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Comparison Display
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class="breadcrumb-section--link">Home</a> </li> <li class="breadcrumb-section--item"> <span>Comparisons</span> </li> </ul> </div> </div> </div> </div> <section id="tabsPage" class="comparison-display"> <section class="section_search-tabs section_create-comparison"> <div class="container"> <div class="row"> <div class="col-lg-12"> <div class="comparison-tabs-navigation-wrapper"> <ul class="tabs-list comparison-tabs-navigation _justified"> <li class="tabs-list-item js-info-tab-item active"> <a href="#informationTab" data-tab="tab1"> <span>Information</span> </a> </li> <li class="tabs-list-item js-graph-tab-item" > <a href="#graphsTab" data-tab="tab2"> <span>Graphs of Equivalence</span> </a> </li> <li class="tabs-list-item js-degrees-tab-item" > <a href="#degreesOfEquivalence" data-tab="tab3"> <span>Degrees of equivalence</span> </a> </li> <li class="tabs-list-item js-statements-tab-item" > <a href="#equivalenceStatementTab" data-tab="tab4"> <span>Equivalence statements</span> </a> </li> <li class="tabs-list-item js-measurements-tab-item"> <a href="#laboratoryMeasurementTab" data-tab="tab5"> <span>Laboratory measurements</span> </a> </li> </ul> </div> </div> </div> </div> </section> <section class="container tab-section" id="graphsTab"> <div class="tab-section__left-sidebar sticky" id="selectSection"> <div class="information-list-wrap"> <div> <div class="tab-top__filter__wrapper"> <a class="mob-filter-btn" href="#">Comparison</a> <div class="mod-title mob-wrapper"> Comparison <a class="mob-close" href="#">close</a> </div> <div class="filter-wrapper mob-wrapper"> <div class="tab-top__filter__item"> <div class="filter__item__title">Results</div> <div class="filter__item__wrapper"> <ul id="sectionList" class="information-list"> <li id="section-id-675"> <a href="#tabsPage" onclick="sectionDetailTabsView.selectSection('675')">Estradiol</a> </li> <li id="section-id-676"> <a href="#tabsPage" onclick="sectionDetailTabsView.selectSection('676')">Related Structure Impurities</a> </li> <li id="section-id-677"> <a href="#tabsPage" onclick="sectionDetailTabsView.selectSection('677')">Water</a> </li> <li id="section-id-678"> <a href="#tabsPage" onclick="sectionDetailTabsView.selectSection('678')">Volatile Organics</a> </li> <li id="section-id-679"> <a href="#tabsPage" onclick="sectionDetailTabsView.selectSection('679')">Non-Volatile Content</a> </li> </ul> </div> </div> </div> </div> </div> </div> </div> <div class="tab-section__content" id="tab-section-675"> <div class="tab-section__content-heading tab-section__content-heading_description-tabs"> <div class="tab-section__title"></div> <div class="tab-btn__wrapper"> <a class="tab-btn print-out" href="#print-out-popup"> <img src="/kcdb/static/icons/print-out-26b37ecfd24015b0ce7c6017c52bb708.svg" alt=""> <span>print out</span> </a> </div> </div> <div class="info-block js-block-content"> <div class="result-description"><p><font class="Verdana_12px" color="#003399"><font class="standard_12px"><strong>MEASURAND : Mass fraction of Estradiol in the CCQM-K55.a samples</strong></font></font></p> <p></p> <p><font color="#1e1182" face="Verdana"><font class="standard_12px"><strong>Degrees of equivalence : offset <em>D<sub>i</sub></em> and expanded uncertainty (<em>k</em> = 2) <em>U<sub>i</sub></em> expressed in mg/g, and also in relative terms</strong></font></font></p> <p align="center"><img border="0" src="/kcdb/comparison/download/published-section-block-file/401/675/degree/675/ccqm-k55.a_graph_estradiol.gif" /></p> <p align="left"><font class="standard_12px"><strong><em>x</em><sub>R</sub> = 984.3 mg/g <br />2 <em>u</em><sub>R </sub>= 0.8 mg/g</strong></font></p></div> </div> </div> <div class="tab-section__content" id="tab-section-676"> <div class="tab-section__content-heading tab-section__content-heading_description-tabs"> <div class="tab-section__title"></div> <div class="tab-btn__wrapper"> <a class="tab-btn print-out" href="#print-out-popup"> <img src="/kcdb/static/icons/print-out-26b37ecfd24015b0ce7c6017c52bb708.svg" alt=""> <span>print out</span> </a> </div> </div> <div class="info-block js-block-content"> <div class="result-description"><p><font class="Verdana_12px" color="#003399"><font class="standard_12px"><strong>MEASURAND : Mass fraction of Related Structure Impurities in the CCQM-K55.a samples</strong></font></font></p> <p></p> <p><font color="#1e1182" face="Verdana"><font class="standard_12px"><strong>Degrees of equivalence : offset <em>D<sub>i</sub></em> and expanded uncertainty (<em>k</em> = 2) <em>U<sub>i</sub></em> expressed in mg/g, and also in relative terms</strong></font></font></p> <p align="center"><img border="0" src="/kcdb/comparison/download/published-section-block-file/401/676/degree/676/ccqm-k55.a_graph_related_structure_impurities.gif" /></p> <p align="left"><font class="standard_12px"><strong><em>x</em><sub>R</sub> = 8.65 mg/g <br />2 <em>u</em><sub>R </sub>= 0.32 mg/g</strong></font></p></div> </div> </div> <div class="tab-section__content" id="tab-section-677"> <div class="tab-section__content-heading tab-section__content-heading_description-tabs"> <div class="tab-section__title"></div> <div class="tab-btn__wrapper"> <a class="tab-btn print-out" href="#print-out-popup"> <img src="/kcdb/static/icons/print-out-26b37ecfd24015b0ce7c6017c52bb708.svg" alt=""> <span>print out</span> </a> </div> </div> <div class="info-block js-block-content"> <div class="result-description"><p><font class="Verdana_12px" color="#003399"><font class="standard_12px"><strong>MEASURAND : Mass fraction of Water in the CCQM-K55.a samples</strong></font></font></p> <p></p> <p><font color="#1e1182" face="Verdana"><font class="standard_12px"><strong>Degrees of equivalence : offset <em>D<sub>i</sub></em> and expanded uncertainty (<em>k</em> = 2) <em>U<sub>i</sub></em> expressed in mg/g, and also in relative terms</strong></font></font></p> <p align="center"><img border="0" src="/kcdb/comparison/download/published-section-block-file/401/677/degree/677/ccqm-k55.a_graph_water.gif" /></p> <p align="left"><font class="standard_12px"><strong><em>x</em><sub>R</sub> = 6.75 mg/g <br />2 <em>u</em><sub>R </sub>= 0.42 mg/g</strong></font></p></div> </div> </div> <div class="tab-section__content" id="tab-section-678"> <div class="tab-section__content-heading tab-section__content-heading_description-tabs"> <div class="tab-section__title"></div> <div class="tab-btn__wrapper"> <a class="tab-btn print-out" href="#print-out-popup"> <img src="/kcdb/static/icons/print-out-26b37ecfd24015b0ce7c6017c52bb708.svg" alt=""> <span>print out</span> </a> </div> </div> <div class="info-block js-block-content"> <div class="result-description"><p><font class="Verdana_12px" color="#003399"><font class="standard_12px"><strong>MEASURAND : Mass fraction of Volatile Organics in the CCQM-K55.a samples</strong></font></font></p> <p></p> <p><font color="#1e1182" face="Verdana"><font class="standard_12px"><strong>Degrees of equivalence : offset <em>D<sub>i</sub></em> and expanded uncertainty (<em>k</em> = 2) <em>U<sub>i</sub></em> expressed in mg/g, and also in relative terms</strong></font></font></p> <p align="center"><img border="0" src="/kcdb/comparison/download/published-section-block-file/401/678/degree/678/ccqm-k55.a_graph_volatile_organics.gif" /></p> <p align="left"><font class="standard_12px"><strong><em>x</em><sub>R</sub> = 0.10 mg/g <br />2 <em>u</em><sub>R </sub>= 0.12 mg/g</strong></font></p></div> </div> </div> <div class="tab-section__content" id="tab-section-679"> <div class="tab-section__content-heading tab-section__content-heading_description-tabs"> <div class="tab-section__title"></div> <div class="tab-btn__wrapper"> <a class="tab-btn print-out" href="#print-out-popup"> <img src="/kcdb/static/icons/print-out-26b37ecfd24015b0ce7c6017c52bb708.svg" alt=""> <span>print out</span> </a> </div> </div> <div class="info-block js-block-content"> <div class="result-description"><p><font class="Verdana_12px" color="#003399"><font class="standard_12px"><strong>MEASURAND : Mass fraction of Non-Volatile Content in the CCQM-K55.a samples</strong></font></font></p> <p></p> <p><font color="#1e1182" face="Verdana"><font class="standard_12px"><strong>Degrees of equivalence : offset <em>D<sub>i</sub></em> and expanded uncertainty (<em>k</em> = 2) <em>U<sub>i</sub></em> expressed in mg/g, and also in relative terms</strong></font></font></p> <p align="center"><img border="0" src="/kcdb/comparison/download/published-section-block-file/401/679/degree/679/ccqm-k55.a_graph_non_volatiles.gif" /></p> <p align="left"><font class="standard_12px"><strong><em>x</em><sub>R</sub> = 0.20 mg/g <br />2 <em>u</em><sub>R </sub>= 0.24 mg/g</strong></font></p></div> </div> </div> </section> <section class="container tab-section" id="degreesOfEquivalence"> <div class="tab-section__left-sidebar sticky" id="selectSection"> <div class="information-list-wrap"> <div> <div class="tab-top__filter__wrapper"> <a class="mob-filter-btn" href="#">Comparison</a> <div class="mod-title mob-wrapper"> Comparison <a class="mob-close" href="#">close</a> </div> <div class="filter-wrapper mob-wrapper"> <div class="tab-top__filter__item"> <div class="filter__item__title">Results</div> <div class="filter__item__wrapper"> <ul id="sectionList" class="information-list"> <li id="section-id-675"> <a href="#tabsPage" onclick="sectionDetailTabsView.selectSection('675')">Estradiol</a> </li> <li id="section-id-676"> <a href="#tabsPage" onclick="sectionDetailTabsView.selectSection('676')">Related Structure Impurities</a> </li> <li id="section-id-677"> <a href="#tabsPage" onclick="sectionDetailTabsView.selectSection('677')">Water</a> </li> <li id="section-id-678"> <a href="#tabsPage" onclick="sectionDetailTabsView.selectSection('678')">Volatile Organics</a> </li> <li id="section-id-679"> <a href="#tabsPage" onclick="sectionDetailTabsView.selectSection('679')">Non-Volatile Content</a> </li> </ul> </div> </div> </div> </div> </div> </div> </div> <div class="tab-section__content" id="tab-section-675"> <div class="tab-section__content-heading tab-section__content-heading_description-tabs"> <div class="tab-section__title"></div> <div class="tab-btn__wrapper"> <a class="tab-btn print-out" href="#print-out-popup"> <img src="/kcdb/static/icons/print-out-26b37ecfd24015b0ce7c6017c52bb708.svg" alt=""> <span>print out</span> </a> </div> </div> <div class="info-block js-block-content"> <div class="result-description"><p></p><p><font class="Verdana_12px" color="#003399"><font class="standard_12px"><strong>MEASURAND : Mass fraction of Estradiol in the CCQM-K55.a samples</strong></font></font></p><p></p><p><font color="#1e1182" face="Verdana"><font class="standard_12px"><strong>Degrees of equivalence : offset <em>D<sub>i</sub></em> and expanded uncertainty (<em>k</em> = 2) <em>U<sub>i</sub></em> expressed in mg/g<br /></strong><font class="standard_12px"><strong><em>x</em><sub>R</sub> = 984.3 mg/g and 2 <em>u</em><sub>R </sub>= 0.8 mg/g</strong></font></font></font></p><p align="center"><img border="0" src="/kcdb/comparison/download/published-section-block-file/401/675/degree/675/ccqm-k55.a_does_estradiol.gif" /></p><p></p><table><tbody><tr><td></td></tr></tbody></table><p></p><p><font class="standard_12px">Results are presented under A4 printable format in <a class="bleu_12px" href="/kcdb/comparison/download/published-section-block-file/401/675/degree/675/ccqm-k55.a_aug12.pdf" target="_blank">Summary Results</a> (PDF file).