width, initial-scale=1.0" /> <meta charset="utf-8"> <meta http-equiv="X-UA-Compatible" content="IE=edge"> <link rel="canonical" href="https://www.scientific.net/KEM.529-530.247" /> <meta property="og:title" content="Effects of Hydrothermal Treatment on Properties of Titanium Nitride Coating for Dental Implants | Scientific.Net" /> <meta property="og:type" content="website" /> <meta property="og:url" content="https://www.scientific.net/KEM.529-530.247" /> <meta property="og:image" content="/Content/app/scinet5/images/metadata_logo.png" /> <meta property="og:image:type" content="image/png" /> <meta property="og:image:width" content="261" /> <meta property="og:image:height" content="260" /> <meta property="og:image:alt" content="Scientific.Net Logo" /> <meta name="citation_language" content="en" /> <meta name="citation_publisher" content="Trans Tech Publications Ltd" /> <meta name="citation_title" content="Effects of Hydrothermal Treatment on Properties of Titanium Nitride Coating for Dental Implants" /> <meta name="citation_publication_date" content="2013" /> <meta name="citation_online_date" content="2012/11/29" /> <meta name="citation_journal_title" content="Key Engineering Materials" /> <meta name="citation_issn" content="1662-9795" /> <meta name="citation_volume" content="529-530" /> <meta name="citation_firstpage" content="247" /> <meta name="citation_lastpage" content="250" /> <meta name="citation_pdf_url" content="https://www.scientific.net/KEM.529-530.247.pdf" /> <meta name="citation_abstract_html_url" content="https://www.scientific.net/KEM.529-530.247" /> <meta name="citation_keywords" content="Calcium;Hydrothermal Treatment;Osteoconductivity;Partial Oxidation;Titanium Nitride" /> <meta name="citation_doi" content="10.4028/www.scientific.net/KEM.529-530.247" /> <meta name="citation_author" content="Xing Ling Shi" /> <meta name="citation_author" content="Kanji Tsuru" /> <meta name="citation_author" content="Giichiro Kawachi" /> <meta name="citation_author" content="Ishikawa Kunio" /> <meta name="citation_reference" content="citation_title=Surface treatments of titanium dental implants for rapid osseointegration; citation_author=L. Le Guéhennec; citation_author=A. Soueidan; citation_author=P. Layrolle; citation_author=Y. Amouriq; citation_volume=23; citation_issue=7; citation_publication_date=2007/7; citation_pages=844-854; citation_doi=10.1016/j.dental.2006.06.025" /> <meta name="citation_reference" content="R. Mengel, C. Meer, L. Flores-de-Jacoby, The treatment of uncoated and titanium nitride-coated abutments with different instruments, Int. J. Oral Maxillofac. Implants 19 (2004) 232-238." /> <meta name="citation_reference" content="citation_title=Plaque formation on surface modified dental implants; citation_author=Birte Größner-Schreiber; citation_author=Michael Griepentrog; citation_author=Ingrun Haustein; citation_author=Wolf-Dieter Müller; citation_author=Helga Briedigkeit; citation_author=Ulf Berthold Göbel; citation_author=Klaus-Peter Lange; citation_volume=12; citation_issue=6; citation_publication_date=2008/7/7; citation_pages=543-551; citation_doi=10.1034/j.1600-0501.2001.120601.x" /> <meta name="citation_reference" content="citation_title=The peri-implant hard and soft tissues at different implant systems. A comparative study in the dog.; citation_author=I. Abrahamsson; citation_author=T. Berglundh; citation_author=J. Wennström; citation_author=J. Lindhe; citation_volume=7; citation_issue=3; citation_publication_date=2002/6/25; citation_pages=212-219; citation_doi=10.1034/j.1600-0501.1996.070303.x" /> <meta name="citation_reference" content="citation_title=Osseointegration of Ti6Al4V alloy implants coated with titanium nitride by a new method; citation_author=G. Sovak; citation_author=A. Weiss; citation_author=I. Gotman; citation_volume=82-B; citation_issue=2; citation_publication_date=2000/3; citation_pages=290-296; citation_doi=10.1302/0301-620x.82b2.0820290" /> <meta name="citation_reference" content="citation_title=Corrigendum to “A comparative study of titanium nitride (TiN), titanium oxy nitride (TiON) and titanium aluminum nitride (TiAlN), as surface coatings for bio implants” [Surf. Coat. Technol. 