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class="flex items-center" data-v-0016287f><p class="m-text text-sm text-color-link-bold cursor-pointer pr-xs" data-v-0016287f>supplementary.zip (46.53KB )</p><svg xmlns="http://www.w3.org/2000/svg" xmlns:xlink="http://www.w3.org/1999/xlink" aria-hidden="true" role="img" data-testid="link" class="text-color-link-bold cursor-pointer" style="" width="16" height="16" viewBox="0 0 16 16" data-v-0016287f></svg></div></div></div></div></div></div><div><div class="pb-md border-b border-color-default pt-sm"><div class="w-full relative overflow-hidden"><div><div class="clamp-3"><span class="pr-sm"><span class="m-text text-sm"><div class="m-avatar flex items-center justify-center overflow-hidden rounded-full bg-brand-bold font-medium text-color-on-brand h-5 w-5 min-w-5 text-[0.575rem] !inline-block align-middle mr-xs" data-testid="m-avatar"><img src="/statics/img/design/default-user.png"><span class="sr-only"></span></div><span><a href="https://sciprofiles.com/profile/4038346" target="_blank" rel="noopener noreferrer">Koray Tanrıver</a></span><sup> *</sup><div class="m-icon-custom text-color-inherit pl-xs inline-block"><a href="https://orcid.org/0009-0007-8904-1878" rel="noopener noreferrer" target="_blank"><img src="/_ipx/_/img/articleorcid.webp" onerror="this.setAttribute('data-error', 1)" data-nuxt-img srcset="/_ipx/_/img/articleorcid.webp 1x, /_ipx/_/img/articleorcid.webp 2x" class="w-4"></a></div><span>,</span></span></span><span class="pr-sm"><span class="m-text text-sm"><span><a href="https://sciprofiles.com/profile/author/OGxpMDdIVHZieGxiUkc5UThHK0JwSWI0NUY5c1libTJyY2R1N0FTenhiVT0=" target="_blank" rel="noopener noreferrer">Mehmet Bilgin</a></span><span>,</span></span></span><span class="pr-sm"><span class="m-text text-sm"><div class="m-avatar flex items-center justify-center overflow-hidden rounded-full bg-brand-bold font-medium text-color-on-brand h-5 w-5 min-w-5 text-[0.575rem] !inline-block align-middle mr-xs" data-testid="m-avatar"><img src="/img/user_image/3397209/Selin_Şahin.png"><span class="sr-only"></span></div><span><a href="https://sciprofiles.com/profile/3397209" target="_blank" rel="noopener noreferrer">Selin Şahin Sevgili</a></span><div class="m-icon-custom text-color-inherit pl-xs inline-block"><a href="https://orcid.org/0000-0002-9989-9823" rel="noopener noreferrer" target="_blank"><img src="/_ipx/_/img/articleorcid.webp" onerror="this.setAttribute('data-error', 1)" data-nuxt-img srcset="/_ipx/_/img/articleorcid.webp 1x, /_ipx/_/img/articleorcid.webp 2x" class="w-4"></a></div><span>,</span></span></span><span class="pr-sm"><span class="m-text text-sm"><span><a href="https://sciprofiles.com/profile/author/RWtBWkc1VGxHVFQ2WElDWFRIRzNlK2J2RGVvWDVMaXY4T0szQjd5M2h2dz0=" target="_blank" rel="noopener noreferrer">İrem Toprakçı Yüksel</a></span><span>,</span></span></span><span class="pr-sm"><span class="m-text text-sm"><span><a href="https://sciprofiles.com/profile/author/WmExeCtHbmoyYWNhOXN1WUdkVlBEdjF5eUJMQjlBN0Rxb3p2cmF3QWhYND0=" target="_blank" rel="noopener noreferrer">Ebru Kurtulbaş Şahin</a></span></span></span></div><div class="invisible absolute"><span class="pr-sm"><span class="m-text text-sm"><div class="m-avatar flex items-center justify-center overflow-hidden rounded-full bg-brand-bold font-medium text-color-on-brand h-5 w-5 min-w-5 text-[0.575rem] !inline-block align-middle mr-xs" data-testid="m-avatar"><img src="/statics/img/design/default-user.png"><span class="sr-only"></span></div><span><a href="https://sciprofiles.com/profile/4038346" target="_blank" rel="noopener noreferrer">Koray Tanrıver</a></span><sup> *</sup><div class="m-icon-custom text-color-inherit pl-xs inline-block"><a href="https://orcid.org/0009-0007-8904-1878" rel="noopener