</font></p></div> </div> </div> <div class="tab-section__content" id="tab-section-676"> <div class="tab-section__content-heading tab-section__content-heading_description-tabs"> <div class="tab-section__title"></div> <div class="tab-btn__wrapper"> <a class="tab-btn print-out" href="#print-out-popup"> <img src="/kcdb/static/icons/print-out-26b37ecfd24015b0ce7c6017c52bb708.svg" alt=""> <span>print out</span> </a> </div> </div> <div class="info-block js-block-content"> <div class="result-description"><p></p><p><font class="Verdana_12px" color="#003399"><font class="standard_12px"><strong>MEASURAND : Mass fraction of Related Structure Impurities in the CCQM-K55.a samples</strong></font></font></p><p></p><p><font color="#1e1182" face="Verdana"><font class="standard_12px"><strong>Degrees of equivalence : offset <em>D<sub>i</sub></em> and expanded uncertainty (<em>k</em> = 2) <em>U<sub>i</sub></em> expressed in mg/g<br /></strong><font class="standard_12px"><strong><em>x</em><sub>R</sub> = 8.65 mg/g and 2 <em>u</em><sub>R </sub>= 0.32 mg/g</strong></font></font></font></p><p align="center"><img border="0" src="/kcdb/comparison/download/published-section-block-file/401/676/degree/676/ccqm-k55.a_does_related_structure_impurities.gif" /></p><p></p><table><tbody><tr><td></td></tr></tbody></table><p></p><p><font class="standard_12px">Results are presented under A4 printable format in <a class="bleu_12px" href="/kcdb/comparison/download/published-section-block-file/401/676/degree/676/ccqm-k55.a_aug12.pdf" target="_blank">Summary Results</a> (PDF file).</font></p></div> </div> </div> <div class="tab-section__content" id="tab-section-677"> <div class="tab-section__content-heading tab-section__content-heading_description-tabs"> <div class="tab-section__title"></div> <div class="tab-btn__wrapper"> <a class="tab-btn print-out" href="#print-out-popup"> <img src="/kcdb/static/icons/print-out-26b37ecfd24015b0ce7c6017c52bb708.svg" alt=""> <span>print out</span> </a> </div> </div> <div class="info-block js-block-content"> <div class="result-description"><p></p><p><font class="Verdana_12px" color="#003399"><font class="standard_12px"><strong>MEASURAND : Mass fraction of Water in the CCQM-K55.a samples</strong></font></font></p><p></p><p><font color="#1e1182" face="Verdana"><font class="standard_12px"><strong>Degrees of equivalence : offset <em>D<sub>i</sub></em> and expanded uncertainty (<em>k</em> = 2) <em>U<sub>i</sub></em> expressed in mg/g<br /></strong><font class="standard_12px"><strong><em>x</em><sub>R</sub> = 6.75 mg/g and 2 <em>u</em><sub>R </sub>= 0.42 mg/g</strong></font></font></font></p><p align="center"><img border="0" src="/kcdb/comparison/download/published-section-block-file/401/677/degree/677/ccqm-k55.a_does_water.gif" /></p><p></p><table><tbody><tr><td></td></tr></tbody></table><p></p><p><font class="standard_12px">Results are presented under A4 printable format in <a class="bleu_12px" href="/kcdb/comparison/download/published-section-block-file/401/677/degree/677/ccqm-k55.a_aug12.pdf" target="_blank">Summary Results</a> (PDF file).</font></p></div> </div> </div> <div class="tab-section__content" id="tab-section-678"> <div class="tab-section__content-heading tab-section__content-heading_description-tabs"> <div class="tab-section__title"></div> <div class="tab-btn__wrapper"> <a class="tab-btn print-out" href="#print-out-popup"> <img src="/kcdb/static/icons/print-out-26b37ecfd24015b0ce7c6017c52bb708.svg" alt=""> <span>print out</span> </a> </div> </div> <div class="info-block js-block-content"> <div class="result-description"><p></p><p><font class="Verdana_12px" color="#003399"><font class="standard_12px"><strong>MEASURAND : Mass fraction of Volatile Organics in the CCQM-K55.a samples</strong></font></font></p><p></p><p><font color="#1e1182" face="Verdana"><font class="standard_12px"><strong>Degrees of equivalence : offset <em>D<sub>i</sub></em> and expanded uncertainty (<em>k</em> = 2) <em>U<sub>i</sub></em> expressed in mg/g<br /></strong><font class="standard_12px"><strong><em>x</em><sub>R</sub> = 0.10 mg/g and 2 <em>u</em><sub>R </sub>= 0.12 mg/g</strong></font></font></font></p><p align="center"><img border="0" src="/kcdb/comparison/download/published-section-block-file/401/678/degree/678/ccqm-k55.a_does_volatile_organics.gif" /></p><p></p><table><tbody><tr><td></td></tr></tbody></table><p></p><p><font class="standard_12px">Results are presented under A4 printable format in <a class="bleu_12px" href="/kcdb/comparison/download/published-section-block-file/401/678/degree/678/ccqm-k55.a_aug12.pdf" target="_blank">Summary Results</a> (PDF file).</font></p></div> </div> </div> <div class="tab-section__content" id="tab-section-679"> <div class="tab-section__content-heading tab-section__content-heading_description-tabs"> <div class="tab-section__title"></div> <div class="tab-btn__wrapper"> <a class="tab-btn print-out" href="#print-out-popup"> <img src="/kcdb/static/icons/print-out-26b37ecfd24015b0ce7c6017c52bb708.svg" alt=""> <span>print out</span> </a> </div> </div> <div class="info-block js-block-content"> <div class="result-description"><p></p><p><font class="Verdana_12px" color="#003399"><font class="standard_12px"><strong>MEASURAND : Mass fraction of Non-Volatile Content in the CCQM-K55.a samples</strong></font></font></p><p></p><p><font color="#1e1182" face="Verdana"><font class="standard_12px"><strong>Degrees of equivalence : offset <em>D<sub>i</sub></em> and expanded uncertainty (<em>k</em> = 2) <em>U<sub>i</sub></em> expressed in mg/g<br /></strong><font class="standard_12px"><strong><em>x</em><sub>R</sub> = 0.20 mg/g and 2 <em>u</em><sub>R </sub>= 0.24 mg/g</strong></font></font></font></p><p align="center"><img border="0" src="/kcdb/comparison/download/published-section-block-file/401/679/degree/679/ccqm-k55.a_does_non_volatiles.gif" /></p><p></p><table><tbody><tr><td></td></tr></tbody></table><p></p><p><font class="standard_12px">Results are presented under A4 printable format in <a class="bleu_12px" href="/kcdb/comparison/download/published-section-block-file/401/679/degree/679/ccqm-k55.a_aug12.pdf" target="_blank">Summary Results</a> (PDF file).</font></p></div> </div> </div> </section> <section class="container tab-section active" id="informationTab"> <div class="tab-section__left-sidebar sticky"> <div class="information-list-wrap"> <div> <div class="tab-top__filter__wrapper"> <a class="mob-filter-btn" href="#">Comparison</a> <div class="mod-title mob-wrapper"> Comparison <a class="mob-close" href="#">close</a> </div> <div class="filter-wrapper mob-wrapper"> <div class="tab-top__filter__item"> <div class="filter__item__title"><span>CC</span> comparison</div> <div class="filter__item__wrapper"> <ul class="information-list"> <li> <a href="/kcdb/comparison?id=401" class="active">CCQM-K55.a</a> </li> </ul> </div> <div class="filter__item__title">Linked comparison</div> <div class="filter__item__wrapper"> <ul class="information-list"> </ul> </div> </div> </div> </div> </div> </div> </div> <div class="tab-section__content"> <div class="tab-section__content-heading"> <div class="tab-section__title">CCQM-K55.a</div> <div class="tab-btn__wrapper"> <a class="tab-btn print-out" href="#print-out-popup"> <img src="/kcdb/static/icons/print-out-26b37ecfd24015b0ce7c6017c52bb708.svg" alt=""> <span>print out</span> </a> </div> </div> <div class="content-tabs"> <ul class="content-tabs__nav"> <li> <a href="#contentTabsInformation" class="active" data-toggle="tab">Information & contact</a> </li> <li> <a href="#contentTabsParticipants" data-toggle="tab">Participants</a> </li> </ul> <div class="content-tabs-wrap"> <div class="content-tab active" id="contentTabsInformation"> <div class="info-block"> <table class="info-block__table"> <tr> <td>Metrology area, Sub-field</td> <td><span>Chemistry and Biology</span>, <span>Organics</span></td> </tr> <tr> <td>Description</td> <td>Purity assessment of high purity organic materials: 17beta-Estradiol</td> </tr> <tr> <td>Time of measurements</td> <td> <span>2008</span><span > - <span>2009</span></span></td> </tr> <tr> <td>Status</td> <td>Approved for equivalence</td> </tr> </table> <table class="info-block__table"> <tr class="row-blue-bg"> <td>Final Reports of the comparisons</td> <td> <div class="without-margin-bottom"> <a href="http://www.bipm.org/utils/common/pdf/final_reports/QM/K55/CCQM-K55.a.pdf" target="_blank">CCQM-K55.a Final Report, 2012, 33 pages</a> </div> <div class="without-margin-bottom"> <a href="http://iopscience.iop.org/0026-1394/49/1A/08009/" target="_blank"><i>Metrologia</i>, 2012, <B>49</B>, <I>Tech. Suppl.