205 (2011) 5014–5020]; citation_author=B. Subramanian; citation_author=C.V. Muraleedharan; citation_author=R. Ananthakumar; citation_author=M. Jayachandran; citation_volume=455; citation_publication_date=2023/2; citation_pages=129224; citation_doi=10.1016/j.surfcoat.2022.129224" /> <meta name="citation_reference" content="citation_title=Tissue-response to calcium-bonded titanium surface; citation_author=Lei Zhang; citation_author=Yasunori Ayukawa; citation_author=Racquel Z. LeGeros; citation_author=Shigeki Matsuya; citation_author=Kiyoshi Koyano; citation_author=Kunio Ishikawa; citation_volume=95A; citation_issue=1; citation_publication_date=2010/8/19; citation_pages=33-39; citation_doi=10.1002/jbm.a.32763" /> <meta name="citation_reference" content="citation_title=Surface modification of titanium by hydrothermal treatment in Mg-containing solution and early osteoblast responses; citation_author=Xingling Shi; citation_author=Masaharu Nakagawa; citation_author=Giichiro Kawachi; citation_author=Lingli Xu; citation_author=Kunio Ishikawa; citation_volume=23; citation_issue=5; citation_publication_date=2012/3/4; citation_pages=1281-1290; citation_doi=10.1007/s10856-012-4596-4" /> <meta name="citation_reference" content="citation_title=A nitrogen doped TiO2 layer on Ti metal for the enhanced formation of apatite; citation_author=Masami Hashimoto; citation_author=Kazumi Kashiwagi; citation_author=Satoshi Kitaoka; citation_volume=22; citation_issue=9; citation_publication_date=2011/7/16; citation_pages=2013-2018; citation_doi=10.1007/s10856-011-4389-1" /> <meta name="citation_reference" content="citation_title=Bioactivity of TiN-coated titanium implants; citation_author=S Piscanec; citation_volume=52; citation_issue=5; citation_publication_date=2004/3/8; citation_pages=1237-1245; citation_doi=10.1016/j.actamat.2003.11.020" /> <meta name="citation_reference" content="citation_title=Effect of Titanium Surface Calcium and Magnesium on Adhesive Activity of Epithelial-Like Cells and Fibroblasts; citation_author=Hideyuki Okawachi; citation_author=Yasunori Ayukawa; citation_author=Ikiru Atsuta; citation_author=Akihiro Furuhashi; citation_author=Mami Sakaguchi; citation_author=Koichi Yamane; citation_author=Kiyoshi Koyano; citation_volume=7; citation_issue=1; citation_publication_date=2012/12; citation_pages=27; citation_doi=10.1007/s13758-012-0027-9" /> <meta name="person" content="Xing Ling Shi, Kanji Tsuru, Giichiro Kawachi, Ishikawa Kunio" /> <meta name="description" content="To improve surface hardness of dental implant made of pure titanium (Ti), titanium nitride (TiN) coating was introduced. However, studies revealed that TiN only showed osseointegration similar or inferior to that of Ti. Therefore it is necessary to improve the biocompatibility of TiN for dental implant coating. In the present study, TiN coating was prepared on pure Ti substrates and hydrothermal treatment was conducted to modify its surface properties. It was found that, TiN surface was partially oxidized after treatment and calcium (Ca) was successfully combined onto its surface. Surface morphology, roughness and hardness were not affected after treatments below 140°C and wettability was obviously improved." /> <meta name="keywords" content="Calcium, Hydrothermal Treatment, Osteoconductivity, Partial Oxidation, Titanium Nitride" /> <meta name="copyright" content="2013 Trans Tech Publications Ltd. 