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The conference participants had the opportunity to submit written questions as well as to ask ad-hoc questions during the session, which were to be answered by a panel of qNMR experts from several application fields. This article provides an edited and referenced transcript of the session. The major topics were centred on instrumental requirements for qNMR, and the participants were in agreement that modern digital NMR spectrometers guarantee a long-term stability of measurements and calibrations, sometimes over several years. However, the panel also agreed that method validation is an absolute necessity in qNMR as in every other field of quantitative analytical chemistry. Validation strategies may depend on the purpose of the method and vary between multi-component analyses of foods and beverages, compared to single target assays e.g. in verification of reference standards. Approaches to establish limits of detection and to ensure the required method accuracy were suggested. 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The experimental procedures that allow precise and quantitative analysis on different foods are relatively simple. For a better sensitivity and resolution, NMR spectroscopy is usually applied to liquid sample by means of extraction procedures that can be addressed to the observation of particular compounds. For the study of semisolid systems such as intact tissues, High-Resolution Magic Angle Spinning (HR-MAS) has received great attention within the biomedical area and beyond. Metabolic profiling and metabolism changes can be investigated both in animal organs and in foods. 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PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/17033055/H_HR_MAS_NMR_Spectroscopy_and_the_Metabolite_Determination_of_Typical_Foods_in_Mediterranean_Diet"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="7" data-entity-id="73418757" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/73418757/Nuclear_magnetic_resonance_spectroscopy_as_a_tool_to_study_carbohydrate_metabolism">Nuclear magnetic resonance spectroscopy as a tool to study carbohydrate metabolism</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="9294596" href="https://independent.academia.edu/PaulGreenhaff">Paul Greenhaff</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Proceedings of the Nutrition Society, 1994</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Nuclear magnetic resonance spectroscopy as a tool to study carbohydrate metabolism","attachmentId":81947778,"attachmentType":"pdf","work_url":"https://www.academia.edu/73418757/Nuclear_magnetic_resonance_spectroscopy_as_a_tool_to_study_carbohydrate_metabolism","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/73418757/Nuclear_magnetic_resonance_spectroscopy_as_a_tool_to_study_carbohydrate_metabolism"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="8" data-entity-id="118335706" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/118335706/Nuclear_Magnetic_Resonance_Spectroscopy_Applications_In_Foods">Nuclear Magnetic Resonance Spectroscopy Applications In Foods</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="49417325" href="https://netbim.academia.edu/NurayG%C3%BCzeler">Nuray Güzeler</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Current research in nutrition and food science, 2016</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Nuclear Magnetic Resonance Spectroscopy Applications In Foods","attachmentId":113987063,"attachmentType":"pdf","work_url":"https://www.academia.edu/118335706/Nuclear_Magnetic_Resonance_Spectroscopy_Applications_In_Foods","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/118335706/Nuclear_Magnetic_Resonance_Spectroscopy_Applications_In_Foods"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div><div class="ds-related-work--container js-wsj-grid-card" data-collection-position="9" data-entity-id="114669664" data-sort-order="default"><a class="ds-related-work--title js-wsj-grid-card-title ds2-5-body-md ds2-5-body-link" href="https://www.academia.edu/114669664/High_Resolution_NMR_Spectroscopy_as_a_Structural_and_Analytical_Tool_for_Unsaturated_Lipids_in_Solution">High Resolution NMR Spectroscopy as a Structural and Analytical Tool for Unsaturated Lipids in Solution</a><div class="ds-related-work--metadata"><a class="js-wsj-grid-card-author