</I>, 08009</a> </div> </td> </tr> <tr> <td>Measurand</td> <td><span class="without-margin-bottom">Mass fraction of 17beta-Estradiol<BR>Nominal value > 970 mg/g</span><br/> <span class="without-margin-bottom"></span></td> </tr> <tr> <td>Transfer device</td> <td class="without-margin-bottom">Dedicated samples</td> </tr> </table> <table class="info-block__table"> <tr> <td>Comparison type</td> <td><span>Key Comparison</span></td> </tr> <tr> <td>Consultative Committee</td> <td><span>CCQM</span> (<span>Consultative Committee for Amount of Substance</span>) </td> </tr> <tr> <td>Conducted by</td> <td><span>CCQM</span> (<span>Consultative Committee for Amount of Substance</span>) </td> </tr> <tr> <td>Comments</td> <td><p></p><p><P><FONT class=standard_12px><STRONG>Results published on 22 August 2012</STRONG></FONT></P> <P><FONT class=standard_12px>Purity assessment of high purity organic materials: 17beta-Estradiol</FONT></P> <P><FONT class=standard_12px></FONT></P></p></td> </tr> <tr class="row-blue-bg"> <td>Pilot institute</td> <td> <a href="http://www.bipm.org" target="_blank">BIPM</a> <br/> <span>Bureau International des Poids et Mesures</span><br/> <span>BIPM - International Organization</span><br/> </tr> <tr class="row-blue-bg"> <td>Contact person</td> <td><span>Steven Westwood</span><br/> <a href="bWFpbHRvOnN0ZXZlbi53ZXN0d29vZEBiaXBtLm9yZw==" target="_blank" class="mlink hidden"></a><div class="mlink-copy" title="Click to copy in the clipboard"></div><br/> <span> +33 (0) 1 45 07 70 57</span></td> </tr> </table> </div> <div id="showInfoPopin" class="mfp-hide white-popup-block small-popup-block"> <div class="form-horizontal form-horizontal_with-padding-top"> <div class="form-group person-names"> <span id="person-first-name" data-name="firstName">First Name</span> <span id="person-last-name" data-name="lastName">Last Name</span> </div> <div class="form-group person-info_wrapper"> <a href="#" class="person-info_item" id="person-mail" data-name="email">wwww@ww.www</a> <span class="person-info_item" id="person-telephone" data-name="phone">+356719836</span> <a href="#" target="_blank" id="person-institute" class="person-info_item" data-name="instituteSite">Institute 1</a> <span id="person-institute" class="person-info_item" data-name="instituteName">Institute 1</span> <span class="person-info_item" id="person-country" data-name="countryName">Khmelnitskiy</span> </div> <div class="form_create-cmc--btn"> <button class="popup-modal-dismiss cmc-button reset" type="button">Quit</button> </div> </div> </div> </div> <div class="content-tab" id="contentTabsParticipants"> <div class="info-block participant-block"> <table class="info-block__table table-blue-bg"> <thead> <tr> <th colspan="2">Pilot laboratory</th> </tr> </thead> <tr> <td> <a class="comparison-link" href="http://www.bipm.org" target="_blank">BIPM</a> </td> <td> <p class="comparison-info"> <span>Bureau International des Poids et Mesures</span>, <span>BIPM - International Organization</span>, <span>N/A</span> </p> </td> </tr> </table> <table class="info-block__table table-bg"> <tr> <td> <a class="comparison-link" href="http://www.bam.de/index4.htm" target="_blank">BAM</a> </td> <td> <p class="comparison-info"> <span>Bundesanstalt für Materialforschung und -prüfung</span>, <span>Germany</span>, <span>EURAMET</span> </p> </td> </tr> </table> <table class="info-block__table table-bg"> <tr> <td> <a class="comparison-link" href="http://www.cenam.mx" target="_blank">CENAM</a> </td> <td> <p class="comparison-info"> <span>Centro Nacional de Metrologia</span>, <span>Mexico</span>, <span>SIM</span> </p> </td> </tr> </table> <table class="info-block__table table-bg"> <tr> <td> <a class="comparison-link" href="http://www.govtlab.gov.hk/" target="_blank">GL</a> </td> <td> <p class="comparison-info"> <span>Government Laboratory</span>, <span>Hong Kong, China</span>, <span>APMP</span> </p> </td> </tr> </table> <table class="info-block__table table-bg"> <tr> <td> <a class="comparison-link" href="https://www.gov.br/inmetro/" target="_blank">INMETRO</a> </td> <td> <p class="comparison-info"> <span>Instituto Nacional de Metrologia, Qualidade e Tecnologia</span>, <span>Brazil</span>, <span>SIM</span> </p> </td> </tr> </table> <table class="info-block__table table-bg"> <tr> <td> <a class="comparison-link" href="http://www.lgc.co.uk" target="_blank">LGC</a> </td> <td> <p class="comparison-info"> <span>Laboratory of the Government Chemist</span>, <span>United Kingdom</span>, <span>EURAMET</span> </p> </td> </tr> </table> <table class="info-block__table table-bg"> <tr> <td> <a class="comparison-link" href="http://www.nim.ac.cn" target="_blank">NIM</a> </td> <td> <p class="comparison-info"> <span>National Institute of Metrology</span>, <span>China</span>, <span>APMP</span> </p> </td> </tr> </table> <table class="info-block__table table-bg"> <tr> <td> <a class="comparison-link" href="http://www.nist.gov" target="_blank">NIST</a> </td> <td> <p class="comparison-info"> <span>National Institute of Standards and Technology</span>, <span>United States</span>, <span>SIM</span> </p> </td> </tr> </table> <table class="info-block__table table-bg"> <tr> <td> <a class="comparison-link" href="http://www.measurement.gov.au/" target="_blank">NMIA</a> </td> <td> <p class="comparison-info"> <span>National Measurement Institute, Australia</span>, <span>Australia</span>, <span>APMP</span> </p> </td> </tr> </table> <table class="info-block__table table-bg"> <tr> <td> <a class="comparison-link" href="https://unit.aist.go.jp/nmij/english/" target="_blank">NMIJ AIST</a> </td> <td> <p class="comparison-info"> <span>National Metrology Institute of Japan</span>, <span>Japan</span>, <span>APMP</span> </p> </td> </tr> </table> <table class="info-block__table table-bg"> <tr> <td> <a class="comparison-link" href="http://www.nmisa.org" target="_blank">NMISA</a> </td> <td> <p class="comparison-info"> <span>National Metrology Institute of South Africa</span>, <span>South Africa</span>, <span>AFRIMETS</span> </p> </td> </tr> </table> <table class="info-block__table table-bg"> <tr> <td> <a class="comparison-link" href="https://nrc.canada.ca/en/research-development/research-collaboration/research-centres/metrology-research-centre" target="_blank">NRC</a> </td> <td> <p class="comparison-info"> <span>National Research Council</span>, <span>Canada</span>, <span>SIM</span> </p> </td> </tr> </table> </div> </div> </div> </div> </div> <div id="print-out-popup" class="popup-action-notification print-out-popup mfp-hide"> <h1>Key and supplementary comparisons - Print out</h1> <div class="print-out-popup__content"> <p>This page proposes print-out on A4 paper (portrait) of the comparison details (best printed out using a black and white printer).</p> <p>Please, select items to be printed out, then click on "OK" :</p> <div class="print-out-form_inner-wrap"> <div class="print-out-form__checkbox-row" > <input type="checkbox" checked="checked" name="informationsAndContacts" class="reloadTable sections" id="informations_and_contacts" onclick="clearPrintOutError();"> <label for="informations_and_contacts"> <span>Information & contact</span> </label> </div> <div class="print-out-form__checkbox-row"> <input type="checkbox" checked="checked" name="participants" class="reloadTable sections" id="participants" onclick="clearPrintOutError();"> <label for="participants"> <span>Participants</span> </label> </div> <div class="print-out-form__checkbox-row" > <span>Results:</span> </div> <div class="print-out-form__checkbox-row _second-level"> <input type="checkbox" checked="checked" name="resultSections" class="reloadTable" id="result_section_0" value="675" onclick="clearPrintOutError();"> <label for="result_section_0"> <span>Estradiol</span> </label> </div> <div class="print-out-form__checkbox-row _second-level"> <input type="checkbox" checked="checked" name="resultSections" class="reloadTable" id="result_section_1" value="676" onclick="clearPrintOutError();"> <label for="result_section_1"> <span>Related Structure Impurities</span> </label> </div> <div class="print-out-form__checkbox-row _second-level"> <input type="checkbox" checked="checked" name="resultSections" class="reloadTable" id="result_section_2" value="677" onclick="clearPrintOutError();"> <label for="result_section_2"> <span>Water</span> </label> </div> <div class="print-out-form__checkbox-row _second-level"> <input type="checkbox" checked="checked" name="resultSections" class="reloadTable" id="result_section_3" value="678" onclick="clearPrintOutError();"> <label for="result_section_3"> <span>Volatile Organics</span> </label> </div> <div class="print-out-form__checkbox-row _second-level"> <input type="checkbox" checked="checked" name="resultSections" class="reloadTable" id="result_section_4" value="679" onclick="clearPrintOutError();"> <label for="result_section_4"> <span>Non-Volatile Content</span> </label> </div> <div class="print-out-form__btn-row"> <button onclick="printOutSubmit(); return false;" class="print-out-form__btn cmc-button submit">OK</button> </div> </div> </div> </div> </section> <section class="container tab-section" id="equivalenceStatementTab" > <div class="tab-section__left-sidebar sticky" id="selectSection"> <div class="information-list-wrap"> <div> <div class="tab-top__filter__wrapper"> <a class="mob-filter-btn" href="#">Comparison</a> <div class="mod-title mob-wrapper"> Comparison <a class="mob-close" href="#">close</a> </div> <div class="filter-wrapper mob-wrapper"> <div class="tab-top__filter__item"> <div class="filter__item__title">Results</div> <div class="filter__item__wrapper"> <ul id="sectionList" class="information-list"> <li id="section-id-675"> <a href="#tabsPage" onclick="sectionDetailTabsView.selectSection('675')">Estradiol</a> </li> <li id="section-id-676"> <a href="#tabsPage" onclick="sectionDetailTabsView.selectSection('676')">Related Structure Impurities</a> </li> <li id="section-id-677"> <a href="#tabsPage" onclick="sectionDetailTabsView.selectSection('677')">Water</a> </li> <li id="section-id-678"> <a href="#tabsPage" onclick="sectionDetailTabsView.selectSection('678')">Volatile Organics</a> </li> <li id="section-id-679"> <a href="#tabsPage" onclick="sectionDetailTabsView.selectSection('679')">Non-Volatile Content</a> </li> </ul> </div> </div> </div> </div> </div> </div> </div> <div class="tab-section__content" id="tab-section-675"> <div class="tab-section__content-heading tab-section__content-heading_description-tabs"> <div class="tab-section__title"></div> <div class="tab-btn__wrapper"> <a class="tab-btn print-out" href="#print-out-popup"> <img src="/kcdb/static/icons/print-out-26b37ecfd24015b0ce7c6017c52bb708.svg" alt=""> <span>print out</span> </a> </div> </div> <div class="info-block js-block-content"> <div class="result-description"><p><font class="Verdana_12px" color="#003399"><font class="standard_12px"><strong>MEASURAND : Mass fraction of Estradiol in the CCQM-K55.a samples</strong></font></font></p> <p></p> <p> </p><table border="0" cellspacing="0" cellpadding="0" width="100%" background="" bgcolor="#ffffff"> <tbody> <tr> <td> <p><font color="#ff0000"><font class="Verdana_12px">The key comparison reference value for the mass fraction of estradiol, <strong><em>x</em><sub>R</sub></strong>, was calculated by subtraction from the limit value of 1000 mg/g of the summation of the individual estimates for each contributing class of impurities present in CCQM-K55.a samples, as explained in page 21 of the <a class="bleu_12px" href="/kcdb/comparison/download/published-section-block-file/401/675/statement/675/ccqm-k55.a.pdf" target="_blank">Final Report</a>. <br />Its standard uncertainty, <strong><em>u</em><sub>R</sub></strong>, is computed by combination in quadrature of the uncertainties associated with each contributing impurity estimate and also uncertainties in the inter-unit homogeneity of water and related structure impurity content.