noreferrer" target="_blank"><img src="/_ipx/_/img/articleorcid.webp" onerror="this.setAttribute('data-error', 1)" data-nuxt-img srcset="/_ipx/_/img/articleorcid.webp 1x, /_ipx/_/img/articleorcid.webp 2x" class="w-4"></a></div><span>,</span></span></span><span class="pr-sm"><span class="m-text text-sm"><span><a href="https://sciprofiles.com/profile/author/OGxpMDdIVHZieGxiUkc5UThHK0JwSWI0NUY5c1libTJyY2R1N0FTenhiVT0=" target="_blank" rel="noopener noreferrer">Mehmet Bilgin</a></span><span>,</span></span></span><span class="pr-sm"><span class="m-text text-sm"><div class="m-avatar flex items-center justify-center overflow-hidden rounded-full bg-brand-bold font-medium text-color-on-brand h-5 w-5 min-w-5 text-[0.575rem] !inline-block align-middle mr-xs" data-testid="m-avatar"><img src="/img/user_image/3397209/Selin_Şahin.png"><span class="sr-only"></span></div><span><a href="https://sciprofiles.com/profile/3397209" target="_blank" rel="noopener noreferrer">Selin Şahin Sevgili</a></span><div class="m-icon-custom text-color-inherit pl-xs inline-block"><a href="https://orcid.org/0000-0002-9989-9823" rel="noopener noreferrer" target="_blank"><img src="/_ipx/_/img/articleorcid.webp" onerror="this.setAttribute('data-error', 1)" data-nuxt-img srcset="/_ipx/_/img/articleorcid.webp 1x, /_ipx/_/img/articleorcid.webp 2x" class="w-4"></a></div><span>,</span></span></span><span class="pr-sm"><span class="m-text text-sm"><span><a href="https://sciprofiles.com/profile/author/RWtBWkc1VGxHVFQ2WElDWFRIRzNlK2J2RGVvWDVMaXY4T0szQjd5M2h2dz0=" target="_blank" rel="noopener noreferrer">İrem Toprakçı Yüksel</a></span><span>,</span></span></span><span class="pr-sm"><span class="m-text text-sm"><span><a href="https://sciprofiles.com/profile/author/WmExeCtHbmoyYWNhOXN1WUdkVlBEdjF5eUJMQjlBN0Rxb3p2cmF3QWhYND0=" target="_blank" rel="noopener noreferrer">Ebru Kurtulbaş Şahin</a></span></span></span></div></div><div style="display:none;" class="mt-sm"><button class="m-button m-button--sm m-button--tertiary rounded !inline-flex after:hidden bg-white" type="button"><span class="inline-flex h-full w-full items-center gap-2 whitespace-nowrap justify-center">Show more <svg xmlns="http://www.w3.org/2000/svg" xmlns:xlink="http://www.w3.org/1999/xlink" aria-hidden="true" role="img" data-testid="keyboard_arrow_down" style="" width="16" height="16" viewBox="0 0 16 16"></svg></span></button></div></div><p class="m-text text-sm text-color-error pt-sm">This version is not peer-reviewed</p></div></div><div class="py-md border-b border-color-default"><div class="m-select common-field bg-white"><div class="common-field__wrapper" data-headlessui-state><div class="relative w-full cursor-default"><div class="flex items-center"><button id="headlessui-listbox-button-mui-52924" type="button" aria-haspopup="listbox" aria-expanded="false" data-headlessui-state data-testid="select-activator" class="common-field__dropdown-input [&>span]:overflow-hidden h-10"><span class="flex w-full items-center gap-1 [&>span]:truncate"><span>Version 1</span></span><div class="flex"><svg xmlns="http://www.w3.org/2000/svg" xmlns:xlink="http://www.w3.org/1999/xlink" aria-hidden="true" role="img" data-testid="keyboard_arrow_down" class="duration-400 transition-transform" style="" width="24" height="24" viewBox="0 0 16 16"></svg></div></button></div></div></div></div><div class="pt-sm"><div class="flex"><p class="m-text text-xs">Submitted:</p><p class="m-text text-xs pl-xs">25 November 2024</p></div><div class="flex pt-sm"><p class="m-text text-xs">Posted: </p><p class="m-text text-xs pl-xs">26 November 2024</p></div></div><div class="pt-sm"><div><p class="m-text text-xs">You are already at the latest version </p></div></div><div></div></div><div class="py-md