ds2-5-body-sm ds2-5-body-link" data-author-id="257268310" href="https://independent.academia.edu/siddiquihina">hina siddiqui</a></div><p class="ds-related-work--metadata ds2-5-body-xs">Molecules (Basel, Switzerland), 2017</p><p class="ds-related-work--abstract ds2-5-body-sm">Mono- and polyunsaturated lipids are widely distributed in Nature, and are structurally and functionally a diverse class of molecules with a variety of physicochemical, biological, medicinal and nutritional properties. High resolution NMR spectroscopic techniques including 1H-, 13C- and 31P-NMR have been successfully employed as a structural and analytical tool for unsaturated lipids. The objective of this review article is to provide: (i) an overview of the critical 1H-, 13C- and 31P-NMR parameters for structural and analytical investigations; (ii) an overview of various 1D and 2D NMR techniques that have been used for resonance assignments; (iii) selected analytical and structural studies with emphasis in the identification of major and minor unsaturated fatty acids in complex lipid extracts without the need for the isolation of the individual components; (iv) selected investigations of oxidation products of lipids; (v) applications in the emerging field of lipidomics; (vi) studie...</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"High Resolution NMR Spectroscopy as a Structural and Analytical Tool for Unsaturated Lipids in Solution","attachmentId":111305802,"attachmentType":"pdf","work_url":"https://www.academia.edu/114669664/High_Resolution_NMR_Spectroscopy_as_a_Structural_and_Analytical_Tool_for_Unsaturated_Lipids_in_Solution","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-wsj-grid-card-view-pdf" href="https://www.academia.edu/114669664/High_Resolution_NMR_Spectroscopy_as_a_Structural_and_Analytical_Tool_for_Unsaturated_Lipids_in_Solution"><span class="ds2-5-text-link__content">View PDF</span><span class="material-symbols-outlined" style="font-size: 18px" translate="no">chevron_right</span></a></div></div></div></div><div class="ds-sticky-ctas--wrapper js-loswp-sticky-ctas hidden"><div class="ds-sticky-ctas--grid-container"><div class="ds-sticky-ctas--container"><button class="ds2-5-button js-swp-download-button" data-signup-modal="{"location":"continue-reading-button--sticky-ctas","attachmentId":104903294,"attachmentType":"pdf","workUrl":null}">See full PDF</button><button class="ds2-5-button ds2-5-button--secondary js-swp-download-button" data-signup-modal="{"location":"download-pdf-button--sticky-ctas","attachmentId":104903294,"attachmentType":"pdf","workUrl":null}"><span class="material-symbols-outlined" style="font-size: 20px" translate="no">download</span>Download PDF</button></div></div></div><div class="ds-below-fold--grid-container"><div class="ds-work--container js-loswp-embedded-document"><div class="attachment_preview" data-attachment="Attachment_104903294" style="display: none"><div class="js-scribd-document-container"><div class="scribd--document-loading js-scribd-document-loader" style="display: block;"><img alt="Loading..." src="//a.academia-assets.com/images/loaders/paper-load.gif" /><p>Loading Preview</p></div></div><div style="text-align: center;"><div class="scribd--no-preview-alert js-preview-unavailable"><p>Sorry, preview is currently unavailable. 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Brosio</a></div><p class="ds-related-work--metadata ds2-5-body-xs">TrAC Trends in Analytical Chemistry, 1982</p><div class="ds-related-work--ctas"><button class="ds2-5-text-link ds2-5-text-link--inline js-swp-download-button" data-signup-modal="{"location":"wsj-grid-card-download-pdf-modal","work_title":"Pulsed low-resolution nuclear magnetic resonance — an analytical tool in food science","attachmentId":45459857,"attachmentType":"pdf","work_url":"https://www.academia.edu/25138977/Pulsed_low_resolution_nuclear_magnetic_resonance_an_analytical_tool_in_food_science","alternativeTracking":true}"><span class="material-symbols-outlined" style="font-size: 18px" translate="no">download</span><span class="ds2-5-text-link__content">Download free PDF</span></button><a class="ds2-5-text-link ds2-5-text-link--inline js-related-work-grid-card-view-pdf" href="https://www.academia.edu/25138977/Pulsed_low_resolution_nuclear_magnetic_resonance_an_analytical_tool_in_food_science"><span 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