<br /><strong><em>x</em><sub>R</sub> = 984.3 mg/g, <em>u</em><sub>R</sub> = 0.41 mg/g</strong></font></font></p></td></tr></tbody></table> <p> </p><table border="0" cellspacing="0" cellpadding="0" width="100%" background=""> <tbody> <tr> <td bgcolor="#e4fefe" background=""><font class="Verdana_12px">The degree of equivalence of laboratory <em><strong>i</strong></em> with respect to the key comparison reference value is given by a pair of terms: <strong><em>D<sub>i</sub></em> = (<em>x</em><em><sub>i</sub> </em>- <em>x</em><sub>R</sub>)</strong> and <em><strong>U<sub>i</sub></strong></em>, its expanded uncertainty (<em>k</em> = 2), both expressed in mg/g, with <strong><em>U<sub>i</sub></em> = 2(<em>u</em><sub><em>i</em></sub><sup>2</sup> + <em>u</em><sub>R</sub><sup>2</sup>)<sup>1/2</sup></strong>.</font></td></tr></tbody></table> <p> </p><table class="NOBORDER" border="0" cellspacing="0" cellpadding="0" width="100%" bgcolor="#ffffe7"> <tbody> <tr> <td><font class="Verdana_12px">No pair-wise degrees of equivalence are computed for this comparison.</font></td></tr></tbody></table></div> </div> </div> <div class="tab-section__content" id="tab-section-676"> <div class="tab-section__content-heading tab-section__content-heading_description-tabs"> <div class="tab-section__title"></div> <div class="tab-btn__wrapper"> <a class="tab-btn print-out" href="#print-out-popup"> <img src="/kcdb/static/icons/print-out-26b37ecfd24015b0ce7c6017c52bb708.svg" alt=""> <span>print out</span> </a> </div> </div> <div class="info-block js-block-content"> <div class="result-description"><p><font class="Verdana_12px" color="#003399"><font class="standard_12px"><strong>MEASURAND : Mass fraction of Related Structure Impurities in the CCQM-K55.a samples</strong></font></font></p> <p></p> <p> </p><table border="0" cellspacing="0" cellpadding="0" width="100%" background="" bgcolor="#ffffff"> <tbody> <tr> <td> <p><font color="#ff0000"><font class="Verdana_12px">Key comparison reference values (<strong><em>x</em><sub>R</sub></strong>) and associated standard uncertainty (<strong><em>u</em><sub>R</sub></strong>) were assigned for the mass fraction of each orthogonal impurity class - related substances, water, volatile organics and non-volatiles - quantified by the participants in CCQM-K55.a who used a mass balance approach to assign the estradiol content. <br />They are consensus values derived from the individual data supplied by each participant. The assignment method varied by impurity class and each is separately described on pages 17 to page 20 of the <a class="bleu_12px" href="/kcdb/comparison/download/published-section-block-file/401/676/statement/676/ccqm-k55.a.pdf" target="_blank">Final Report</a>.</font></font></p> <p><font color="#ff0000"><font class="Verdana_12px"><strong>For Total Related Structure Impurities,</strong> <strong><em>x</em><sub>R</sub> = 8.65 mg/g, <em>u</em><sub>R</sub> = 0.16 mg/g</strong></font></font></p></td></tr></tbody></table> <p> </p><table border="0" cellspacing="0" cellpadding="0" width="100%" background=""> <tbody> <tr> <td bgcolor="#e4fefe" background=""><font class="Verdana_12px">The degree of equivalence of laboratory <em><strong>i</strong></em> with respect to the key comparison reference value is given by a pair of terms: <strong><em>D<sub>i</sub></em> = (<em>x</em><em><sub>i</sub> </em>- <em>x</em><sub>R</sub>)</strong> and <em><strong>U<sub>i</sub></strong></em>, its expanded uncertainty (<em>k</em> = 2), both expressed in mg/g, with <strong><em>U<sub>i</sub></em> = 2(<em>u</em><sub><em>i</em></sub><sup>2</sup> + <em>u</em><sub>R</sub><sup>2</sup>)<sup>1/2</sup></strong>.</font></td></tr></tbody></table> <p> </p><table class="NOBORDER" border="0" cellspacing="0" cellpadding="0" width="100%" bgcolor="#ffffe7"> <tbody> <tr> <td><font class="Verdana_12px">No pair-wise degrees of equivalence are computed for this comparison.</font></td></tr></tbody></table></div> </div> </div> <div class="tab-section__content" id="tab-section-677"> <div class="tab-section__content-heading tab-section__content-heading_description-tabs"> <div class="tab-section__title"></div> <div class="tab-btn__wrapper"> <a class="tab-btn print-out" href="#print-out-popup"> <img src="/kcdb/static/icons/print-out-26b37ecfd24015b0ce7c6017c52bb708.svg" alt=""> <span>print out</span> </a> </div> </div> <div class="info-block js-block-content"> <div class="result-description"><p><font class="Verdana_12px" color="#003399"><font class="standard_12px"><strong>MEASURAND : Mass fraction of Water in the CCQM-K55.a samples</strong></font></font></p> <p></p> <p> </p><table border="0" cellspacing="0" cellpadding="0" width="100%" background="" bgcolor="#ffffff"> <tbody> <tr> <td> <p><font color="#ff0000"><font class="Verdana_12px">Key comparison reference values (<strong><em>x</em><sub>R</sub></strong>) and associated standard uncertainty (<strong><em>u</em><sub>R</sub></strong>) were assigned for the mass fraction of each orthogonal impurity class - related substances, water, volatile organics and non-volatiles - quantified by the participants in CCQM-K55.a who used a mass balance approach to assign the estradiol content. <br />They are consensus values derived from the individual data supplied by each participant. The assignment method varied by impurity class and each is separately described on pages 17 to page 20 of the <a class="bleu_12px" href="/kcdb/comparison/download/published-section-block-file/401/677/statement/677/ccqm-k55.a.pdf" target="_blank">Final Report</a>.</font></font></p> <p><font color="#ff0000"><font class="Verdana_12px"><strong>For Water,</strong> <strong><em>x</em><sub>R</sub> = 6.75 mg/g, <em>u</em><sub>R</sub> = 0.21 mg/g</strong></font></font></p></td></tr></tbody></table> <p> </p><table border="0" cellspacing="0" cellpadding="0" width="100%" background=""> <tbody> <tr> <td bgcolor="#e4fefe" background=""><font class="Verdana_12px">The degree of equivalence of laboratory <em><strong>i</strong></em> with respect to the key comparison reference value is given by a pair of terms: <strong><em>D<sub>i</sub></em> = (<em>x</em><em><sub>i</sub> </em>- <em>x</em><sub>R</sub>)</strong> and <em><strong>U<sub>i</sub></strong></em>, its expanded uncertainty (<em>k</em> = 2), both expressed in mg/g, with <strong><em>U<sub>i</sub></em> = 2(<em>u</em><sub><em>i</em></sub><sup>2</sup> + <em>u</em><sub>R</sub><sup>2</sup>)<sup>1/2</sup></strong>.</font></td></tr></tbody></table> <p> </p><table class="NOBORDER" border="0" cellspacing="0" cellpadding="0" width="100%" bgcolor="#ffffe7"> <tbody> <tr> <td><font class="Verdana_12px">No pair-wise degrees of equivalence are computed for this comparison.</font></td></tr></tbody></table></div> </div> </div> <div class="tab-section__content" id="tab-section-678"> <div class="tab-section__content-heading tab-section__content-heading_description-tabs"> <div class="tab-section__title"></div> <div class="tab-btn__wrapper"> <a class="tab-btn print-out" href="#print-out-popup"> <img src="/kcdb/static/icons/print-out-26b37ecfd24015b0ce7c6017c52bb708.svg" alt=""> <span>print out</span> </a> </div> </div> <div class="info-block js-block-content"> <div class="result-description"><p><font class="Verdana_12px" color="#003399"><font class="standard_12px"><strong>MEASURAND : Mass fraction of Volatile Organics in the CCQM-K55.a samples</strong></font></font></p> <p></p> <p> </p><table border="0" cellspacing="0" cellpadding="0" width="100%" background="" bgcolor="#ffffff"> <tbody> <tr> <td> <p><font color="#ff0000"><font class="Verdana_12px">Key comparison reference values (<strong><em>x</em><sub>R</sub></strong>) and associated standard uncertainty (<strong><em>u</em><sub>R</sub></strong>) were assigned for the mass fraction of each orthogonal impurity class - related substances, water, volatile organics and non-volatiles - quantified by the participants in CCQM-K55.a who used a mass balance approach to assign the estradiol content. <br />They are consensus values derived from the individual data supplied by each participant. The assignment method varied by impurity class and each is separately described on pages 17 to page 20 of the <a class="bleu_12px" href="/kcdb/comparison/download/published-section-block-file/401/678/statement/678/ccqm-k55.a.pdf" target="_blank">Final Report</a>.