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Characterization of Nb Coating in HIE-ISOLDE QWR Superconducting Accelerating Cavities by means of SEM-FIB and TEM - CERN Document Server
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The Nb film thickness, morphology, purity and quality are critical parameters for RF performances of the cavity. They have been investigated in a detailed material study. The coating structure at different positions along a test cavity was observed by cross-section imaging using SEM-FIB instrument. The samples from the top of the cavity showed presence of unexpected porosities, whose volume was investigated using FIB tomography. TEM lamella was prepared for two samples (top part and inner conductor of the cavity) to study in detail the grain orientation in the coating, its chemical composition and structure. The 14-layer structure in thick coating was indeed evidenced by the TEM analysis. Chemical mapping revealed the presence of a few nm in size copper precipitates close to the Nb/Cu interface and a passivating oxide layer of 10 nm thickness on top of the coating and around porosities. However no impurities or interface layer along the coating profile were present. 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var affiliation = $(this).data('affiliation') + '</br>'; var contribution = $(this).data('contribution') + '</br>'; $.magnificPopup.open({ items: { src: '<div id="ovelary-mathjax" class="overlay-white oc-content overlay-white-500">' + author + affiliation + contribution + '</div>', type: 'inline' }, callbacks: { open: function() { var div = document.getElementById("overlay-mathjax") MathJax.Hub.Queue(["Typeset", MathJax.Hub, div]); }, } }) }) }); </script> <tr><td class="formatRecordLabel"> Report number </td><td style="padding-left:5px;">CERN-ACC-2015-228</td></tr> <tr><td class="formatRecordLabel"> Title </td><td style="padding-left:5px;"><b>Characterization of Nb Coating in HIE-ISOLDE QWR Superconducting Accelerating Cavities by means of SEM-FIB and TEM</b></td></tr> <tr><td class="formatRecordLabel"><span style="white-space:nowrap;"> Author(s) </span> </td><td style="padding-left:5px;"><a href="https://cds.cern.ch/search?f=author&p=B%C3%A1rtov%C3%A1%2C%20Barbora&ln=en">Bártová, Barbora</a> (CERN) ; <a href="https://cds.cern.ch/search?f=author&p=Aebersold%2C%20Arthur&ln=en">Aebersold, Arthur</a> (Ecole Polytechnique, Lausanne) ; <a href="https://cds.cern.ch/search?f=author&p=Alexander%2C%20Duncan&ln=en">Alexander, Duncan</a> (Ecole Polytechnique, Lausanne) ; <a href="https://cds.cern.ch/search?f=author&p=Calatroni%2C%20Sergio&ln=en">Calatroni, Sergio</a> (CERN) ; <a href="https://cds.cern.ch/search?f=author&p=Cantoni%2C%20Marco&ln=en">Cantoni, Marco</a> (Ecole Polytechnique, Lausanne) ; <a href="https://cds.cern.ch/search?f=author&p=Sublet%2C%20Alban&ln=en">Sublet, Alban</a> (CERN) ; <a href="https://cds.cern.ch/search?f=author&p=Taborelli%2C%20Mauro&ln=en">Taborelli, Mauro</a> (CERN)</td></tr> <tr><td class="formatRecordLabel"> Publication </td><td style="padding-left:5px;">2015</td></tr> <tr><td class="formatRecordLabel"> Number of pages </td><td style="padding-left:5px;">4</td></tr> <tr><td class="formatRecordLabel"> In: </td><td style="padding-left:5px;"><a href="https://cds.cern.ch/record/2024999">6th International Particle Accelerator Conference</a>, Richmond, VA, USA, 3 - 8 May 2015, pp.WEPHA022</td></tr> <tr><td class="formatRecordLabel"> Subject category </td><td style="padding-left:5px;">Accelerators and Storage Rings</td></tr> <tr><td class="formatRecordLabel"> Accelerator/Facility, Experiment </td><td style="padding-left:5px;"><a href="https://cds.cern.ch/search?p=CERN%20ISOLDE&f=693__a">CERN ISOLDE</a></td></tr> <tr><td class="formatRecordLabel"> Abstract </td><td style="padding-left:5px;">The Quarter Wave Resonators (QWR) high-β cavities (0.3m diameter and 0.9m height) are made from OFE 3D-forged copper and are coated by DC-bias diode sputtering with a thin superconducting layer of niobium. The Nb film thickness, morphology, purity and quality are critical parameters for RF performances of the cavity. They have been investigated in a detailed material study. The coating structure at different positions along a test cavity was observed by cross-section imaging using SEM-FIB instrument. The samples from the top of the cavity showed presence of unexpected porosities, whose volume was investigated using FIB tomography. TEM lamella was prepared for two samples (top part and inner conductor of the cavity) to study in detail the grain orientation in the coating, its chemical composition and structure. The 14-layer structure in thick coating was indeed evidenced by the TEM analysis. Chemical mapping revealed the presence of a few nm in size copper precipitates close to the Nb/Cu interface and a passivating oxide layer of 10 nm thickness on top of the coating and around porosities. However no impurities or interface layer along the coating profile were present.