border-b border-color-default flex items-center justify-between" data-v-d8c082ee><div class="flex-none flex items-center" data-v-d8c082ee><span class="m-text text-xs pr-xs font-semibold flex-none" data-v-d8c082ee>Alerts</span><span data-v-d8c082ee></span></div><div class="m-switch flex items-center gap-2" data-v-d8c082ee><button class="relative inline-flex h-[1.4rem] w-[2.75rem] shrink-0 cursor-pointer items-center rounded-full border-2 border-color-transparent transition-colors duration-150 ease-out ui-focus-visible:ring-2 ui-focus-visible:ring-brand-bold ui-focus-visible:ring-opacity-75 bg-content-default hover:bg-content-bold active:bg-content-bolder" aria-label="Switch on" id="headlessui-switch-mui-52925" role="switch" type="button" tabindex="0" aria-checked="false" data-headlessui-state><span aria-hidden="true" class="pointer-events-none inline-block h-[1rem] w-[1rem] transform rounded-full bg-white shadow-lg ring-0 transition duration-200 ease-in-out translate-x-0.5"></span></button></div></div><div data-v-d8c082ee data-v-03f1a75d></div><div><h6 class="m-heading text-inherit m-h6 font-semibold pt-lg">Abstract</h6><div class="">There is an increasing demand for antioxidants, nutraceuticals and natural colorants. ß-Carotene is one of the commonly used commodities which fits description. ß-Carotene is a highly hydrophobic molecule; therefore, commercial extraction processes generally use highly non-polar solvents and these are barely environmentally friendly chemicals. The aim of this research was to develop effective and sustainable extraction processes for ß-Carotene from pumpkin and spinach using environmentally friendly green chemicals. A series of deep eutectic solvents with L-menthol and carboxylic aliphatic acids were synthesized for extraction of β-carotene from pumpkin and spinach via mechanical mixing (MMAE) and homogenization assisted extraction (HAE). Response surface methodology and ANOVA analyses were used to analyze the data. Menthol:Propionic Acid DESs had the best effect on the extraction of ß-Carotene (11.528 μg-ß-Carotene/gr-pumpkin for MMAE, 8.966 μg-ß-Carotene/gr-pumpkin for HAE, 16.924 μg-ß-Carotene/gr-spinach for MMAE and 18.870 μg-ß-Carotene/gr-spinach for HAE) under the optimal conditions (HBD molar ratio: 0.6452, 15 min. for MMAE of ß-Carotene from pumpkin, HBD molar ratio: 0.6198, 30.0 sec., 7061 rpm for HAE of ß-Carotene from pumpkin, HBD molar ratio: 0.8000, 60 min. for MMAE of ß-Carotene from spinach, HBD molar ratio: 0.8000, 120.0 sec., 7000 rpm for HAE of ß-Carotene from spinach).</div></div><div data-v-3ce94018><div class="pt-lg" data-v-3ce94018><span class="m-text text-body font-semibold" data-v-3ce94018>Keywords: </span><span class="m-text text-body pt-sm" data-v-3ce94018></span></div></div><div class="flex-1 pt-lg mr-lg lg:pt-0" data-v-6afb3413><div class="pt-md" data-v-6afb3413><div class="flex flex-wrap lg:flex-nowrap items-center" data-v-6afb3413><span class="m-text text-body font-semibold" data-v-6afb3413>Subject: </span><span class="m-text text-body" data-v-6afb3413>Chemistry and Materials Science</span><span class="" data-v-6afb3413> - </span><span class="m-text text-body" data-v-6afb3413>Applied Chemistry</span></div></div><div class="content-container" id="articleRef" data-v-6afb3413></div><div class="pt-lg" data-v-6afb3413><span class="m-text text-body font-semibold" data-v-6afb3413>Copyright: </span><span class="m-text text-body" data-v-6afb3413>This open access article is published under a <a href="https://creativecommons.org/licenses/by/4.0/" target="_blank" data-v-6afb3413><span class="hover:underline cursor-pointer text-color-link-bold" data-v-6afb3413>Creative Commons CC BY 4.0 license</span></a>, which permit the free download, distribution, and reuse, provided that the author and preprint are cited in any reuse.