</font></font></p> <p><font color="#ff0000"><font class="Verdana_12px"><strong>For Volatile Organics,</strong> <strong><em>x</em><sub>R</sub> = 0.10 mg/g, <em>u</em><sub>R</sub> = 0.06 mg/g</strong></font></font></p></td></tr></tbody></table> <p> </p><table border="0" cellspacing="0" cellpadding="0" width="100%" background=""> <tbody> <tr> <td bgcolor="#e4fefe" background=""><font class="Verdana_12px">The degree of equivalence of laboratory <em><strong>i</strong></em> with respect to the key comparison reference value is given by a pair of terms: <strong><em>D<sub>i</sub></em> = (<em>x</em><em><sub>i</sub> </em>- <em>x</em><sub>R</sub>)</strong> and <em><strong>U<sub>i</sub></strong></em>, its expanded uncertainty (<em>k</em> = 2), both expressed in mg/g, with <strong><em>U<sub>i</sub></em> = 2(<em>u</em><sub><em>i</em></sub><sup>2</sup> + <em>u</em><sub>R</sub><sup>2</sup>)<sup>1/2</sup></strong>.</font></td></tr></tbody></table> <p> </p><table class="NOBORDER" border="0" cellspacing="0" cellpadding="0" width="100%" bgcolor="#ffffe7"> <tbody> <tr> <td><font class="Verdana_12px">No pair-wise degrees of equivalence are computed for this comparison.</font></td></tr></tbody></table></div> </div> </div> <div class="tab-section__content" id="tab-section-679"> <div class="tab-section__content-heading tab-section__content-heading_description-tabs"> <div class="tab-section__title"></div> <div class="tab-btn__wrapper"> <a class="tab-btn print-out" href="#print-out-popup"> <img src="/kcdb/static/icons/print-out-26b37ecfd24015b0ce7c6017c52bb708.svg" alt=""> <span>print out</span> </a> </div> </div> <div class="info-block js-block-content"> <div class="result-description"><p><font class="Verdana_12px" color="#003399"><font class="standard_12px"><strong>MEASURAND : Mass fraction of Non-Volatile Content in the CCQM-K55.a samples</strong></font></font></p> <p></p> <p> </p><table border="0" cellspacing="0" cellpadding="0" width="100%" background="" bgcolor="#ffffff"> <tbody> <tr> <td> <p><font color="#ff0000"><font class="Verdana_12px">Key comparison reference values (<strong><em>x</em><sub>R</sub></strong>) and associated standard uncertainty (<strong><em>u</em><sub>R</sub></strong>) were assigned for the mass fraction of each orthogonal impurity class - related substances, water, volatile organics and non-volatiles - quantified by the participants in CCQM-K55.a who used a mass balance approach to assign the estradiol content. <br />They are consensus values derived from the individual data supplied by each participant. The assignment method varied by impurity class and each is separately described on pages 17 to page 20 of the <a class="bleu_12px" href="/kcdb/comparison/download/published-section-block-file/401/679/statement/679/ccqm-k55.a.pdf" target="_blank">Final Report</a>.</font></font></p> <p><font color="#ff0000"><font class="Verdana_12px"><strong>For Non-Volatile Content,</strong> <strong><em>x</em><sub>R</sub> = 0.20 mg/g, <em>u</em><sub>R</sub> = 0.12 mg/g</strong></font></font></p></td></tr></tbody></table> <p> </p><table border="0" cellspacing="0" cellpadding="0" width="100%" background=""> <tbody> <tr> <td bgcolor="#e4fefe" background=""><font class="Verdana_12px">The degree of equivalence of laboratory <em><strong>i</strong></em> with respect to the key comparison reference value is given by a pair of terms: <strong><em>D<sub>i</sub></em> = (<em>x</em><em><sub>i</sub> </em>- <em>x</em><sub>R</sub>)</strong> and <em><strong>U<sub>i</sub></strong></em>, its expanded uncertainty (<em>k</em> = 2), both expressed in mg/g, with <strong><em>U<sub>i</sub></em> = 2(<em>u</em><sub><em>i</em></sub><sup>2</sup> + <em>u</em><sub>R</sub><sup>2</sup>)<sup>1/2</sup></strong>.</font></td></tr></tbody></table> <p> </p><table class="NOBORDER" border="0" cellspacing="0" cellpadding="0" width="100%" bgcolor="#ffffe7"> <tbody> <tr> <td><font class="Verdana_12px">No pair-wise degrees of equivalence are computed for this comparison.</font></td></tr></tbody></table></div> </div> </div> </section> <section class="container tab-section" id="laboratoryMeasurementTab"> <div class="tab-section__left-sidebar sticky" id="selectSection"> <div class="information-list-wrap"> <div> <div class="tab-top__filter__wrapper"> <a class="mob-filter-btn" href="#">Comparison</a> <div class="mod-title mob-wrapper"> Comparison <a class="mob-close" href="#">close</a> </div> <div class="filter-wrapper mob-wrapper"> <div class="tab-top__filter__item"> <div class="filter__item__title">Results</div> <div class="filter__item__wrapper"> <ul id="sectionList" class="information-list"> <li id="section-id-675"> <a href="#tabsPage" onclick="sectionDetailTabsView.selectSection('675')">Estradiol</a> </li> <li id="section-id-676"> <a href="#tabsPage" onclick="sectionDetailTabsView.selectSection('676')">Related Structure Impurities</a> </li> <li id="section-id-677"> <a href="#tabsPage" onclick="sectionDetailTabsView.selectSection('677')">Water</a> </li> <li id="section-id-678"> <a href="#tabsPage" onclick="sectionDetailTabsView.selectSection('678')">Volatile Organics</a> </li> <li id="section-id-679"> <a href="#tabsPage" onclick="sectionDetailTabsView.selectSection('679')">Non-Volatile Content</a> </li> </ul> </div> </div> </div> </div> </div> </div> </div> <div class="tab-section__content" id="tab-section-675"> <div class="tab-section__content-heading tab-section__content-heading_description-tabs"> <div class="tab-section__title"></div> <div class="tab-btn__wrapper"> <a class="tab-btn print-out" href="#print-out-popup"> <img src="/kcdb/static/icons/print-out-26b37ecfd24015b0ce7c6017c52bb708.svg" alt=""> <span>print out</span> </a> </div> </div> <div class="info-block js-block-content"> <div class="result-description"><p></p><p><font class="Verdana_12px" color="#003399"><font class="standard_12px"><strong>MEASURAND : Mass fraction of Estradiol in the CCQM-K55.a samples</strong></font></font></p><p></p><p><font class="Verdana_12px"><strong></strong><font color="#003399"><font class="standard_12px"><em>x</em><sub><em>i</em></sub> <font class="standard_12px">: result of measurement carried out by laboratory <em><strong>i</strong><br /></em><font class="Verdana_12px"><strong></strong><font color="#003399"><font class="standard_12px"><em>u</em><sub><em>i</em></sub><em> </em><font class="standard_12px">: combined standard uncertainty of <strong><em>x<sub>i</sub></em></strong></font></font></font></font></font></font></font></font></p><p><img border="0" src="/kcdb/comparison/download/published-section-block-file/401/675/measurement/675/ccqm-k55.a_lim_estradiol.gif" /></p><p></p></div> </div> </div> <div class="tab-section__content" id="tab-section-676"> <div class="tab-section__content-heading tab-section__content-heading_description-tabs"> <div class="tab-section__title"></div> <div class="tab-btn__wrapper"> <a class="tab-btn print-out" href="#print-out-popup"> <img src="/kcdb/static/icons/print-out-26b37ecfd24015b0ce7c6017c52bb708.svg" alt=""> <span>print out</span> </a> </div> </div> <div class="info-block js-block-content"> <div class="result-description"><p></p><p><font class="Verdana_12px" color="#003399"><font class="standard_12px"><strong>MEASURAND : Mass fraction of Related Structure Impurities in the CCQM-K55.a samples</strong></font></font></p><p></p><p><font class="Verdana_12px"><strong></strong><font color="#003399"><font class="standard_12px"><em>x</em><sub><em>i</em></sub> <font class="standard_12px">: result of measurement carried out by laboratory <em><strong>i</strong><br /></em><font class="Verdana_12px"><strong></strong><font color="#003399"><font class="standard_12px"><em>u</em><sub><em>i</em></sub><em> </em><font class="standard_12px">: combined standard uncertainty of <strong><em>x<sub>i</sub></em></strong></font></font></font></font></font></font></font></font></p><p><img border="0" src="/kcdb/comparison/download/published-section-block-file/401/676/measurement/676/ccqm-k55.a_lim_related_structure_impurities.gif" /></p><p></p></div> </div> </div> <div class="tab-section__content" id="tab-section-677"> <div class="tab-section__content-heading tab-section__content-heading_description-tabs"> <div class="tab-section__title"></div> <div class="tab-btn__wrapper"> <a class="tab-btn print-out" href="#print-out-popup"> <img src="/kcdb/static/icons/print-out-26b37ecfd24015b0ce7c6017c52bb708.svg" alt=""> <span>print out</span> </a> </div> </div> <div class="info-block js-block-content"> <div class="result-description"><p></p><p><font class="Verdana_12px" color="#003399"><font class="standard_12px"><strong>MEASURAND : Mass fraction of Water in the CCQM-K55.a samples</strong></font></font></p><p></p><p><font class="Verdana_12px"><strong></strong><font color="#003399"><font class="standard_12px"><em>x</em><sub><em>i</em></sub> <font class="standard_12px">: result of measurement carried out by laboratory <em><strong>i</strong><br /></em><font class="Verdana_12px"><strong></strong><font color="#003399"><font class="standard_12px"><em>u</em><sub><em>i</em></sub><em> </em><font class="standard_12px">: combined standard uncertainty of <strong><em>x<sub>i</sub></em></strong></font></font></font></font></font></font></font></font></p><p><img border="0" src="/kcdb/comparison/download/published-section-block-file/401/677/measurement/677/ccqm-k55.a_lim_water.gif" /></p><p></p></div> </div> </div> <div class="tab-section__content" id="tab-section-678"> <div class="tab-section__content-heading tab-section__content-heading_description-tabs"> <div class="tab-section__title"></div> <div class="tab-btn__wrapper"> <a class="tab-btn print-out" href="#print-out-popup"> <img src="/kcdb/static/icons/print-out-26b37ecfd24015b0ce7c6017c52bb708.svg" alt=""> <span>print out</span> </a> </div> </div> <div class="info-block js-block-content"> <div class="result-description"><p></p><p><font class="Verdana_12px" color="#003399"><font class="standard_12px"><strong>MEASURAND : Mass fraction of Volatile Organics in the CCQM-K55.a samples</strong></font></font></p><p></p><p><font class="Verdana_12px"><strong></strong><font color="#003399"><font class="standard_12px"><em>x</em><sub><em>i</em></sub> <font class="standard_12px">: result of measurement carried out by laboratory <em><strong>i</strong><br /></em><font class="Verdana_12px"><strong></strong><font color="#003399"><font class="standard_12px"><em>u</em><sub><em>i</em></sub><em> </em><font class="standard_12px">: combined standard uncertainty of <strong><em>x<sub>i</sub></em></strong></font></font></font></font></font></font></font></font></p><p><img