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class="paper-statistics"> <div class="loading"> <i class="inline-icon download-and-visitor-statistics-icon"></i> <span class="normal-text" id="paperDownloadsAndVisitorsCount"></span> </div> </div> <div class="clearfix"></div> <div class="page-paper-title"> <div class="preview-block"> <img alt="Article Preview" width="128" height="180" src="/KEM.529-530.247/thumbnail.gif"> <div id="preview-button" data-url-preview-log="/Paper/PreviewImageLog?paperId=225572"> <i class="inline-icon preview-icon"></i> </div>  <div id="paper-preview-modal" class="modal fade"> <div class="modal-dialog" role="document"> <div class="popup-page-name underline-begin"> <div class="page-name-block-text">Article Preview</div> </div> <img alt="Article Preview" class="preview-image lazyload" data-src="/KEM.529-530.247/preview.gif"> <a data-dismiss="modal" title="Close" class="inline-icon close-icon"></a> </div> </div>  </div> <div class="abstract-block-description"> <h3 class="page-paper-first-header">Abstract:</h3> <p class="normal-text"> To improve surface hardness of dental implant made of pure titanium (Ti), titanium nitride (TiN) coating was introduced. However, studies revealed that TiN only showed osseointegration similar or inferior to that of Ti. Therefore it is necessary to improve the biocompatibility of TiN for dental implant coating. In the present study, TiN coating was prepared on pure Ti substrates and hydrothermal treatment was conducted to modify its surface properties. It was found that, TiN surface was partially oxidized after treatment and calcium (Ca) was successfully combined onto its surface. Surface morphology, roughness and hardness were not affected after treatments below 140°C and wettability was obviously improved. </p> </div> <div class="paper-access-buttons col-xs-12"> <div class="row"> <div class="sa-button-wrap"> <a id="sa-button" class="wayfinder-login d-flex sa-button" href="javascript:;"> <div class="sa-button-logo-wrap"> <i class="inline-icon sa-white"></i> </div> <div class="d-flex justify-content-center align-items-center sa-button-text text-truncate"> <div class="sa-button-text-primary text-truncate">Access through your institution</div> </div> </a> </div> <div class="title-button-pdf"> <button id="readPaperButton" data-url-read-paper-log="/Paper/ReadThePaperLog?paperId=225572" class="button button-160"> <span class="inline-element">Read The Paper</span> </button> </div> </div> <div class="row"> </div> </div> <div class="clearfix"></div> <div class="connected-title-container"> <div class="connected-title-text semibold-middle-text">You might also be 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Kunio</a> </div> </div> </div> </div> <div class="papers-block-info col-lg-12"> <div class="row"> <div class="info-row-name normal-text-gray col-md-2 col-sm-3 col-xs-4"> <div class="row"> <p>Keywords:</p> </div> </div> <div class="info-row-content semibold-middle-text col-md-10 col-sm-9 col-xs-8"> <div class="row"> <a href="/paper-keyword/calcium">Calcium</a>, <a href="/paper-keyword/hydrothermal-treatment">Hydrothermal Treatment</a>, <a href="/paper-keyword/osteoconductivity">Osteoconductivity</a>, <a href="/paper-keyword/partial-oxidation">Partial Oxidation</a>, <a href="/paper-keyword/titanium-nitride">Titanium Nitride</a> </div> </div> </div> </div> <div class="papers-block-info col-lg-12"> <div class="row"> <div class="info-row-name normal-text-gray col-md-2 col-sm-3 col-xs-4"> <div class="row"> <p>Export:</p> </div> </div> <div class="info-row-content semibold-middle-text col-md-10 col-sm-9 col-xs-8"> <div class="row"> <a href="/KEM.529-530.247.ris">RIS</a>, <a 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