</td></tr> <tr><td class="formatRecordLabel"> Copyright/License </td><td style="padding-left:5px;">publication: © 2015-2024 The Author(s) (License: <a href="http://creativecommons.org/licenses/by/3.0/">CC-BY-3.0</a>)</td></tr> </table> <br/>Corresponding record in: <a href="http://inspirehep.net/record/1418051">Inspire</a> <small> </small> <br/> <br/><br/><div align="right"><div style="padding-bottom:2px;padding-top:30px;"><span class="moreinfo" style="margin-right:10px;"> <a href="" class="moreinfo">Back to search</a> </span></div></div> <div class="bottom-left-folded"><div class="recordlastmodifiedbox" style="position:relative;margin-left:1px"> Record created 2016-03-27, last modified 2024-02-23</div></div> <div class="bottom-right-folded" style="text-align:right;padding-bottom:2px;"> <span class="moreinfo" style="margin-right:10px;"><a href="/search?ln=en&p=recid%3A2141886&rm=wrd" class="moreinfo">Similar records</a></span></div> </div> </div> </div> <br/> <br /> <div class="detailedrecordminipanel"> <div class="top-left"></div><div class="top-right"></div> <div class="inside"> <div id="detailedrecordminipanelfile" style="width:33%;float:left;text-align:center;margin-top:0"> <div><small class="detailedRecordActions">Published version from JACoW:</small> <br /><a href="/record/2141886/files/wepha022.pdf"><img style="border:none" src="/img/file-icon-text-12x16.gif" alt="Download fulltext"/>PDF</a><br /></div><small class="detailedRecordActions">External link:</small><br /><small><a href="https://accelconf.web.cern.ch/IPAC2015/papers/wepha022.pdf"><img style="border:none" src="/img/file-icon-text-12x16.gif" alt="Download fulltext"/>JACOW</a></small> </div> <div id="detailedrecordminipanelreview" style="width:30%;float:left;text-align:center"> </div> <div id="detailedrecordminipanelactions" style="width:36%;float:right;text-align:right;"> <ul class="detailedrecordactions"> <li><a href="/yourbaskets/add?ln=en&recid=2141886">Add to personal basket</a></li> <li>Export as <a style="text-decoration:underline;font-weight:normal" href="/record/2141886/export/hx?ln=en">BibTeX</a>, <a style="text-decoration:underline;font-weight:normal" href="/record/2141886/export/hm?ln=en">MARC</a>, <a style="text-decoration:underline;font-weight:normal" href="/record/2141886/export/xm?ln=en">MARCXML</a>, <a style="text-decoration:underline;font-weight:normal" href="/record/2141886/export/xd?ln=en">DC</a>, <a style="text-decoration:underline;font-weight:normal" href="/record/2141886/export/xe?ln=en">EndNote</a>, <!-- <a style="text-decoration:underline;font-weight:normal" href="/record/2141886/export/xe8x?ln=en">EndNote (8-X)</a>,--> <a style="text-decoration:underline;font-weight:normal" href="/record/2141886/export/xn?ln=en">NLM</a>, <a style="text-decoration:underline;font-weight:normal" href="/record/2141886/export/xw?ln=en">RefWorks</a> </li> </ul> <div style='padding-left: 13px;'> <!-- JQuery Bookmark Button BEGIN --> <div id="bookmark"></div> <div id="bookmark_sciencewise"></div> <style type="text/css"> #bookmark_sciencewise, #bookmark {float: left;} #bookmark_sciencewise li {padding: 2px; width: 25px;} #bookmark_sciencewise ul, #bookmark ul {list-style-image: none;} </style> <script type="text/javascript" src="/js/jquery.bookmark.min.js"></script> <style type="text/css">@import "/css/jquery.bookmark.css";</style> <script type="text/javascript">// <![CDATA[ $.bookmark.addSite('sciencewise', 'ScienceWise.info', 'https://cds.cern.ch/img/sciencewise.png', 'en', 'bookmark', 'http://sciencewise.info/bookmarks/cds:2141886/add'); $('#bookmark_sciencewise').bookmark({sites: ['sciencewise']}); $('#bookmark').bookmark({ sites: ['facebook', 'twitter', 'linkedin', 'google_plusone'], icons: '/img/bookmarks.png', url: 'https://cds.cern.ch/record/2141886', addEmail: true, title: "Characterization of Nb Coating in HIE-ISOLDE QWR Superconducting Accelerating Cavities by means of SEM-FIB and TEM", description: "The Quarter Wave Resonators (QWR) high-\u03b2 cavities (0.3m diameter and 0.9m height) are made from OFE 3D-forged copper and are coated by DC-bias diode sputtering with a thin superconducting layer of niobium. The Nb film thickness, morphology, purity and quality are critical parameters for RF performances of the cavity. They have been investigated in a detailed material study. The coating structure at different positions along a test cavity was observed by cross-section imaging using SEM-FIB instrument. The samples from the top of the cavity showed presence of unexpected porosities, whose volume was investigated using FIB tomography. TEM lamella was prepared for two samples (top part and inner conductor of the cavity) to study in detail the grain orientation in the coating, its chemical composition and structure. The 14-layer structure in thick coating was indeed evidenced by the TEM analysis. Chemical mapping revealed the presence of a few nm in size copper precipitates close to the Nb/Cu interface and a passivating oxide layer of 10 nm thickness on top of the coating and around porosities. 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