border="0" src="/kcdb/comparison/download/published-section-block-file/401/678/measurement/678/ccqm-k55.a_lim_volatile_organics.gif" /></p><p></p></div> </div> </div> <div class="tab-section__content" id="tab-section-679"> <div class="tab-section__content-heading tab-section__content-heading_description-tabs"> <div class="tab-section__title"></div> <div class="tab-btn__wrapper"> <a class="tab-btn print-out" href="#print-out-popup"> <img src="/kcdb/static/icons/print-out-26b37ecfd24015b0ce7c6017c52bb708.svg" alt=""> <span>print out</span> </a> </div> </div> <div class="info-block js-block-content"> <div class="result-description"><p></p><p><font class="Verdana_12px" color="#003399"><font class="standard_12px"><strong>MEASURAND : Mass fraction of Non-Volatile Content in the CCQM-K55.a samples</strong></font></font></p><p></p><p><font class="Verdana_12px"><strong></strong><font color="#003399"><font class="standard_12px"><em>x</em><sub><em>i</em></sub> <font class="standard_12px">: result of measurement carried out by laboratory <em><strong>i</strong><br /></em><font class="Verdana_12px"><strong></strong><font color="#003399"><font class="standard_12px"><em>u</em><sub><em>i</em></sub><em> </em><font class="standard_12px">: combined standard uncertainty of <strong><em>x<sub>i</sub></em></strong></font></font></font></font></font></font></font></font></p><p><img border="0" src="/kcdb/comparison/download/published-section-block-file/401/679/measurement/679/ccqm-k55.a_lim_non_volatiles.gif" /></p><p></p></div> </div> </div> </section> </section> <footer class="ds-footer"> <section class="footer-section clearfix"> <div class="footer-section__top-section" id="accordion"> <div class="container"> <div class="row"> <div class="col-lg-12 col-md-12 col-sm-12 col-xs-12 clearfix 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ResultSectionDetailViewTabsService([{"id":675,"comparisonId":401,"name":"Estradiol","description":"Estradiol","degreesBlocks":[{"id":675,"sectionId":675,"mode":2,"descriptionBeforeTable":null,"descriptionAfterTable":null,"descriptionAfterGraph":null,"descriptionBeforeGraph":null,"descriptionDegrees":"<p><P><FONT class=Verdana_12px color=#003399><FONT class=standard_12px><STRONG>MEASURAND : Mass fraction of Estradiol in the CCQM-K55.a samples<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><\/P>\r\n<P><FONT color=#1e1182 face=Verdana><FONT class=standard_12px><STRONG>Degrees of equivalence : offset <EM>D<SUB>i<\/SUB><\/EM> and expanded uncertainty (<EM>k<\/EM> = 2) <EM>U<SUB>i<\/SUB><\/EM> expressed in mg\/g<BR><\/STRONG><\/FONT><\/FONT><FONT class=standard_12px><STRONG><EM>x<\/EM><SUB>R<\/SUB> = 984.3 mg\/g and 2 <EM>u<\/EM><SUB>R <\/SUB>= 0.8 mg\/g<\/STRONG><\/FONT><\/P>\r\n<P align=center><IMG border=0 src=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/675\/degree\/675\/ccqm-k55.a_does_estradiol.gif\"><\/P><\/p><p><table><tr><td><\/td><\/tr><\/table><\/p><p><P><FONT class=standard_12px>Results are presented under A4 printable format in <A class=bleu_12px href=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/675\/degree\/675\/ccqm-k55.a_aug12.pdf\" target=_blank>Summary Results<\/A> (PDF file).<\/FONT><\/P><\/p>","descriptionGraph":"<P><FONT class=Verdana_12px color=#003399><FONT class=standard_12px><STRONG>MEASURAND : Mass fraction of Estradiol in the CCQM-K55.a samples<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><\/P>\r\n<P><FONT color=#1e1182 face=Verdana><FONT class=standard_12px><STRONG>Degrees of equivalence : offset <EM>D<SUB>i<\/SUB><\/EM> and expanded uncertainty (<EM>k<\/EM> = 2) <EM>U<SUB>i<\/SUB><\/EM> expressed in mg\/g, and also in relative terms<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P align=center><IMG border=0 src=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/675\/degree\/675\/ccqm-k55.a_graph_estradiol.gif\"><\/P>\r\n<P align=left><FONT class=standard_12px><STRONG><EM>x<\/EM><SUB>R<\/SUB> = 984.3 mg\/g <BR>2 <EM>u<\/EM><SUB>R <\/SUB>= 0.8 mg\/g<\/STRONG><\/FONT><\/P>","unit":null,"dataFileName":null,"dataRows":[],"numericFormat":null,"xlegend":null,"ylegend":null}],"statements":[{"id":675,"description":"<P><FONT class=Verdana_12px color=#003399><FONT class=standard_12px><STRONG>MEASURAND : Mass fraction of Estradiol in the CCQM-K55.a samples<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><\/P>\r\n<P>\r\n<TABLE border=0 cellSpacing=0 cellPadding=0 width=\"100%\" background=\"\" bgColor=#ffffff>\r\n<TBODY>\r\n<TR>\r\n<TD>\r\n<P><FONT color=#ff0000><FONT class=Verdana_12px>The key comparison reference value for the mass fraction of estradiol, <STRONG><EM>x<\/EM><SUB>R<\/SUB><\/STRONG>, was calculated by subtraction from the limit value of 1000 mg\/g\u0026nbsp;of the summation of the individual estimates for each contributing class of impurities present in CCQM-K55.a samples, as explained in page 21 of the <A class=bleu_12px href=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/675\/statement\/675\/ccqm-k55.a.pdf\" target=_blank>Final Report<\/A>. <BR>Its standard uncertainty, <STRONG><EM>u<\/EM><SUB>R<\/SUB><\/STRONG>, is computed by combination in quadrature of the uncertainties associated with each contributing impurity estimate and also uncertainties in the inter-unit homogeneity of water and related structure impurity content.<BR><STRONG><EM>x<\/EM><SUB>R<\/SUB> = 984.3 mg\/g, <EM>u<\/EM><SUB>R<\/SUB> = 0.41 mg\/g<\/STRONG><\/FONT><\/FONT><\/P><\/TD><\/TR><\/TBODY><\/TABLE><\/P>\r\n<P>\r\n<TABLE border=0 cellSpacing=0 cellPadding=0 width=\"100%\" background=\"\">\r\n<TBODY>\r\n<TR>\r\n<TD bgColor=#e4fefe background=\"\"><FONT class=Verdana_12px>The degree of equivalence of laboratory <EM><STRONG>i<\/STRONG><\/EM> with respect to the key comparison reference value is given by a pair of terms: <STRONG><EM>D<SUB>i<\/SUB><\/EM> = (<EM>x<\/EM><EM><SUB>i<\/SUB> <\/EM>- <EM>x<\/EM><SUB>R<\/SUB>)<\/STRONG> and <EM><STRONG>U<SUB>i<\/SUB><\/STRONG><\/EM>, its expanded uncertainty (<EM>k<\/EM> = 2), both expressed in mg\/g, with <STRONG><EM>U<SUB>i<\/SUB><\/EM> = 2(<EM>u<\/EM><SUB><EM>i<\/EM><\/SUB><SUP>2<\/SUP> + <EM>u<\/EM><SUB>R<\/SUB><SUP>2<\/SUP>)<SUP>1\/2<\/SUP><\/STRONG>.<\/FONT><\/TD><\/TR><\/TBODY><\/TABLE><\/P>\r\n<P>\r\n<TABLE class=NOBORDER border=0 cellSpacing=0 cellPadding=0 width=\"100%\" bgColor=#ffffe7>\r\n<TBODY>\r\n<TR>\r\n<TD><FONT class=Verdana_12px>No pair-wise degrees of equivalence are computed for this comparison.<\/FONT><\/TD><\/TR><\/TBODY><\/TABLE><\/P>","sectionId":675}],"measurements":[{"id":675,"description":"<p><P><FONT class=Verdana_12px color=#003399><FONT class=standard_12px><STRONG>MEASURAND : Mass fraction of Estradiol in the CCQM-K55.a samples<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><\/P>\r\n<P><FONT class=Verdana_12px><STRONG><FONT color=#003399><FONT class=standard_12px><EM>x<\/EM><SUB><EM>i<\/EM><\/SUB><\/FONT><\/FONT><\/STRONG> <FONT class=standard_12px>: result of measurement carried out by laboratory <EM><STRONG>i<\/STRONG><BR><\/EM><\/FONT><\/FONT><FONT class=Verdana_12px><STRONG><FONT color=#003399><FONT class=standard_12px><EM>u<\/EM><SUB><EM>i<\/EM><\/SUB><\/FONT><\/FONT><EM> <\/EM><\/STRONG><FONT class=standard_12px>: combined standard uncertainty of <STRONG><EM>x<SUB>i<\/SUB><\/EM><\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><IMG border=0 src=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/675\/measurement\/675\/ccqm-k55.a_lim_estradiol.gif\"><\/P><\/p><p><\/p>","sectionId":675}]},{"id":676,"comparisonId":401,"name":"Related Structure Impurities","description":"Related Structure Impurities","degreesBlocks":[{"id":676,"sectionId":676,"mode":2,"descriptionBeforeTable":null,"descriptionAfterTable":null,"descriptionAfterGraph":null,"descriptionBeforeGraph":null,"descriptionDegrees":"<p><P><FONT class=Verdana_12px color=#003399><FONT class=standard_12px><STRONG>MEASURAND : Mass fraction of Related Structure Impurities in the CCQM-K55.a samples<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><\/P>\r\n<P><FONT color=#1e1182 face=Verdana><FONT class=standard_12px><STRONG>Degrees of equivalence : offset <EM>D<SUB>i<\/SUB><\/EM> and expanded uncertainty (<EM>k<\/EM> = 2) <EM>U<SUB>i<\/SUB><\/EM> expressed in mg\/g<BR><\/STRONG><\/FONT><\/FONT><FONT class=standard_12px><STRONG><EM>x<\/EM><SUB>R<\/SUB> = 8.65 mg\/g and 2 <EM>u<\/EM><SUB>R <\/SUB>= 0.32 mg\/g<\/STRONG><\/FONT><\/P>\r\n<P align=center><IMG border=0 src=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/676\/degree\/676\/ccqm-k55.a_does_related_structure_impurities.gif\"><\/P><\/p><p><table><tr><td><\/td><\/tr><\/table><\/p><p><P><FONT class=standard_12px>Results are presented under A4 printable format in <A class=bleu_12px href=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/676\/degree\/676\/ccqm-k55.a_aug12.pdf\" target=_blank>Summary Results<\/A> (PDF file).<\/FONT><\/P><\/p>","descriptionGraph":"<P><FONT class=Verdana_12px color=#003399><FONT class=standard_12px><STRONG>MEASURAND : Mass fraction of Related Structure Impurities in the CCQM-K55.a samples<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><\/P>\r\n<P><FONT color=#1e1182 face=Verdana><FONT class=standard_12px><STRONG>Degrees of equivalence : offset <EM>D<SUB>i<\/SUB><\/EM> and expanded uncertainty (<EM>k<\/EM> = 2) <EM>U<SUB>i<\/SUB><\/EM> expressed in mg\/g, and also in relative terms<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P align=center><IMG border=0 src=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/676\/degree\/676\/ccqm-k55.a_graph_related_structure_impurities.gif\"><\/P>\r\n<P align=left><FONT class=standard_12px><STRONG><EM>x<\/EM><SUB>R<\/SUB> = 8.65 mg\/g <BR>2 <EM>u<\/EM><SUB>R <\/SUB>= 0.32 mg\/g<\/STRONG><\/FONT><\/P>","unit":null,"dataFileName":null,"dataRows":[],"numericFormat":null,"xlegend":null,"ylegend":null}],"statements":[{"id":676,"description":"<P><FONT class=Verdana_12px color=#003399><FONT class=standard_12px><STRONG>MEASURAND : Mass fraction of Related Structure Impurities in the CCQM-K55.a samples<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><\/P>\r\n<P>\r\n<TABLE border=0 cellSpacing=0 cellPadding=0 width=\"100%\" background=\"\" bgColor=#ffffff>\r\n<TBODY>\r\n<TR>\r\n<TD>\r\n<P><FONT color=#ff0000><FONT class=Verdana_12px>Key comparison reference values (<STRONG><EM>x<\/EM><SUB>R<\/SUB><\/STRONG>) and associated standard uncertainty (<STRONG><EM>u<\/EM><SUB>R<\/SUB><\/STRONG>) were assigned for the mass fraction of each orthogonal impurity class -\u0026nbsp; related substances, water, volatile organics and non-volatiles - quantified by the participants in CCQM-K55.a who used a mass balance approach to assign the estradiol content. <BR>They are consensus values derived from the individual data supplied by each participant. The assignment method varied by impurity class and each is separately described on pages 17 to page 20 of the <A class=bleu_12px href=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/676\/statement\/676\/ccqm-k55.a.pdf\" target=_blank>Final Report<\/A>.