</span></div></div><div class="pt-md"></div><div class="pt-md lg:pt-lg" data-v-273fe5dc><div class="m-accordion mx-auto flex w-full 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The aim of this research was to develop effective and sustainable extraction processes for ß-Carotene from pumpkin and spinach using environmentally friendly green chemicals. A series of deep eutectic solvents with L-menthol and carboxylic aliphatic acids were synthesized for extraction of β-carotene from pumpkin and spinach via mechanical mixing (MMAE) and homogenization assisted extraction (HAE). Response surface methodology and ANOVA analyses were used to analyze the data. Menthol:Propionic Acid DESs had the best effect on the extraction of ß-Carotene (11.528 μg-ß-Carotene/gr-pumpkin for MMAE, 8.966 μg-ß-Carotene/gr-pumpkin for HAE, 16.924 μg-ß-Carotene/gr-spinach for MMAE and 18.870 μg-ß-Carotene/gr-spinach for HAE) under the optimal conditions (HBD molar ratio: 0.6452, 15 min. for MMAE of ß-Carotene from pumpkin, HBD molar ratio: 0.6198, 30.0 sec., 7061 rpm for HAE of ß-Carotene from pumpkin, HBD molar ratio: 0.8000, 60 min. for MMAE of ß-Carotene from spinach, HBD molar ratio: 0.8000, 120.0 sec., 7000 rpm for HAE of ß-Carotene from spinach).","Extraction of ß-Carotene from Pumpkin (\u003Cem>Curcubita moschata\u003C/em>) and Spinach (\u003Cem>Spinacia oleracea\u003C/em>) Using Environmentally Friendly Deep Eutectic Solvents (DESs)","ß-carotene; deep eutectic solvents; menthol; acetic acid; propionic acid; butyric acid; pumpkin; spinach; extraction; biomass",false,[],{"id":135,"name":136},52,"Applied Chemistry",{"id":66,"name":67},{"id":139,"name":140},15,"Article","2024-11-25 10:30:31","2024-11-26 13:06:11",[144,152,158,165,170],{"id":145,"name":146,"email":147,"is_corresponding":6,"orcid_link":148,"author_mark":149,"sp_link":150,"avatar":151},590576,"Koray Tanrıver","koray.tanriver@ogr.iuc.edu.tr","https://orcid.org/0009-0007-8904-1878","*","https://sciprofiles.com/profile/4038346","/statics/img/design/default-user.png",{"id":153,"name":154,"email":155,"is_corresponding":132,"orcid_link":47,"author_mark":156,"sp_link":157,"avatar":47},590577,"Mehmet Bilgin","mbilgin@iuc.edu.tr","","https://sciprofiles.com/profile/author/OGxpMDdIVHZieGxiUkc5UThHK0JwSWI0NUY5c1libTJyY2R1N0FTenhiVT0=",{"id":159,"name":160,"email":161,"is_corresponding":132,"orcid_link":162,"author_mark":156,"sp_link":163,"avatar":164},590578,"Selin Şahin Sevgili","selins@iuc.edu.tr","https://orcid.org/0000-0002-9989-9823","https://sciprofiles.com/profile/3397209","/img/user_image/3397209/Selin_Şahin.png",{"id":166,"name":167,"email":168,"is_corresponding":132,"orcid_link":47,"author_mark":156,"sp_link":169,"avatar":47},590579,"İrem Toprakçı Yüksel","irem.toprakciyuksel@iuc.edu.tr","https://sciprofiles.com/profile/author/RWtBWkc1VGxHVFQ2WElDWFRIRzNlK2J2RGVvWDVMaXY4T0szQjd5M2h2dz0=",{"id":171,"name":172,"email":173,"is_corresponding":132,"orcid_link":47,"author_mark":156,"sp_link":174,"avatar":47},590580,"Ebru Kurtulbaş Şahin","ebru.kurtulbas@iuc.edu.tr","https://sciprofiles.com/profile/author/WmExeCtHbmoyYWNhOXN1WUdkVlBEdjF5eUJMQjlBN0Rxb3p2cmF3QWhYND0=",{"filename":176,"url":177,"filesize":178},"supplementary.zip","/frontend/manuscript/f6fd592b9b7ae83892917e39b0a3a8b0/download_pub/supplementary",47651,{"filename":180,"url":181,"filesize":182},"final_file.pdf","/frontend/manuscript/f6fd592b9b7ae83892917e39b0a3a8b0/download_pub",1518013,[],{"viewed":185,"downloaded":186},"10","8",[188],{"version":7,"hash_key":127,"id":126,"change":47},"Tanrıver, K.; Bilgin, M.; Şahin Sevgili, S.; Toprakçı Yüksel, İ.; Kurtulbaş Şahin, E. 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