<\/FONT><\/FONT><\/P>\r\n<P><FONT color=#ff0000><FONT class=Verdana_12px><STRONG>For Total Related Structure Impurities,<\/STRONG> <STRONG><EM>x<\/EM><SUB>R<\/SUB> = 8.65 mg\/g, <EM>u<\/EM><SUB>R<\/SUB> = 0.16 mg\/g<\/STRONG><\/FONT><\/FONT><\/P><\/TD><\/TR><\/TBODY><\/TABLE><\/P>\r\n<P>\r\n<TABLE border=0 cellSpacing=0 cellPadding=0 width=\"100%\" background=\"\">\r\n<TBODY>\r\n<TR>\r\n<TD bgColor=#e4fefe background=\"\"><FONT class=Verdana_12px>The degree of equivalence of laboratory <EM><STRONG>i<\/STRONG><\/EM> with respect to the key comparison reference value is given by a pair of terms: <STRONG><EM>D<SUB>i<\/SUB><\/EM> = (<EM>x<\/EM><EM><SUB>i<\/SUB> <\/EM>- <EM>x<\/EM><SUB>R<\/SUB>)<\/STRONG> and <EM><STRONG>U<SUB>i<\/SUB><\/STRONG><\/EM>, its expanded uncertainty (<EM>k<\/EM> = 2), both expressed in mg\/g, with <STRONG><EM>U<SUB>i<\/SUB><\/EM> = 2(<EM>u<\/EM><SUB><EM>i<\/EM><\/SUB><SUP>2<\/SUP> + <EM>u<\/EM><SUB>R<\/SUB><SUP>2<\/SUP>)<SUP>1\/2<\/SUP><\/STRONG>.<\/FONT><\/TD><\/TR><\/TBODY><\/TABLE><\/P>\r\n<P>\r\n<TABLE class=NOBORDER border=0 cellSpacing=0 cellPadding=0 width=\"100%\" bgColor=#ffffe7>\r\n<TBODY>\r\n<TR>\r\n<TD><FONT class=Verdana_12px>No pair-wise degrees of equivalence are computed for this comparison.<\/FONT><\/TD><\/TR><\/TBODY><\/TABLE><\/P>","sectionId":676}],"measurements":[{"id":676,"description":"<p><P><FONT class=Verdana_12px color=#003399><FONT class=standard_12px><STRONG>MEASURAND : Mass fraction of Related Structure Impurities in the CCQM-K55.a samples<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><\/P>\r\n<P><FONT class=Verdana_12px><STRONG><FONT color=#003399><FONT class=standard_12px><EM>x<\/EM><SUB><EM>i<\/EM><\/SUB><\/FONT><\/FONT><\/STRONG> <FONT class=standard_12px>: result of measurement carried out by laboratory <EM><STRONG>i<\/STRONG><BR><\/EM><\/FONT><\/FONT><FONT class=Verdana_12px><STRONG><FONT color=#003399><FONT class=standard_12px><EM>u<\/EM><SUB><EM>i<\/EM><\/SUB><\/FONT><\/FONT><EM> <\/EM><\/STRONG><FONT class=standard_12px>: combined standard uncertainty of <STRONG><EM>x<SUB>i<\/SUB><\/EM><\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><IMG border=0 src=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/676\/measurement\/676\/ccqm-k55.a_lim_related_structure_impurities.gif\"><\/P><\/p><p><\/p>","sectionId":676}]},{"id":677,"comparisonId":401,"name":"Water","description":"Water","degreesBlocks":[{"id":677,"sectionId":677,"mode":2,"descriptionBeforeTable":null,"descriptionAfterTable":null,"descriptionAfterGraph":null,"descriptionBeforeGraph":null,"descriptionDegrees":"<p><P><FONT class=Verdana_12px color=#003399><FONT class=standard_12px><STRONG>MEASURAND : Mass fraction of Water in the CCQM-K55.a samples<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><\/P>\r\n<P><FONT color=#1e1182 face=Verdana><FONT class=standard_12px><STRONG>Degrees of equivalence : offset <EM>D<SUB>i<\/SUB><\/EM> and expanded uncertainty (<EM>k<\/EM> = 2) <EM>U<SUB>i<\/SUB><\/EM> expressed in mg\/g<BR><\/STRONG><\/FONT><\/FONT><FONT class=standard_12px><STRONG><EM>x<\/EM><SUB>R<\/SUB> = 6.75 mg\/g and 2 <EM>u<\/EM><SUB>R <\/SUB>= 0.42 mg\/g<\/STRONG><\/FONT><\/P>\r\n<P align=center><IMG border=0 src=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/677\/degree\/677\/ccqm-k55.a_does_water.gif\"><\/P><\/p><p><table><tr><td><\/td><\/tr><\/table><\/p><p><P><FONT class=standard_12px>Results are presented under A4 printable format in <A class=bleu_12px href=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/677\/degree\/677\/ccqm-k55.a_aug12.pdf\" target=_blank>Summary Results<\/A> (PDF file).<\/FONT><\/P><\/p>","descriptionGraph":"<P><FONT class=Verdana_12px color=#003399><FONT class=standard_12px><STRONG>MEASURAND : Mass fraction of Water in the CCQM-K55.a samples<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><\/P>\r\n<P><FONT color=#1e1182 face=Verdana><FONT class=standard_12px><STRONG>Degrees of equivalence : offset <EM>D<SUB>i<\/SUB><\/EM> and expanded uncertainty (<EM>k<\/EM> = 2) <EM>U<SUB>i<\/SUB><\/EM> expressed in mg\/g, and also in relative terms<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P align=center><IMG border=0 src=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/677\/degree\/677\/ccqm-k55.a_graph_water.gif\"><\/P>\r\n<P align=left><FONT class=standard_12px><STRONG><EM>x<\/EM><SUB>R<\/SUB> = 6.75 mg\/g <BR>2 <EM>u<\/EM><SUB>R <\/SUB>= 0.42 mg\/g<\/STRONG><\/FONT><\/P>","unit":null,"dataFileName":null,"dataRows":[],"numericFormat":null,"xlegend":null,"ylegend":null}],"statements":[{"id":677,"description":"<P><FONT class=Verdana_12px color=#003399><FONT class=standard_12px><STRONG>MEASURAND : Mass fraction of Water in the CCQM-K55.a samples<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><\/P>\r\n<P>\r\n<TABLE border=0 cellSpacing=0 cellPadding=0 width=\"100%\" background=\"\" bgColor=#ffffff>\r\n<TBODY>\r\n<TR>\r\n<TD>\r\n<P><FONT color=#ff0000><FONT class=Verdana_12px>Key comparison reference values (<STRONG><EM>x<\/EM><SUB>R<\/SUB><\/STRONG>) and associated standard uncertainty (<STRONG><EM>u<\/EM><SUB>R<\/SUB><\/STRONG>) were assigned for the mass fraction of each orthogonal impurity class - related substances, water, volatile organics and non-volatiles - quantified by the participants in CCQM-K55.a who used a mass balance approach to assign the estradiol content. <BR>They are consensus values derived from the individual data supplied by each participant. The assignment method varied by impurity class and each is separately described on pages 17 to page 20 of the <A class=bleu_12px href=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/677\/statement\/677\/ccqm-k55.a.pdf\" target=_blank>Final Report<\/A>.<\/FONT><\/FONT><\/P>\r\n<P><FONT color=#ff0000><FONT class=Verdana_12px><STRONG>For Water,<\/STRONG> <STRONG><EM>x<\/EM><SUB>R<\/SUB> = 6.75 mg\/g, <EM>u<\/EM><SUB>R<\/SUB> = 0.21 mg\/g<\/STRONG><\/FONT><\/FONT><\/P><\/TD><\/TR><\/TBODY><\/TABLE><\/P>\r\n<P>\r\n<TABLE border=0 cellSpacing=0 cellPadding=0 width=\"100%\" background=\"\">\r\n<TBODY>\r\n<TR>\r\n<TD bgColor=#e4fefe background=\"\"><FONT class=Verdana_12px>The degree of equivalence of laboratory <EM><STRONG>i<\/STRONG><\/EM> with respect to the key comparison reference value is given by a pair of terms: <STRONG><EM>D<SUB>i<\/SUB><\/EM> = (<EM>x<\/EM><EM><SUB>i<\/SUB> <\/EM>- <EM>x<\/EM><SUB>R<\/SUB>)<\/STRONG> and <EM><STRONG>U<SUB>i<\/SUB><\/STRONG><\/EM>, its expanded uncertainty (<EM>k<\/EM> = 2), both expressed in mg\/g, with <STRONG><EM>U<SUB>i<\/SUB><\/EM> = 2(<EM>u<\/EM><SUB><EM>i<\/EM><\/SUB><SUP>2<\/SUP> + <EM>u<\/EM><SUB>R<\/SUB><SUP>2<\/SUP>)<SUP>1\/2<\/SUP><\/STRONG>.<\/FONT><\/TD><\/TR><\/TBODY><\/TABLE><\/P>\r\n<P>\r\n<TABLE class=NOBORDER border=0 cellSpacing=0 cellPadding=0 width=\"100%\" bgColor=#ffffe7>\r\n<TBODY>\r\n<TR>\r\n<TD><FONT class=Verdana_12px>No pair-wise degrees of equivalence are computed for this comparison.<\/FONT><\/TD><\/TR><\/TBODY><\/TABLE><\/P>","sectionId":677}],"measurements":[{"id":677,"description":"<p><P><FONT class=Verdana_12px color=#003399><FONT class=standard_12px><STRONG>MEASURAND : Mass fraction of Water in the CCQM-K55.a samples<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><\/P>\r\n<P><FONT class=Verdana_12px><STRONG><FONT color=#003399><FONT class=standard_12px><EM>x<\/EM><SUB><EM>i<\/EM><\/SUB><\/FONT><\/FONT><\/STRONG> <FONT class=standard_12px>: result of measurement carried out by laboratory <EM><STRONG>i<\/STRONG><BR><\/EM><\/FONT><\/FONT><FONT class=Verdana_12px><STRONG><FONT color=#003399><FONT class=standard_12px><EM>u<\/EM><SUB><EM>i<\/EM><\/SUB><\/FONT><\/FONT><EM> <\/EM><\/STRONG><FONT class=standard_12px>: combined standard uncertainty of <STRONG><EM>x<SUB>i<\/SUB><\/EM><\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><IMG border=0 src=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/677\/measurement\/677\/ccqm-k55.a_lim_water.gif\"><\/P><\/p><p><\/p>","sectionId":677}]},{"id":678,"comparisonId":401,"name":"Volatile Organics","description":"Volatile Organics","degreesBlocks":[{"id":678,"sectionId":678,"mode":2,"descriptionBeforeTable":null,"descriptionAfterTable":null,"descriptionAfterGraph":null,"descriptionBeforeGraph":null,"descriptionDegrees":"<p><P><FONT class=Verdana_12px color=#003399><FONT class=standard_12px><STRONG>MEASURAND : Mass fraction of Volatile Organics in the CCQM-K55.a samples<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><\/P>\r\n<P><FONT color=#1e1182 face=Verdana><FONT class=standard_12px><STRONG>Degrees of equivalence : offset <EM>D<SUB>i<\/SUB><\/EM> and expanded uncertainty (<EM>k<\/EM> = 2) <EM>U<SUB>i<\/SUB><\/EM> expressed in mg\/g<BR><\/STRONG><\/FONT><\/FONT><FONT class=standard_12px><STRONG><EM>x<\/EM><SUB>R<\/SUB> = 0.10 mg\/g and 2 <EM>u<\/EM><SUB>R <\/SUB>= 0.12 mg\/g<\/STRONG><\/FONT><\/P>\r\n<P align=center><IMG border=0 src=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/678\/degree\/678\/ccqm-k55.a_does_volatile_organics.gif\"><\/P><\/p><p><table><tr><td><\/td><\/tr><\/table><\/p><p><P><FONT class=standard_12px>Results are presented under A4 printable format in <A class=bleu_12px href=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/678\/degree\/678\/ccqm-k55.a_aug12.pdf\" target=_blank>Summary Results<\/A> (PDF file).<\/FONT><\/P><\/p>","descriptionGraph":"<P><FONT class=Verdana_12px color=#003399><FONT class=standard_12px><STRONG>MEASURAND : Mass fraction of Volatile Organics in the CCQM-K55.a samples<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><\/P>\r\n<P><FONT color=#1e1182 face=Verdana><FONT class=standard_12px><STRONG>Degrees of equivalence : offset <EM>D<SUB>i<\/SUB><\/EM> and expanded uncertainty (<EM>k<\/EM> = 2) <EM>U<SUB>i<\/SUB><\/EM> expressed in mg\/g, and also in relative terms<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P align=center><IMG border=0 src=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/678\/degree\/678\/ccqm-k55.a_graph_volatile_organics.gif\"><\/P>\r\n<P align=left><FONT class=standard_12px><STRONG><EM>x<\/EM><SUB>R<\/SUB> = 0.10 mg\/g <BR>2 <EM>u<\/EM><SUB>R <\/SUB>= 0.12 mg\/g<\/STRONG><\/FONT><\/P>","unit":null,"dataFileName":null,"dataRows":[],"numericFormat":null,"xlegend":null,"ylegend":null}],"statements":[{"id":678,"description":"<P><FONT class=Verdana_12px color=#003399><FONT class=standard_12px><STRONG>MEASURAND : Mass fraction of Volatile Organics in the CCQM-K55.a samples<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><\/P>\r\n<P>\r\n<TABLE border=0 cellSpacing=0 cellPadding=0 width=\"100%\" background=\"\" bgColor=#ffffff>\r\n<TBODY>\r\n<TR>\r\n<TD>\r\n<P><FONT color=#ff0000><FONT class=Verdana_12px>Key comparison reference values (<STRONG><EM>x<\/EM><SUB>R<\/SUB><\/STRONG>) and associated standard uncertainty (<STRONG><EM>u<\/EM><SUB>R<\/SUB><\/STRONG>) were assigned for the mass fraction of each orthogonal impurity class - related substances, water, volatile organics and non-volatiles - quantified by the participants in CCQM-K55.a who used a mass balance approach to assign the estradiol content. <BR>They are consensus values derived from the individual data supplied by each participant. The assignment method varied by impurity class and each is separately described on pages 17 to page 20 of the <A class=bleu_12px href=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/678\/statement\/678\/ccqm-k55.a.pdf\" target=_blank>Final Report<\/A>.<\/FONT><\/FONT><\/P>\r\n<P><FONT color=#ff0000><FONT class=Verdana_12px><STRONG>For Volatile Organics,<\/STRONG> <STRONG><EM>x<\/EM><SUB>R<\/SUB> = 0.10 mg\/g, <EM>u<\/EM><SUB>R<\/SUB> = 0.06 mg\/g<\/STRONG><\/FONT><\/FONT><\/P><\/TD><\/TR><\/TBODY><\/TABLE><\/P>\r\n<P>\r\n<TABLE border=0 cellSpacing=0 cellPadding=0 width=\"100%\" background=\"\">\r\n<TBODY>\r\n<TR>\r\n<TD bgColor=#e4fefe background=\"\"><FONT class=Verdana_12px>The degree of equivalence of laboratory <EM><STRONG>i<\/STRONG><\/EM> with respect to the key comparison reference value is given by a pair of terms: <STRONG><EM>D<SUB>i<\/SUB><\/EM> = (<EM>x<\/EM><EM><SUB>i<\/SUB> <\/EM>- <EM>x<\/EM><SUB>R<\/SUB>)<\/STRONG> and <EM><STRONG>U<SUB>i<\/SUB><\/STRONG><\/EM>, its expanded uncertainty (<EM>k<\/EM> = 2), both expressed in mg\/g, with <STRONG><EM>U<SUB>i<\/SUB><\/EM> = 2(<EM>u<\/EM><SUB><EM>i<\/EM><\/SUB><SUP>2<\/SUP> + <EM>u<\/EM><SUB>R<\/SUB><SUP>2<\/SUP>)<SUP>1\/2<\/SUP><\/STRONG>.<\/FONT><\/TD><\/TR><\/TBODY><\/TABLE><\/P>\r\n<P>\r\n<TABLE class=NOBORDER border=0 cellSpacing=0 cellPadding=0 width=\"100%\" bgColor=#ffffe7>\r\n<TBODY>\r\n<TR>\r\n<TD><FONT class=Verdana_12px>No pair-wise degrees of equivalence are computed for this comparison.<\/FONT><\/TD><\/TR><\/TBODY><\/TABLE><\/P>","sectionId":678}],"measurements":[{"id":678,"description":"<p><P><FONT class=Verdana_12px color=#003399><FONT class=standard_12px><STRONG>MEASURAND : Mass fraction of Volatile Organics in the CCQM-K55.a samples<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><\/P>\r\n<P><FONT class=Verdana_12px><STRONG><FONT color=#003399><FONT class=standard_12px><EM>x<\/EM><SUB><EM>i<\/EM><\/SUB><\/FONT><\/FONT><\/STRONG> <FONT class=standard_12px>: result of measurement carried out by laboratory <EM><STRONG>i<\/STRONG><BR><\/EM><\/FONT><\/FONT><FONT class=Verdana_12px><STRONG><FONT color=#003399><FONT class=standard_12px><EM>u<\/EM><SUB><EM>i<\/EM><\/SUB><\/FONT><\/FONT><EM> <\/EM><\/STRONG><FONT class=standard_12px>: combined standard uncertainty of <STRONG><EM>x<SUB>i<\/SUB><\/EM><\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><IMG border=0 src=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/678\/measurement\/678\/ccqm-k55.a_lim_volatile_organics.gif\"><\/P><\/p><p><\/p>","sectionId":678}]},{"id":679,"comparisonId":401,"name":"Non-Volatile Content","description":"Non-Volatile Content","degreesBlocks":[{"id":679,"sectionId":679,"mode":2,"descriptionBeforeTable":null,"descriptionAfterTable":null,"descriptionAfterGraph":null,"descriptionBeforeGraph":null,"descriptionDegrees":"<p><P><FONT class=Verdana_12px color=#003399><FONT class=standard_12px><STRONG>MEASURAND : Mass fraction of Non-Volatile Content in the CCQM-K55.a samples<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><\/P>\r\n<P><FONT color=#1e1182 face=Verdana><FONT class=standard_12px><STRONG>Degrees of equivalence : offset <EM>D<SUB>i<\/SUB><\/EM> and expanded uncertainty (<EM>k<\/EM> = 2) <EM>U<SUB>i<\/SUB><\/EM> expressed in mg\/g<BR><\/STRONG><\/FONT><\/FONT><FONT class=standard_12px><STRONG><EM>x<\/EM><SUB>R<\/SUB> = 0.20 mg\/g and 2 <EM>u<\/EM><SUB>R <\/SUB>= 0.24 mg\/g<\/STRONG><\/FONT><\/P>\r\n<P align=center><IMG border=0 src=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/679\/degree\/679\/ccqm-k55.a_does_non_volatiles.gif\"><\/P><\/p><p><table><tr><td><\/td><\/tr><\/table><\/p><p><P><FONT class=standard_12px>Results are presented under A4 printable format in <A class=bleu_12px href=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/679\/degree\/679\/ccqm-k55.a_aug12.pdf\" target=_blank>Summary Results<\/A> (PDF file).<\/FONT><\/P><\/p>","descriptionGraph":"<P><FONT class=Verdana_12px color=#003399><FONT class=standard_12px><STRONG>MEASURAND : Mass fraction of Non-Volatile Content in the CCQM-K55.a samples<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><\/P>\r\n<P><FONT color=#1e1182 face=Verdana><FONT class=standard_12px><STRONG>Degrees of equivalence : offset <EM>D<SUB>i<\/SUB><\/EM> and expanded uncertainty (<EM>k<\/EM> = 2) <EM>U<SUB>i<\/SUB><\/EM> expressed in mg\/g, and also in relative terms<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P align=center><IMG border=0 src=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/679\/degree\/679\/ccqm-k55.a_graph_non_volatiles.gif\"><\/P>\r\n<P align=left><FONT class=standard_12px><STRONG><EM>x<\/EM><SUB>R<\/SUB> = 0.20 mg\/g <BR>2 <EM>u<\/EM><SUB>R <\/SUB>= 0.24 mg\/g<\/STRONG><\/FONT><\/P>","unit":null,"dataFileName":null,"dataRows":[],"numericFormat":null,"xlegend":null,"ylegend":null}],"statements":[{"id":679,"description":"<P><FONT class=Verdana_12px color=#003399><FONT class=standard_12px><STRONG>MEASURAND : Mass fraction of Non-Volatile Content in the CCQM-K55.a samples<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><\/P>\r\n<P>\r\n<TABLE border=0 cellSpacing=0 cellPadding=0 width=\"100%\" background=\"\" bgColor=#ffffff>\r\n<TBODY>\r\n<TR>\r\n<TD>\r\n<P><FONT color=#ff0000><FONT class=Verdana_12px>Key comparison reference values (<STRONG><EM>x<\/EM><SUB>R<\/SUB><\/STRONG>) and associated standard uncertainty (<STRONG><EM>u<\/EM><SUB>R<\/SUB><\/STRONG>) were assigned for the mass fraction of each orthogonal impurity class - related substances, water, volatile organics and non-volatiles - quantified by the participants in CCQM-K55.a who used a mass balance approach to assign the estradiol content. <BR>They are consensus values derived from the individual data supplied by each participant. The assignment method varied by impurity class and each is separately described on pages 17 to page 20 of the <A class=bleu_12px href=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/679\/statement\/679\/ccqm-k55.a.pdf\" target=_blank>Final Report<\/A>.<\/FONT><\/FONT><\/P>\r\n<P><FONT color=#ff0000><FONT class=Verdana_12px><STRONG>For Non-Volatile Content,<\/STRONG> <STRONG><EM>x<\/EM><SUB>R<\/SUB> = 0.20 mg\/g, <EM>u<\/EM><SUB>R<\/SUB> = 0.12 mg\/g<\/STRONG><\/FONT><\/FONT><\/P><\/TD><\/TR><\/TBODY><\/TABLE><\/P>\r\n<P>\r\n<TABLE border=0 cellSpacing=0 cellPadding=0 width=\"100%\" background=\"\">\r\n<TBODY>\r\n<TR>\r\n<TD bgColor=#e4fefe background=\"\"><FONT class=Verdana_12px>The degree of equivalence of laboratory <EM><STRONG>i<\/STRONG><\/EM> with respect to the key comparison reference value is given by a pair of terms: <STRONG><EM>D<SUB>i<\/SUB><\/EM> = (<EM>x<\/EM><EM><SUB>i<\/SUB> <\/EM>- <EM>x<\/EM><SUB>R<\/SUB>)<\/STRONG> and <EM><STRONG>U<SUB>i<\/SUB><\/STRONG><\/EM>, its expanded uncertainty (<EM>k<\/EM> = 2), both expressed in mg\/g, with <STRONG><EM>U<SUB>i<\/SUB><\/EM> = 2(<EM>u<\/EM><SUB><EM>i<\/EM><\/SUB><SUP>2<\/SUP> + <EM>u<\/EM><SUB>R<\/SUB><SUP>2<\/SUP>)<SUP>1\/2<\/SUP><\/STRONG>.<\/FONT><\/TD><\/TR><\/TBODY><\/TABLE><\/P>\r\n<P>\r\n<TABLE class=NOBORDER border=0 cellSpacing=0 cellPadding=0 width=\"100%\" bgColor=#ffffe7>\r\n<TBODY>\r\n<TR>\r\n<TD><FONT class=Verdana_12px>No pair-wise degrees of equivalence are computed for this comparison.<\/FONT><\/TD><\/TR><\/TBODY><\/TABLE><\/P>","sectionId":679}],"measurements":[{"id":679,"description":"<p><P><FONT class=Verdana_12px color=#003399><FONT class=standard_12px><STRONG>MEASURAND : Mass fraction of Non-Volatile Content in the CCQM-K55.a samples<\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><\/P>\r\n<P><FONT class=Verdana_12px><STRONG><FONT color=#003399><FONT class=standard_12px><EM>x<\/EM><SUB><EM>i<\/EM><\/SUB><\/FONT><\/FONT><\/STRONG> <FONT class=standard_12px>: result of measurement carried out by laboratory <EM><STRONG>i<\/STRONG><BR><\/EM><\/FONT><\/FONT><FONT class=Verdana_12px><STRONG><FONT color=#003399><FONT class=standard_12px><EM>u<\/EM><SUB><EM>i<\/EM><\/SUB><\/FONT><\/FONT><EM> <\/EM><\/STRONG><FONT class=standard_12px>: combined standard uncertainty of <STRONG><EM>x<SUB>i<\/SUB><\/EM><\/STRONG><\/FONT><\/FONT><\/P>\r\n<P><IMG border=0 src=\"\/kcdb\/comparison\/download\/published-section-block-file\/401\/679\/measurement\/679\/ccqm-k55.a_lim_non_volatiles.gif\"><\/P><\/p><p><\/p>","sectionId":679}]}]); 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